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941.
In the gold wire bonding of aluminum in microelectronic devices the presence of aluminum oxide on the metallization surface may be expected. Electron transparent couples containing an oxide layer at the interface were heated in a TEM to determine the effects of a passivation layer on intermetallic formation. Intermetallic phases were evidenced by changes in sample appearance and their structure was determined by electron diffraction. The presence of an oxide at the interface hindered second phase formation at temperatures at which they were usually expected to form. In aluminum rich couples, the formation of the AuAl2 intermetallic was not observed to form until about 350°C with the oxide present. In a reverse configuration involving a gold rich couple, an amorphous oxide phase was observed between the Al and the advancing Au2Al front. The movement of the reaction front appeared to be controlled by surface diffusion across this phase. 相似文献
942.
The results of investigation of mechanochemical reactions in the mixtures of hydroxides and carbonates of alkaline and alkaline earth metals with zirconium oxychloride and oxynitrate are presented. It is shown that one of the features of interaction between the components is the formation of the salts of alkaline and alkaline earth metals along with X-ray amorphous zirconium-containing compound. It is demonstrated that the mechanical activation of the mixture of yttrium carbonate and zirconium oxynitrate, followed by thermal treatment of this mechanically activated mixture, results in the formation of solid solution ZrO2-Y2O3 in cubic modification. 相似文献
943.
944.
945.
E. Cerri 《Journal of Materials Science》2004,39(9):3115-3119
Thixocast samples of an Al-Si-Cu alloy were solution treated at 500°C for 4 h, aged at 170°C for different times and tensile tested at room temperature. Statistical analysis on the fractured Si particles has pointed out how the fraction of damaged particles is influenced by the ageing treatments performed before deformation. The damage accumulation per unit of strain decreases with increasing ductility of the samples. The Considére criterion for plastic instability shows no significative necking. 相似文献
946.
947.
M. Loidl E. Leblanc T. Branger H. Rotzinger T. Daniyarov M. Linck A. Fleischmann C. Enss 《Nuclear instruments & methods in physics research. Section A, Accelerators, spectrometers, detectors and associated equipment》2004,520(1-3):73-75
We report on a feasibility study on precise determination of mass-specific activity of low-energy emitting radioisotopes. Conventional methods of activity measurement suffer from source self-absorption and a strong decrease in detection efficiency for low-energy electrons and photons. We propose a new method based on metallic magnetic microcalorimeters with the source embedded in the detector target in a 4π geometry. First results with a 55Fe source show that electrons and photons are detected with a detection efficiency close to unity and with little loss of energy for electrons. The aim of this study is to provide standards of activity with very low uncertainties in the framework of radiation metrology. 相似文献
948.
S. Zh. Davrenbekov E. S. Mustafin B. K. Kasenov S. T. Edil'baeva Sh. B. Kasenova E. K. Zhumadilov Zh. I. Sagintaeva 《Inorganic Materials》2004,40(9):976-978
NdMCr2O5 (M = Na, K, Cs) and NdMgCr2O5.5 are prepared by solid-state reactions between appropriate oxides and carbonates and are shown to have a tetragonal structure. The heat capacity of these chromites, measured from 298.15 to 673 K, exhibits sharp changes attributable to second-order phase transitions. The C
p
0(T) data are represented by quadratic best fit equations. The electrical resistivity of the chromites is measured between 303 and 493 K. The results attest to semiconducting behavior of the materials in certain temperature ranges. 相似文献
949.
A. D. Bulanov A. N. Moiseev O. Yu. Troshin V. V. Balabanov D. V. Isaev 《Inorganic Materials》2004,40(6):555-557
High-purity isotopically enriched (99.98% 28Si, 99.57% 29Si, and 99.83% 30Si) silane samples are prepared for the first time. The total hydrocarbon content of the samples is no higher than 0.1–0.3 ppm. The concentration of electroactive impurities in the silicon prepared from the purified monoisotopic silane is below 1015 cm–3. 相似文献
950.
I. A. Grishin V. A. Gur'ev E. B. Intyushin Yu. E. Elliev A. P. Savikin 《Inorganic Materials》2004,40(4):431-433
TeO2–WO3 glasses coactivated with Er3+ and Yb3+ are prepared. The effect of Yb content on the efficiency of Er photoluminescence (PL) in the visible and IR spectral regions is studied. The highest PL efficiency is achieved at an Er : Yb atomic ratio of 1 : 1. The PL lifetime for the Er3+
4
I
13/2 level is determined to be 7–9 ms. 相似文献