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Titanium oxides were reduced to metallic titanium using the liquid calcium floating on the molten CaCl2. A part of Ca dissolved into CaCl2 and reacted with TiO2 settled below CaCl2. The by-product CaO also dissolved by about 20 mol pct into CaCl2, which was effective in reducing the oxygen concentration in the obtained Ti particles. The compositional region in the Ca-CaCl2-CaO system was examined for the less oxygen contamination in Ti and the better handling in leaching. A large amount of the
residual calcium oxidized the titanium powder in leaching. The metallic Ti powder less than 1000 mass ppm oxygen could be
obtained only for 3.6 ks using 5 to 7 mol pct Ca-CaCl2 at 1173 K. The powder was slightly sintered like sponge, and contained approximately 1500 ppm Ca. The anatase phae, the intermediate
product in the refining process of TiO2, could be also supplied as raw material as well as rutile. 相似文献
139.
The corrosion behaviour of nitrogen-containing austenitic stainless steel in methanol containing different concentrations
of H2SO4, HCl, LiCl and H2SO4 + HCl has been investigated using a potentiostatic polarization method. The cathodic reaction in the H2SO4, HCl and H2SO4 + HCl solutions was proton reduction whereas in the neutral LiCl solution, oxygen reduction was the predominant cathodic
reaction. Active, passive and transpassive behaviours were observed only for higher concentrations of H2SO4 (0.01–2.0 M) due to the inherent water content. A cathodic loop, characterized by measured negative current in the anodic
region, was also observed in solutions, in which the concentration of H2SO4 was 1.0 M or higher. The relative stability of the passive films decreased as the H2SO4 concentration increased, and thus the steel suffered from mild pitting corrosion. In the chloride environment, the rate of
corrosion increased as the Cl− ion concentration increased. The presence of acid along with Cl− ions enhanced corrosion, and the corrosion rate increased significantly. The steel suffered from mild intergranular corrosion
in acidic chloride solutions of methanol. In the H2SO4 + HCl solutions, passive films were only formed when the H2SO4 to HCl concentration ratio was greater than ∼10:1. 相似文献
140.
In this study, nanocrystalline Ni powders and thermally sprayed coatings, containing ultrafine AlN particles, were synthesized
and characterized. The results indicated that the presence of AlN particles in the powders drastically decreased the dimension
of agglomerates formed by cryomilling and increased the surface roughness of the agglomerates. The AlN phase was broken down
into ultrafine particles of approximately 30 nm in size. These particles were dispersed in the Ni matrix and enhanced the
development of a nanocrystalline structure in the Ni matrix during cryomilling. Selected-area diffraction patterns, obtained
from transmission electron microscopy (TEM) and X-ray mapping with scanning electron microscopy (SEM), confirmed the presence
of AlN particles in the coatings. The presence of AlN particles also led to an increase in the amount of NiO phase that was
distributed in the coating, in the form of ultrafine, round particles. AlN particles increased the microhardness of the Ni
coating by approximately 60 pct. Indentation-fracture results also indicated that the fine, dispersed AlN particles raised
the apparent toughness of the Ni coating. The synthesized Ni coatings containing ultrafine AlN particles were characterized
as equiaxed nanocrystalline grains with an average size of 24 nm, in which twins were observed. The increase in microhardness
resulted from both grain refinement and the presence of ultrafine particles. The latter played the primary role in strengthening. 相似文献