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81.
Akinori Sawada Yuji Masubuchi Teruki Motohashi Shinichi Kikkawa 《Journal of the American Ceramic Society》2014,97(5):1356-1358
Amorphous thin films of Ti1?ySiy(N,O) with y ≥ 0.38 were prepared by reactive sputter deposition in a nitrogen atmosphere. Thermal annealing of the films in an ammonia flow above 800°C yielded Si(N,O) amorphous thin films dispersed with precipitated TiN nanosized particles. The film color changed with Si content y and the annealing conditions, from carrot orange to cream yellow in the as‐deposited films due to their oxynitride nature, and from dark green to canary yellow and from iron blue to horizon blue at respective annealing temperatures of 800°C and 900°C due to metallic nature of the TiN nanosized particles precipitated in the annealing. 相似文献
82.
Stress-corrosion lives and pitting potentials of Al---4%Cu alloys with various aging structures have been measured in de-aerated 1M NaCl under conditions of controlled potential. It was found that the alloys aged having the higher susceptibility to stress-corrosion cracking showed two pitting potentials corresponding to pitting at grain boundaries and grain bodies, respectively. The susceptibility to stress corrosion cracking of the alloys appeared above the pitting potentials for grain boundaries. The maximum susceptibility to stress-corrosion cracking was obtained when the alloy was aged to attain the largest difference in pitting potentials between grain boundaries and grain bodies. 相似文献
83.
JIAHong-bo CHENBao-xue ZHOUJian-zhong ZHAODe-xir LUHong-liang YUANYi-fang ISOMamoru 《半导体光子学与技术》2004,10(1):21-27
Based on the measurement of dispersion characteristic and birefractive index of the fluorinated polyimide film,a statistical optimum design method is proposed and used to realize the design of 32-and 36-wavelengths optical waveguide wavelength-interleave coupler (i,e.,interleaver) with the optimization of polarization fluctuation and wavelength interval of 0.8nm at 1550nm. The largest cross coupling ratios of the two interleavers are respectively less than 1.8% and 3.5%, while the least through coupling ratios are respectively greater than 98. 2% and 96. 5%. The output differences due to polarization fluctuation are less than 1.7% and 3.2% 相似文献
84.
Hideo Sawada Sachiko HataNobuhito Kawasaki Jun-ichi IidzukaKentaro Tokugi Jun KyokaneTomomi Maekawa Tokuzo Kawase 《Polymer》2002,43(3):1035-1038
New fluoroalkyl end-capped fullerene cooligomers were prepared by the reactions of fluoroalkanoyl peroxides with fullerene and comonomers such as acryloylmorpholine, N,N-dimethylacrylamide and acrylic acid. These fluorinated fullerene cooligomers were easily soluble in water and common organic solvents, and were able to reduce the surface tensions of both water and benzene, quite effectively. Additionally, these fullerene cooligomers were found to form a stable monomolecular film at the air-water interface, and the modified polystyrene surface treated with these cooligomers was shown to have a strong hydrophilicity with good oil repellency. 相似文献
85.
Techniques are introduced to solve two problems caused by the wide bandwidth of HDTV signals. One problem is that HDTV signals have more random noise than conventional TV signals, which causes coding efficiency degradation. The other is that very high sampling frequencies are required, which restricts the hardware implementation of the coding algorithm. To solve the first problem, it is proposed to use a spatio-temporal adaptive filter that can reduce random noise and improve coding efficiency. With regard to the second problem, an extrapolative and interpolative coding algorithm with adaptive intrafield/interframe prediction is presented. This algorithm eliminates the problem caused by the high sampling frequencies and provides efficient coding performance. A computer simulation is carried out to estimate the coding performance. Based on the simulation results, experimental coder hardware was implemented for 1125-line/60 Hz HDTV signals in order to evaluate real-time coding performance. The experimental results show that this coding method can provide good picture quality at around 90 or 135 Mb/s, and that HDTV digital transmission is very promising at the broadband ISDN H4 rate 相似文献
86.
Rong-Jun Xie Naoto Hirosaki Mamoru Mitomo Takayuki Suehiro Xin Xu Hidehiko Tanaka 《Journal of the American Ceramic Society》2005,88(10):2883-2888
Rare-earth-doped Ca-α-SiAlON phosphors, with the compositions of (Ca1−3/2 x RE x ) m /2 Si12− m − n Al m+n O n N16− n (RE=Ce, Sm, and Dy, 0.5≤ m =2 n ≤3.0), were prepared by sintering at 1700°C for 2 h under 10 atm N2 . The concentration of rare earths varied from 3 to 30 at.% with respect to Ca. The photoluminescence (PL) properties were investigated as functions of the composition of the host matrix (i.e., m ) and the concentration of rare earths (i.e., x ). The results show that the emission properties can be optimized by tailoring m and x . The Ce3+ luminescence originating from the 4 f –5 d interconfigurational transitions is greatly affected by the environment surrounding the Ce3+ ions, which differs from the Sm3+ or Dy3+ luminescence arising from the 4 f –4 f intraconfigurational transitions. X-ray diffraction and scanning electron microscopy were used to explain the composition and concentration dependence of PL properties. 相似文献
87.
88.
89.
Chie Ando Toshimasa Suzuki Youichi Mizuno Hiroshi Kishi Sayuri Nakayama Mamoru Senna 《Journal of Materials Science》2008,43(18):6182-6192
In an attempt to obtain finest possible microparticles of BaTiO3 (BT) with highest possible tetragonality via a solid state route, starting mixtures comprising BaCO3 and TiO2 were subjected to various pretreatments including addition of glycine and mechanical activation. Reaction processes were
monitored by the changes in the weight, crystallinity, and morphology in detail. While mechanical activation with glycine
significantly increased the rate of reaction and homogeneity of the particle size of the product, BT, simultaneous particle
growth of BT was intolerably acute for micro-electronic devices. The fast particle coarsening was predominated by the coalescence
of BT tiny particles formed around titania. A mixture with higher homogeneity was attained by using finer starting materials
under wet mixing, avoiding significant mechanical stressing. Particle growth of BT was suppressed to ca. 100 nm to obtain
fully crystallized BT particles without significant loss of tetragonality and, hence, close to meet our requirements for MLCCs. 相似文献
90.
Conditions for synthesizing acicular fine particles of goethite with high aspect ratio were devised by oxidizing mixed slurry
comprising ferrous carbonate and hydroxide after neutralizing by alkali carbonate. By bubbling N2 after neutralization into the slurry containing FeCO3 and Fe(OH)2, dissolved CO2 is ejected. As a consequence, the relative concentration of CO32− decreases and that of hydroxide increases. These favor the increase of the aspect ratio of the goethite particles via two
factors, i.e., (1) decrease in the critical size of the nuclei and (2) suppression of growth inhibition at the tip of needle-like
particles due to CO32− adsorption. We propose a reaction scheme for the entire processing. 相似文献