SUPERHEATED STEAM DRYING OF SINTERED SPHERES OF GLASS BEADS UNDER VACUUM

Drying of sintered spheres of coarse glass beads with a wide sintering range in superheated steam under vacuum was studied.

In samples with sintered angles of 7.5° –27°, the experimental normalized drying rates in superheated steam at pressures of 7.3-7.9mmHg were smaller than those for 56.0-767.6 mmHg in the vicinity of the critical moisture cotents for 56.0-767.6GmmHg. As reported in an earlier paper, there were     

Chemical constituents of the leaves of rabbiteye blueberry (Vaccinium ashei) and characterisation of polymeric proanthocyanidins containing phenylpropanoid units and A-type linkages

Chemical constituents of the leaves of rabbiteye blueberry (Vaccinium ashei READE) were investigated in detail. The major phenolic components were caffeoyl quinic acids, flavonol glycosides, flavan-3-ols and proanthocyanidins. Catechins and proanthocyanidins having additional phenylpropanoid units, such as cinchonains, kandelins and mururins, characterised the polyphenols of this plant. Among them, vaccinin A, an isomer of mururin A, was found to be a new compound, and the structure was characterised by spectroscopic methods. The most abundant polyphenols (11.3% of freeze-dried leaves) were oligomeric proanthocyanidins. Thiol degradation with mercaptoethanol indicated that the polymer was constituted of (+)-catechin and (−)-epicatechin as the terminal units and (−)-epicatechin, procyanidin A-2, and cinchonains Ia and Ib as the extension units. Mass spectral analysis suggested the presence of at least dodecamers with A-type linkages and phenylpropanoid moieties.     

亚微米颗粒对铝基复合材料基体显微结构的影响

选用0．15μm和5μm的Al2O3颗粒，采用挤压铸造法制备了体积分数为40％的铝基复合材料。利用选区电子衍射和高分辨电子显微技术研究了Al2O3P／1070Al界面附近基体的显微组织。结果表明，复合材料增强体颗粒为5μm时，基体存在大量的Eh热错配应力引发的位错，颗粒粒径为0．15μm时，基体表现为近无位错的组织特征，其缺陷形式为1～5nm的“微畸变区”，这主要是由于粒径小、分布弥散，微区应力均匀所致。     

Flow characteristics of gas–liquid two phase plunging jet absorber–gas holdup and bubble penetration depth

A gas-liquid two phase plunging jet is formed through a gas sucking type multi-jet ejector nozzle. In this study, the effects of various conditions in the multi-jet ejector nozzle, the column diameter, and the liquid jet length on penetration depth of air bubblesl _B and gas holdup h_G in a gas-liquid two phase plunging jet absorber were studied experimentally. Consequently, empirical equations concerningl _B and h_G were obtained, respectively. These equations agree with the experimental data with an accuracy of ±20% forl _B and ±25% for h_G.     

Patterned hydrophobic-hydrophilic templates made from microwave-plasma enhanced chemical vapor deposited thin films

In the present research, nano-structured materials exhibiting super-hydrophobic behavior obtained by microwave-plasma enhanced chemical vapor deposition (MPECVD) had their surface chemical status altered through vacuum ultraviolet (VUV) light irradiation. Falling water droplets rolled and bounced without wetting or spreading over the initially super-hydrophobic surfaces. We demonstrate a surface preparation technique to create a patterned super-hydrophobic/super-hydrophilic substrate in which micropatterns with super-hydrophobic and super-hydrophilic regions were prepared through irradiation with VUV light. To confirm the method, growth of water droplets is observed in situ on such super-hydrophobic/super-hydrophilic micropatterns. We discuss the applicability of the super-hydrophobic/super-hydrophilic pattern to the bottom-up assembling of materials, like site-selective electroless Cu plating on patterned substrates made of paper and selective cell culture experiments.     

Hepatic arterial infusion chemotherapy (HAI) for advanced hepatocellular carcinoma inefficacious with transcatheter arterial embolization (TAE)

For 6 patients with advanced hepatocellular carcinoma (HCC) in whom TAE was inefficacious, we tried hepatic arterial infusion chemotherapy. 5-FU 500 mg/day + CDDP 10 mg/day was administered during 5 days. The AFP level was decreased for 4 patients, and 2 patients showed a partial response in CT image. These 2 patients have been alive over 22 and 18 months, respectively. These results suggest that 5-FU + CDDP HAI might be a useful treatment of HCC inefficacious with TAE.