Cholesterol‐imprinted polymer receptor prepared by a hybrid imprinting method

A novel cholesterol‐imprinted polymer (CMIP‐H) was prepared by a hybrid method of covalent imprinting and non‐covalent imprinting. This approach involves the copolymerization of a template‐containing monomer, cholesteryl 2‐hydroxyethyl methacrylate carbonate, and a cross‐linker, followed by hydrolysis to afford a flexible guest‐binding site accompanied with the easy and efficient removal of a ‘sacrificial spacer’. The effect of solvent on the binding capacity of CMIP‐H towards cholesterol was studied, indicating that a good binding capacity towards cholesterol could be achieved in a less‐polar solvent. The binding experiments of CMIP‐H towards a series of structural analogues of cholesterol, including cholesterol acetate, progesterone and stigmasterol, were carried out in hexane. The results showed that CMIP‐H almost did not bind cholesterol acetate at all because the hydrogen‐bonding site is blocked. It exhibited a similar binding towards both cholesterol and stigmasterol, but much higher binding towards progesterone. Copyright © 2005 Society of Chemical Industry     

Study of a BGO calorimeter using electron and hadron beams from 1 to 50 GeV

A calorimeter of 25 bismuth germanate (BGO) crystals equipped with silicon photodiode readout has been tested at the CERN SPS in the energy range 1–50 GeV. The response for electrons has been shown to be linear in this energy range and the rms resolution obtained ( ) is approximately 1%, for E > 4 GeV. The electron/pion separation was found to be better than 1:500 in the energy range 1–20 GeV. Data on lateral and longitudinal shower development were compared with the results of a Monte Carlo simulation using the SLAC-EGS program and found to be in good agreement.     

常宁市民营水电站运行管理模式初探

常宁市小水电资源主要蕴藏于境内东南山区,其地质结构以4～40中粒线变砂岩为主断裂带较少,结构稳定,特别适合小水电开发。目前国营小水电和民营小水电并驾齐驱,在一定程度上缓解了常宁市用电紧张局面。文章针对常宁市当前民营水电站在其发展过程中的存在一些困难和问题,对如何科学运行管理,发挥优势,克服弊端,最大限度、安全地创造经济效益和社会效益进行了探讨。     

近年来攀钢烧结工序采用的新技术

为了提高烧结矿强度、改善烧结矿粒度组成，提高烧结矿质量，对近年来攀钢烧结工序采用的一些新技术及其效果作了系统介绍。     

浅析异步电机电子软起动器的现状和展望

本文在分析异步电机电子软起动器的现状和展望的基础上，以一个当前正在设计完善的电子软起动器为例，基本说明新型电子软起动器的特点和结构功能。     

MIMO系统中简单的扩展空时块编码分集技术研究

本文提出一种多输入多输出（MIMO）天线系统中简单的扩展空时块编码（SSTBC）分集技术，采用沃尔什码来区分各天线发送数据子流。采用这种方法，在系统带宽一定时，不降低发送信息速率，同时接收机简单。不同天线的发送信息经过了所有收一发天线对之间的空间子信道，获得了所有路径的部分空间分集增益，仿真结果表明，这种增益的获得不受限于接收分集阶数，并且随发射天线的增加以一定的线性关系增加。     

超声波流量计计量系统性能的主要影响因素

随着我国天然气工业的发展，已有大量超声波流量计用于高压、大流量的天然气计量。尽管我国已于2001年颁布并实施了气体超声波流量计使用方面的国家标准GB/T18604-2001，但是随着超声波流量计越来越广泛的使用，国内外对超声波流量计计量性能的影响因素已有了进一步的研究；而且，目前我国超声波流量计在天然气计量中的应用效果也还需要进一步改善。因此，根据目前国、内外最新研究成果，对噪声、脏污、压力及温度测量对超声波流量计计量系统性能的主要影响因素以及控制对策进行了分析探讨，以期改变虽经实验室检定合格、但用于现场却不能达到预期计量性能效果的情况，使超声波流量计在现场能够得到更好的应用。     

Preparation of BaMgAl10O17∶Eu2+ and Its Phase Behavior in Microemulsion System

BaMgAl10O17∶Eu2 (BAM) was prepared in the microemulsion system and its phase behavior was studied. There exists a small region in the reverse microemulsion system where the dispersed particles are of spherical form. In this way, BAM blue phosphor with good dispersion can be synthesized. The microemulsion phase diagrams of the pseudo-ternary system (Triton X-100/cosurfactant-oil-BAM brine) were first established intuitively by the dilution method. The microstructure of microemulsions was determined through eyeballing, conductance technique, and polar optical microscopy. Its phase behavior is affected by various factors, such as temperature (room temperature, 30, 40 ℃), oil, surfactants, and cosurfactants in microemulsions. According to the phase diagrams, the microemulsion system of Triton X-100/1-hexanol-hexane-BAM brine was chosen to prepare the precursor. The BAM phosphor can be obtained via sintering the precursor at a comparatively low temperature. The phosphors were characterized by XRD and vacuum ultraviolet (VUV) spectra.     

绍兴市城区河道整治工程若干问题初探

通过对绍兴城区环城河、大环河、古运河、古城河等河道整治工程内容和整治成效的分析，总结了绍兴城区河道整治的5大特点，针对河道建设中存在的有关问题，提出了今后城市河道整治的4条具体措施。