Soft magnetic properties of NiFeTa thin films for biasing film applications in magnetoresistive elements

The effects of Ta addition on the magnetic properties of permalloy thin films have been investigated. The alloy compositions on a weight basis are (Ni₈₁Fe₁₉)_1-x Ta _x with 0 x 0.105, and the films are sputtered onto a glass substrate at between room temperature and 300 C. The saturation magnetization and anisotropic magnetic field decrease with increasing Ta content. The saturation magnetization is 0.75 T at 5 wt % Ta. The coercivity remains constant at 125 Am^-1. The electrical resistivity increases linearly with increasing Ta content, then saturates at approximately 7.5 wt% Ta. The saturation resistivity is approximately 1.00 m. The magnetoresistivity ratio (/) decreases with increasing Ta content, mainly due to increased electrical resistivity (). The magnetostriction changes from negative to positive with increasing Ta content and reaches nearly zero at 2 wt% Ta. The NiFeTa films containing 5–6 wt% Ta have potential for use as the soft-biasing film in magnetoresistive elements.     

Discharge properties and chemical stability of SrZrO films

Abstract— MgO thin film is currently used as a surface protective layer for dielectric materials because MgO has a high resistance during ion sputtering and exhibits effective secondary electron emission. The secondary‐electron‐emission coefficient γ of MgO is high for Ne ions; however, it is low for Xe ions. The Xe content of the discharge gas of PDPs needs to be raised in order to increase the luminous efficiency. Thus, the development of high‐γ materials replacing MgO is required. The discharge properties and chemical surface stability of SrO containing Zr (SrZrO) as the candidate high‐γ protective layer for noble PDPs have been characterized. SrZrO films have superior chemical stability, especially the resistance to carbonation because of the existence of a few adsorption sites due to their amorphous structure. The firing voltage is 60 V lower than that of MgO films for a discharge gas of Ne/Xe = 85/15 at 60 kPa.     

Retrieval of clothing images based on relevance feedback with focus on collar designs

The content-based image retrieval methods are developed to help people find what they desire based on preferred images instead of linguistic information. This paper focuses on capturing the image features representing details of the collar designs, which is important for people to choose clothing. The quality of the feature extraction methods is important for the queries. This paper presents several new methods for the collar-design feature extraction. A prototype of clothing image retrieval system based on relevance feedback approach and optimum-path forest algorithm is also developed to improve the query results and allows users to find clothing image of more preferred design. A series of experiments are conducted to test the qualities of the feature extraction methods and validate the effectiveness and efficiency of the RF-OPF prototype from multiple aspects. The evaluation scores of initial query results are used to test the qualities of the feature extraction methods. The average scores of all RF steps, the average numbers of RF iterations taken before achieving desired results and the score transition of RF iterations are used to validate the effectiveness and efficiency of the proposed RF-OPF prototype.     

An adaptive observer for a spacecraft–manipulator system using a camera mounted on its spacecraft

This paper deals with a motion control system for a space robot with a manipulator. Many motion controllers require the positions of the robot body and the manipulator hand with respect to an inertial coordinate system. In order to measure them, a visual sensor using a camera is frequently used. However, there are two difficulties in measuring them by means of a camera. The first one is that a camera is mounted on the robot body, and hence it is difficult to directly measure the position of the robot body by means of it. The second one is that the sampling period of a vision system with a general-purpose camera is much longer than that of a general servo system. In this paper, we develop an adaptive state observer that overcomes the two difficulties. In order to investigate its performance, we design a motion control system that is constructed by combining the observer with a PD control input, and then conduct numerical simulations for the control system. Simulation results demonstrate the effectiveness of the proposed observer.     

Defect distribution near abraded surface of III–V compound semiconductors

Microstructures of damaged layers near the abraded surface of GaP, GaAs_0.6P_0.4 and GaAs single crystals have been observed with a transmission electron microscope. The damage due to 0.3 m Al₂O₃ abrasion consists of dislocations. Dislocation densities in the abrasion band and other regions are larger than 5×10¹¹ cm^–2 and about 10¹¹ cm^–2, respectively. Dislocation density decreases with increasing distance (depth) from the abraded surface. The depths of the damage layers for GaP, GaAs_0.6P_0.4 and GaAs are about 0.4, 0.55, and 0.8 m, respectively. The Burgers vector of dislocations is a/2[1 1 0], and A and B dislocations are observed. During annealing, the dislocations are rearranged and eliminated by the reaction of the dislocations with different Burgers vectors and climbing motion. The rearrangement temperatures for dislocations in GaP and GaAs are about 500 and 450° C, respectively. Electrical resistance changes in the damaged layer of GaP are recognized by electrical resistance measurements.     

