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61.
Thermal,mechanical, and barrier properties of polyethylene/surlyn/organoclay nanocomposites blown films prepared by different mixing methods 下载免费PDF全文
Homayoon Hosseinkhanli Jamal Aalaie Mahdi Abdollahi Talat Khalkhali Mehrdad Shojaei 《乙烯基与添加剂工艺杂志》2015,21(1):60-69
(Low‐density polyethylene) (LDPE)/clay nanocomposites were prepared by melt blending in a twin‐screw extruder by using different mixing methods. Zinc‐neutralized carboxylate ionomer was used as a compatibilizer. Blown films of the nanocomposites were then prepared. The effect of mixing method on the clay dispersion and properties of the nanocomposites was evaluated by wide‐angle X‐ray diffraction analysis, mechanical properties, thermal properties, and barrier properties. The structure and properties of nanocomposites containing different amounts of nanoclay prepared by selected mixing techniques were also investigated. It was found that melt compounding of Surlyn/clay masterbatch with pure LDPE and Surlyn (two‐step‐a method) results in better dispersion and intercalation of the nanofillers than melt mixing of LDPE/Surlyn/clay masterbatch with pure LDPE and surlyn (two‐step‐b method) and direct mixing of LDPE with clay. The films containing ionomer have good barrier properties. A wide‐angle X‐ray diffraction pattern indicates that intercalation of polymer chains into the clay galleries decreases by increasing the clay content. Barrier properties and tensile modulus of the films were improved by increasing the clay content. In addition, tensile strength increased in the machine direction, but it decreased in the transverse direction by increasing the clay content. DSC results showed that increasing the clay content does not show significant change in the melting and crystallization temperatures. The results of thermogravimetric analysis showed that the thermal stability of the nanocomposites decreased by increasing the clay content more than 1 wt%. J. VINYL ADDIT. TECHNOL., 21:60–69, 2015. © 2014 Society of Plastics Engineers 相似文献
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Amir Movafeghi Yahaghi Effat Rokrok Behrouz Mirzapour Mahdi 《Russian Journal of Nondestructive Testing》2020,56(4):361-368
Russian Journal of Nondestructive Testing - The location of reinforcement bar in concrete, the bar corrosion, diameter and the depth below the surface are important factors in the evaluation of the... 相似文献
63.
Ligand‐Free Synthesis of Aluminum‐Doped Zinc Oxide Nanocrystals and their Use as Optical Spacers in Color‐Tuned Highly Efficient Organic Solar Cells 下载免费PDF全文
Meriem Gaceur Sadok Ben Dkhil David Duché Fatima Bencheikh Jean‐Jacques Simon Ludovic Escoubas Mahdi Mansour Antonio Guerrero Germà Garcia‐Belmonte Xianjie Liu Mats Fahlman Walid Dachraoui Abdou Karim Diallo Christine Videlot‐Ackermann Olivier Margeat Jörg Ackermann 《Advanced functional materials》2016,26(2):243-253
The color of polymer solar cells using an opaque electrode is given by the reflected light, which depends on the composition and thickness of each layer of the device. Metal‐oxide‐based optical spacers are intensively studied in polymer solar cells aiming to optimize the light absorption. However, the low conductivity of materials such as ZnO and TiO2 limits the thickness of such optical spacers to tenths of nanometers. A novel synthesis route of cluster‐free Al‐doped ZnO (AZO) nanocrystals (NCs) is presented for solution processing of highly conductive layers without the need of temperature annealing, including thick optical spacers on top of polymer blends. The processing of 80 nm thick optical spacers based on AZO nanocrystal solutions on top of 200 nm thick polymer blend layer is demonstrated leading to improved photocurrent density of 17% compared to solar cells using standard active layers of 90 nm in combination with thin ZnO‐based optical spacers. These AZO NCs also open new opportunities for the processing of high‐efficiency color tuned solar cells. For the first time, it is shown that applying solution‐processed thick optical spacer with polymer blends of different thicknesses can process solar cells of similar efficiency over 7% but of different colors. 相似文献
64.
