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101.
Summary Well-defined water-soluble poly(styrenesulfonate)-b-poly(ethylene glycol)-b- poly(styrenesulfonate) (PSS-b-PEG-b-PSS) triblock
copolymers with narrow molecular weight distribution (1.29 < Mw/Mn < 1.36) were synthesized in aqueous solution at 70 oC via reversible addition-fragmentation chain transfer (RAFT) polymerization. The complex formed by the PSS-b-PEG-b-PSS triblock
copolymer coordinated with aluminum ion was investigated with turbidimetry, dynamic light scattering (DSL), zeta-potential,
and transmission electron microscopy (TEM). The aggregation formation was based on the neutralization of the SO3- groups in the PSS blocks with Al3+ ions. The appearance, size and stability of the PSS-b-PEG-b-PSS/Al3+ aggregates were controlled by varying the PSS block length and degree of neutralization (DN). At DN = 0.33, where the PSS-b-PEG-b-PSS
copolymer was completely neutralized with Al3+, the aggregate size increased with increasing PSS block length. The transition from the shrinking coil of small size to the
interchain aggregates of large size was found at DN of about 0.33. 相似文献
102.
Modellierung in der Lehre an Hochschulen: Thesen und Erfahrungen 总被引:1,自引:1,他引:0
Martin Glinz 《Informatik-Spektrum》2008,31(5):425-434
Zusammenfassung Nicht erst seit Modellierung zum Modewort geworden ist, ist Modellierung ein wichtiges Thema in der Informatikausbildung.
Dieser Beitrag beleuchtet in zw?lf Thesen das Warum, Was, Wie viel, Wo, Wann und Wie von Modellierung in der Lehre im Rahmen
informatikbezogener Studieng?nge. Die Thesen basieren auf der Erfahrung des Verfassers mit einer seit über zehn Jahren gehaltenen
Modellierungsvorlesung an der Universit?t Zürich sowie dem Gedankenaustausch mit anderen Hochschullehrerinnen und -lehrern
im Rahmen der GI-Workshopreihe ,,Modellierung“. Zus?tzlich liefert eine Befragung von Absolventinnen und Absolventen an der
Universit?t Zürich empirische Evidenz für eine Reihe der Thesen. 相似文献
103.
This paper will describe the solid oxide membrane (SOM) process as it applies to the energy-efficient and environmentally
sound production of magnesium from magnesium oxide. Also, it will describe the challenges encountered while using this process
for the production of transition metals like titanium from its higher oxides. Finally, a novel magnesiothermic SOM process
will be proposed that can enable production of transition metals from its higher oxides. 相似文献
104.
Do Hoon Kim Umme Farva Woo Sik Jung Eui Jung Kim Chinho Park 《Korean Journal of Chemical Engineering》2008,25(5):1184-1189
This paper reports an alternative method for the growth of GaN epitaxial layer on (0001) Al2O3 substrate by hot-wall vapor phase epitaxy technique. Tris (N,N-dimethyldithiocarbamato)-gallium (III), Ga(mDTC)3 was introduced as a precursor material for the seed layer formation in the growth of GaN. Optimal growth conditions with
seed layers formed by the Ga(mDTC)3 concentration of 0.047 mol/L were identified: Growth temperature was found to be 850 °C, and optimal distance between the
reactant outlet and substrate was determined to be 12.5 cm. Characterization results showed that this growth method produce
high-crystallinity GaN epitaxial layers at a relatively lower growth temperature compared to the existing growth techniques
and simplify the growth process. 相似文献
105.
The rate of filtration and the water content of cake are influenced by the existence of a dense skin in a highly compressible
cake. The phenomenon of the dense skin has been rarely studied, and its existence has not been verified experimentally. In
this study, the porosity variation in a very compressible cake is measured by using a new experimental apparatus, and with
this the existence of dense skin has been established experimentally. ‘Unified theory on solid-liquid separation’, a recently
developed theory, is utilized for calculating the porosity variation in a very compressible cake. 相似文献
106.
Camelia Betianu Florentina A Caliman Maria Gavrilescu Igor Cretescu Corneliu Cojocaru Ioannis Poulios 《Journal of chemical technology and biotechnology (Oxford, Oxfordshire : 1986)》2008,83(11):1454-1465
BACKGROUND: Heterogeneous photocatalysis is influenced by a number of parameters involving synergistic effects; hence, an experimental strategy design that considers interactions between the main variables is needed. The response surface methodology was applied for the investigation of photodegradation of 20 mg L?1 Orange II in aqueous solutions and for optimization of color removal efficiency. Preliminary studies were performed to identify the parameters to be selected for optimization. RESULTS: The input variables considered for experimental design were: solution initial pH, oxidizing agent (H2O2) initial concentration and UV‐A irradiation time. The multivariate experimental design allowed the development of a quadratic response surface model to be used for the prediction of color removal efficiency over the full range of the experimental region. Under the optimum conditions established in the region of experimentation (pH = 6.9, [H2O2]0 = 183 mg L?1 and t = 32 min), a 100% color removal efficiency was obtained in experiments. CONCLUSIONS: It was found that the variables considered have important effects on color removal efficiency. The results demonstrate that the use of experimental design strategy is indispensable for successful investigation and adequate modeling of the process because the interdependence of the reaction parameters cannot be neglected. Copyright © 2008 Society of Chemical Industry 相似文献
107.
108.
Chih-Chun Hsieh Tao-Chih Chang Dong-Yih Lin Ming-Che Chen Weite Wu 《Metals and Materials International》2007,13(5):411-416
The purpose of this study is to investigate the precipitation characteristics of σ phase in the fusion zone of stainless steel
welds at various welding passes during a tungsten are welding (GTAW) process. The morphology, quantity, and chemical composition
of the δ-ferrite and σ phase were analyzed using optical microscopy (OM), a ferritscope (FS), a X-ray diffractometer (XRD),
scanning electron microscopy (SEM), an electron probe micro-analyzer (EPMA), and a wavelength dispersive spectrometer (WDS),
respectively. Massive δ-ferrite was observed in the fusion zone of the first pass welds during welding of dissimilar stainless
steels. The σ phase precipitated at the inner δ-ferrite particles and decreased δ-ferrite content during the third pass welding.
The σ and δ phases can be stabilized by Si element, which promoted the phase transformation of σ→ϱ+λ2 in the fusion zone of the third pass welds. It was found that the σ phase was a Fe−Cr−Si intermetallic compound found in
the fusion zone of the third pass welds during multi-pass welding. 相似文献
109.
Ivan Cimrák 《Archives of Computational Methods in Engineering》2007,15(3):277-309
The Landau-Lifshitz (LL)equation of micromagnetism governs rich variety of the evolution of magnetization patterns in ferromagnetic
media. This is due to the complexity of physical quantities appearing in the LL equation. This complexity causes also an interesting
mathematical properties of the LL equation: nonlocal character for some quantities,nonconvex side-constraints, strongly nonlinear
terms. These effects influence also the numerical approximations. In this work, recent developments on the approximation of
weak solutions, together with the overview of well-known methods for strong solutions,are addressed.
Author is supported by the Fund for Scientific Research - Flanders FWO (Belgium). 相似文献
110.