Dielectric Dispersion of Polycrystalline Aluminum Nitride at Microwave Frequencies

Complex permittivity of polycrystalline AlN was measured over the frequency range 100 MHz to 13 GHz using reflection coefficient and cavity resonator methods. Dielectric relaxation peaks of loss tangent were observed in the frequency range 200 MHz to 3 GHz. The maximum value of loss tangent was ∼200 × 10⁻⁴. Relative permittivities decreased by ∼4% with increased frequency at the region of relaxation peaks. It was shown that these dispersion frequencies were inversely proportional to the grain sizes of AlN and independent of purities and processes. Model calculations for elastic vibration of a single-crystal grain of AlN were performed to investigate the origin of the dielectric dispersion due to piezoelectric effect. The calculated results of elastic sphere and 14-faced-polyhedron models showed a good quantitative agreement with the observed dispersion frequencies, which suggested that the dispersion was due to a piezoelectric vibration of a single grain of AlN ceramics at microwave frequencies.     

Strength Analysis of Yttria-Stabilized Tetragonal Zirconia Polycrystals

Tensile strength of Y₂O₃-stabilized ZrO₂ polycrystals (Y-TZP) was measured by a newly developed tensile testing method with a rectangular bar. The tensile strength of Y-TZP was lower than that of the three-point bend strength, and the shape of the tensile strength distribution was quite different from that of the three-point bend strength distribution. It was difficult to predict the distribution curve of the tensile strength using the data of the three-point bend strength by one-modal Weibull distribution. The distribution of the tensile strength was analyzed by two- or three-model Weibull distribution coupled with an analysis of fracture origins. The distribution curve of the three-point bend strength which was estimated by multimodal Weibull distribution agreed favorably with that of the measured three-point bend strength values. A two-modal Weibull distribution function was formulated approximately from the distributions of the tensile and three-point bend strengths, and the estimated two-modal Weibull distribution function for the four-point bend strength agreed well with the measured four-point bend strength.     

Colorimetric microdetermination of sulphites in foods by use of the modified rankine apparatus. IV.

Summary Detection and determination of traces of sulphites in foods was attempted by use of the modified Rankine apparatus and pararosaniline colorimetry. Replacement of alkaline titration reported previously by pararosaniline colorimetry lowered the absolute detection limit from 30 g (titration method) to 2 g. In view of clean analysis, in the color developing system, 0.1 N-sodium hydroxide was used in place of mercuric chloride solution commonly used as an absorbant of sulphites. In order to prevent oxidative decomposition of sulphites during operation, nitrogen gas was used as carrier instead of air. Dimedone and sodium azide were used for the elimination of aldehydes and nitrites, respecitvely, in the sample, which will disturb the color development of sulphites with pararosaniline-formaldehyde reagents. With this improved method, it was possible to determine the residual sulphites in frozen peeled shrimps, sugared beans and other foods with low sulphite contents accurately.

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Colorimetrische Mikrobestimmung von Sulfiten in Lebensmitteln bei Anwendung der modifizierten IV. Rankine Apparatur

Zusammenfassung Geringe Sulfitmengen in Lebensmitteln (geschälte Garnelen, gezuckerte Bohnen) können colorimetrisch bestimmt werden. Die neuentwickelte Methode beruht auf einer Kombination von colorimetrischer Bestimmung mittels p-Rosanilin und der Bestimmungsmethode nach Rankine. Auf diese Weise lassen sich Gehalte von 2 g noch genau bestimmen. Bei der Farbentwicklung wurde das giftige Quecksilbertetrachlorid durch 0.1 n-NaOH ersetzt, anstelle von Luft Stickstoff als Trägergas verwendet und somit eine Oxydation des Sulfits während der Bestimmung vermieden. Da Nitrit und Aldehyde die Farbentwicklung stören, wurde ihr Einfluß durch Dimedon und Natriumazid ausgeschaltet.

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Studies on the Analyses of Sulphites in Foods (IV)     

Hot-water treatment of sol–gel derived SiO2–TiO2 microparticles and application to electrophoretic deposition for thick films

SiO₂–TiO₂ spherical microparticles of about 0.7 μm in diameter were prepared by the sol–gel method. Anatase nanocrystals were formed in the microparticles and their specific surface area was increased after a hot-water treatment at 90 °C. From the changes in the concentration of I₂ photocatalytically generated from KI aqueous solution, the activity of the SiO₂–TiO₂ microparticles was found to increase with increasing the hot-water treatment time. Particulate, thick films were electrophoretically deposited on indium tin oxide (ITO)-coated glass substrates using the anatase nanocrystal-precipitated SiO₂–TiO₂ microparticles. The thickness of the electrophoretically deposited particulate film increased to be approximately 10 μm with an increase in applied voltage. The resultant thick film showed a high photocatalytic activity.     

Experimental study of perforation and cracking of water-filled aluminum tubes impacted by steel spheres

Water-filled aluminum tubes were subjected to impact by six steel spherical projectiles of different diameters at impact velocities of 40–200 m/s. The effects of the diameter of the steel projectiles and of the material properties of the tubes on cracking and perforation were discussed. Water decreased the wall strength of the aluminum alloy tubes, and the impact velocity at which a steel projectile first passes through the tube wall decreased with increasing diameter of the steel projectile. Using the velocity at which the steel projectile perforates the tube wall, empirical equations of the energies required to perforate the tube wall were derived. Also, the energy balance in the steel projectile during a collision is discussed referring to the pressure history in the filled water and the velocities of the steel projectile before and after collision.