Seied Mahdi Pourmortazavi Mehdi Rahimi-Nasrabadi Ali Akbar Davoudi-Dehaghani Abdollah Javidan Mir Mahdi Zahedi Seiedeh Somayyeh Hajimirsadeghi 《Materials Research Bulletin》2012,47(4):1045-1050
Taguchi robust design was used for optimization of direct precipitation reaction conditions in order to simple and fast synthesis of manganese carbonate nanoparticles. Manganese carbonate nanoparticles were synthesized in this study by addition of manganese ion solution to the aqueous carbonate reagent. Effects of several reaction variables, such as manganese and carbonate concentrations, flow rate of reagent addition and temperature on particle size of prepared manganese carbonate were investigated. The significance of these parameters in tuning the size of manganese carbonate particles was quantitatively evaluated by analysis of variance. The results showed that manganese concentration and carbonate concentration in the solutions and also flow rate have significant effects in preparation of manganese carbonate nanoparticles. Also, optimum conditions for synthesis of manganese carbonate nanoparticles via precipitation reaction were proposed. Analysis of variance showed that under the optimum condition, the size of manganese carbonate nanoparticles will be about 54 ± 12 nm. In another part of this study, solid state thermal decomposition reaction of precursor was used for preparation of Mn2O3 nanoparticles. The results showed that Mn2O3 nanoparticles synthesized via thermal decomposition of manganese carbonate nanoparticles have average size of 90 nm. 相似文献
65.
In this paper, all-optical tunable filters based on two-dimensional photonic crystals with very small dimensions for optical telecommunication of WDM technology are designed and simulated. The structure is made of air holes in a dielectric background. The tuning is done by changing resonant defect angle. The channels obtained for this structure will be set in wavelength range of 1550 nm. Created channels are at wavelengths of 1550, 1551, 1552, and 1565 (16 channels); the distance between adjacent channels is 1 nm. Design and simulation of this filter is done by RSOFT software. Quality factor, transmission efficiency, and band gap shows that filter performance is very good. 相似文献
66.
Microfluidic Manipulation of Core/Shell Nanoparticles for Oral Delivery of Chemotherapeutics: A New Treatment Approach for Colorectal Cancer 下载免费PDF全文
Mohammad Mahdi Hasani‐Sadrabadi Shahrouz Taranejoo Erfan Dashtimoghadam Ghasem Bahlakeh Fatemeh Sadat Majedi Jules John VanDersarl Mohsen Janmaleki Fatemeh Sharifi Arnaud Bertsch Kerry Hourigan Lobat Tayebi Philippe Renaud Karl I. Jacob 《Advanced materials (Deerfield Beach, Fla.)》2016,28(21):4134-4141
67.
Mostafa Rezazadeh Shirdar Mohammad Mahdi Taheri Izman Sudin Arezou Shafaghat Muhd Zaimi Abd. Majid 《Journal of Experimental Nanoscience》2016,11(10):816-822
ABSTRACTThe present study is an investigation to demonstrate the effectiveness of in situ approach in the synthesis of hydroxyapatite-grafted titanium nanotube composite (HA-TNT). This method involves combining the process of HA sol–gel and rapid breakdown anodisation of titanium in a novel solution consisting of NaCl and N3PO4. This new synthesis approach produced a uniform dispersion of Anatase and Rutile phases of TiO2 nanotubes with minimal agglomeration in the matrix of crystalline HA. The characterisation of homogenised HA-TNT composite was investigated via field emission scanning electron microscopy (FESEM), energy dispersive spectroscopy (EDS), transmission electron microscope (TEM) and X-ray diffraction (XRD). FESEM and TEM images indicated the nanostructure of composite with TiO2 nanotube diameter of approximately 10 nm. XRD and EDS analyses confirmed the formation of HA crystalline with the Ca/P ratio of 1.58 and formation of Anatase and Rutile phase of TiO2 nanotubes. 相似文献
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