Microstructure of Titanium after Hydrogenation

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Bi-Pb-Tl三元系相图

用室温、高温X射线衍射及淬火的方法,测定了Bi-Pb-Tl三元系25℃的等温截面及该体系中的相结构。     

CHARACTERISTICS OF INTERNAL FRICTION AND MODULUS ASSOCIATED WITH NON-EQUILIBRIUM DIFFUSION-TYPE PHASE TRANSFORMATION IN EUTECTOID Al-Zn ALLOY

The characteristics of the low frequency internal friction and the modulus effect associatedwith the non-equilibrium spinodal pretransformation and the following discontinuous trans-formation was investigated in an as-quenched eutectiod Al-Zn alloy.It was observed that theloss of the stability in the lattice,which corresponded to the large-amplitude long-wavelengthstatic concentration wave in the non-equilibrium spinodal pretransformation,did not induceany effect of localized soft modulus.Although there are two aging internal friction peaks inphase transformation which correspond to the appearance and disappearance of the coherencyin spinodal pretransformation and the maximum of the interface area in the discontinuoustransformation respectively,the effect of localized soft modulus did not take place yet.     

CERTAIN CRITERION FOR THE FORMATION OF AMORPHOUS SOLIDS

<正> 根据成核理论,当仅考虑均匀核化时,在过冷熔体中结晶成核率可用下式表示: I=N_v~°kT/(3πα_°~3η)exp(-16πα~3β/3T_rΔT_r~2) (1)其中α=(N_v~°)~(1/3)σ/ΔH_m,β=1ΔH_m/RT_m=T/T_m, ΔT_r=T_m-T/T_m.各参量分别表示:I,成核率(cm~(-3)·s~(-1);N_v~°单位体积中的分子数(cm~(-3);η,粘滞系数(P);σ,比表面能(cal·cm~(-2));ΔH_m,熔化时的焓变(cal·mol~(-1));N,阿佛加德罗常数;v,克分子体积;T,熔体温度(K);T_m,熔点(K);k,玻尔兹曼常数;R,气体常数;α_0,分子直径。     

MAGNETIC PROPERTY AND THERMOSTABILITY OF Fe-BASE AMORPHOUS ALLOYS WITH HIGH SATURATION MAGNETIZATION

非晶态Fe_80B_(20),Fe_(17.84)B_(16.81)Si_(3.49)C_(1.36),Fe_(65.66)Co_(17.3)B_(15.84)Si_(1.2)和Fe_(6(?).92)Co_(17)B_(19.29)Si_(1.59)C_((?).(?))P_((?).(?))合金用单辊急冷法制备.测量了饱和磁化强度与温度的关系.得到0K时的原子磁矩(?)都在2.03—2.07μ_B之间.非晶态Fe_(80)B_(20)和Fe_(77.84)B_(16.81)Si_(3.49)C_((?).(?))合金的室温饱和磁化强度σ_s(R.T.)和Curie温度Tc相近,而含Co样品的σ_s(R.T.)和T_c分别高于Fe_(80)B_(20)约6%和13%.由热磁、电阻率、差热分析和X射线衍射的测量结果分析了样品的晶化转变.含Co样品的晶化温度T_(cr)与Fe_(80)B_(20)相近,而Fe_(77.84)B_(16.81)Si_(3.49)C_(1.86)的T_(cr)高于Fe_(80)B_(20)约80K.用化学键、T_(cr)与e/α的关系以及晶化过程的复杂性讨论了影响高饱和非晶态合金稳定性的因素.     

Nd_2(Fe_(0.9)Si_(0.1))_(14)B的中子衍射研究SCIEI

本文用中子衍射对Nd_2(Fe_(0.9)Si_(0.1))_(14)B在室温及77K进行了测量,用衍射峰的形状分析法进行了数据拟合。结果表明,在室温,Si择优占据4c,8j_1及16k_2晶位;Nd与Fe的磁矩平行于C轴排列。在77K,Si仍择优占据上述三个晶位。算得的Nd磁矩的方向偏离C轴37.8°。     

La在KCl-NaCl和LaCl_3-KCl-NaCl熔体中的溶解行为SCIEI

本文利用透明槽技术、电化学循环V-A法及量子化学EHMO三种方法,研究了La在KCl-NaCl(1:1mol)及LaCl_3-KCl-NaCl熔体中的溶解行为。初步认为:溶解在KCl-NaCl熔体中的La是以中性金属状态存在。在LaCl_3-KCl-NaCl熔体中,溶解的La与La^(3+)作用生成低价La^(2+)离子,La^(2+)又与周围的La^(3+)作用形成原子簇离子La_m^(n+)赋存于熔体之中。     

固溶处理对电解制备的A356合金硅颗粒的影响

以电解低钛铝基合金为原料制备了A356合金,研究了在535℃下固溶处理时间对合金共晶硅相细化、球化和分布的影响.测量了硅颗粒的长径和短径,计算了颗粒的直径和长短径比值等参数,分析了上述参数随固溶时间的变化及其概率密度分布.实验结果表明:由该电解合金制备的A356合金经2～4 h的固溶处理,共晶硅就可得到较好的细化和球化效果,具有较高的分布集中度;A356合金的固溶处理时间可有效缩短.     

Analysis of junction temperatures in high-power GaN-based LEDs

We presented the analysis of the incomplete conduction in bonding medium in high power GaN-based light-emitting diode (LED) packages. A numerical study was carried out with parametric model to understand the junction temperature variation due to bonding medium defects. Transient thermal measurement was performed to evaluate LED’s junction temperature. Thermal resistance from chip to lead frame was 20 K/W in our sample LED. It was suggested that only 60% of the surface area of the bonding medium was involved...     

碱处理对MCM-22分子筛催化汽油烷基化脱硫的影响

通过氢氧化钠碱处理对MCM-22分子筛进行了改性,并考察了经碱处理后的MCM-22分子筛在汽油烷基化反应中的催化性能。结果表明,经碱处理后的分子筛在微介孔并存的情况下出现了介孔变大且原有的微孔结构保持几乎不变的情形,同时分子筛的酸性中心也得到增强,致催化剂的活性、稳定性都有所增加。