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61.
Daniel S. Camarda Matthew J. Lampe Alan J. Lesser Philippe Desbois Klaus Stoll Claus Gabriel Rupert Konradi 《应用聚合物科学杂志》2021,138(41):51203
The creation of graft copolymers by selectively grafting a second polymer to the amorphous fraction of a semi-crystalline polymer in supercritical CO2 is demonstrated herein. The graft copolymer is synthesized by free radical polymerization of a vinyl monomer within the semi-crystalline polymer below its melt temperature. Such conditions afford selective grafting on the amorphous regions (block “B”) while leaving the crystalline domains (block “A”) unmodified. Accordingly, unique A-B, A-B-A, A-B-A-B-A, and so forth. block structures are formed. In this work, styrene is polymerized within polyamide 6, polyethylene terephthalate, and isotactic polypropylene. Purification of these material is performed to remove the un-grafted homopolymer, allowing for determination of the graft yield, the portion of polymer which covalently bonds to the semi-crystalline matrix. Grafting yields achieved in polyamide 6, polyethylene terephthalate, and isotactic polypropylene were 98%, 59%, and 15%, respectively. Property enhancements were observed upon further characterization of polystyrene-polyamide 6 copolymers, including high glass transition temperatures, the ability to be remelted, and tunable grafting molecular weight. Additionally, hydrophobicity is controlled by varying polystyrene composition. The remarkable range of accessed properties demonstrates this as a potential route to upcycling plastics. 相似文献
62.
Michael P. Balogh Camille Y. Jones J.F. Herbst Louis G. Hector Jr. Matthew Kundrat 《Journal of Alloys and Compounds》2006,420(1-2):326-336
Half-Heusler compounds of Sn-doped TiCoSb “TiCoSnxSb1−x (x = 0.0, 0.01, and 0.05)” were prepared and their thermoelectric properties were measured above room temperature. From the EDX analysis, all the samples have three phases: the TiCoSnxSb1−x, Co-rich, and Ti-rich phases. The values of the thermoelectric power increase with Sn doping, and a positive thermoelectric power is obtained in the sample of TiCoSn0.05Sb0.95. The thermal conductivity decreases both with increasing temperature and with Sn content. The maximum value of ZT for p-type material is 0.030 at 988 K in the sample of TiCoSn0.05Sb0.95. 相似文献
63.
Chloride rich reinforced concrete prisms were coupled to chloride-free prisms and exposed to diurnal and seasonal temperature cycles typical of those found in the UK. Acoustic emissions (AE) and galvanic currents were continuously monitored and correlated with ambient temperature. AE and galvanic currents were found to emulate the evolution of temperature in the diurnal cycles, although no specific relationship between AE and galvanic current could be obtained. The influence of seasonal variations in galvanic current had no obvious influence on AE Energy per second over the range of corrosion rates studied. The findings suggest that AE is more sensitive to short term (diurnal) changes in corrosion rates than the longer (seasonal) effects. It was hypothesised that this is due to transitory changes in the internal microclimate of the concrete. 相似文献
64.
The study of numerical abilities, and how they are acquired, is being used to explore the continuity between ontogenesis and environmental learning. One technique that proves useful in this exploration is the artificial simulation of numerical abilities with neural networks, using different learning paradigms to explore development. A neural network simulation of subitization, sometimes referred to as visual enumeration, and of counting, a recurrent operation, has been developed using the so-called multi-net architecture. Our numerical ability simulations use two or more neural networks combining supervised and unsupervised learning techniques to model subitization and counting. Subitization has been simulated using networks employing unsupervised self-organizing learning, the results of which agree with infant subitization experiments and are comparable with supervised neural network simulations of subitization reported in the literature. Counting has been simulated using a multi-net system of supervised static and recurrent backpropagation networks that learn their individual tasks within an unsupervised, competitive framework. The developmental profile of the counting simulation shows similarities to that of children learning to count and demonstrates how neural networks can learn how to be combined together in a process modelling development. 相似文献
65.
This paper reports the development of a novel ultrasonic inspection technique that detects radial fatigue cracks on the far side of thin airframe stiffener ‘weep’ holes. These cracks are located on the upper part of the weep hole (12 o'clock position), away from the lower skin of the wing. Cracks in this position are not readily detectable by conventional ultrasonic inspection techniques, particularly for short cracks. A special technique using circumferential creeping waves was adapted to inspect for these cracks. The conventional creeping wave technique experiences a strong specular reflection from the near surface of the hole that masks the creeping wave signal that arrives later in time. In order to overcome this difficulty, a split-aperture (two-element) transducer was used that resulted in the specular and creeping wave echoes being approximately equal in magnitude. The two separate transducers allowed us to alternate between pulse-echo and pitch-catch modes of operation with a resulting improvement in detection sensitivity. In the case of 0.25-inch-diameter weep holes, optimum sensitivity was calculated to be around 5 MHz. The detection threshold was found to be approximately 0.003 inches and the signal saturated at crack lengths in excess of 0.020 inches. The original paint and surface finish had no substantial adverse effects on the technique's sensitivity. Similarly, changing the weep hole diameter or chamfer conditions did not significantly affect the technique's performance. These results were obtained using specimens with both machined notches and real fatigue cracks. 相似文献
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69.
The development of flexible organic light emitting diode displays and flexible thin film photovoltaic devices is dependent on the use of flexible, low-cost, optically transparent and durable barriers to moisture and/or oxygen. It is estimated that this will require high moisture barriers with water vapor transmission rates (WVTR) between 10(-4) and 10(-6) g/m(2)/day. Thus there is a need to develop a relatively fast, low-cost, and quantitative method to evaluate such low permeation rates. Here, we demonstrate a method where the resistance changes of patterned Ca films, upon reaction with moisture, enable one to calculate a WVTR between 10 and 10(-6) g/m(2)/day or better. Samples are configured with variable aperture size such that the sensitivity and/or measurement time of the experiment can be controlled. The samples are connected to a data acquisition system by means of individual signal cables permitting samples to be tested under a variety of conditions in multiple environmental chambers. An edge card connector is used to connect samples to the measurement wires enabling easy switching of samples in and out of test. This measurement method can be conducted with as little as 1 h of labor time per sample. Furthermore, multiple samples can be measured in parallel, making this an inexpensive and high volume method for measuring high moisture barriers. 相似文献
70.
Matthew Poepael 《互联网周刊》2010,(14):70-71
随着互联网的飞速发展,电子商务应用早已成为人们生活不可或缺的一部分,越来越多的人选择进行网上购物,很多传统行业也在逐步开通网上营销渠道。根据研究显示,走在行业领先地位的美国电子商务公司实际上大多是多渠道运营,互联网渠道作为其中之一,也许目前销售额所占比例不算太大,但是增长速度确是惊人的。 相似文献