镁钴铝类水滑石催化合成安息香甲醚

采用共沉淀法制备了镁钴铝类水滑石化合物(MgCoAl-HTLcs),并用 X 射线衍射、扫描电子显微镜、NH_3程序升温脱附等方法对 MgCoAl-HTLcs 进行了表征,并以 MgCoAl-HTLcs 为催化剂催化苯甲醛与甲醇反应合成安息香甲醚,研究了n(Mg):n(Co):n(Al)、催化剂用量、原料配比、反应温度、反应时间对合成反应的影响。表征结果显示,MgCoAl-HTLcs 的晶相完整,表面主要为弱酸、弱碱性。催化合成安息香甲醚的适宜条件为:MgCoAl-HTLcs 催化剂用量0.10 g(约为原料总质量的0.23%),n(Mg):n(Co):n(Al)=0.4:1.6:1.0,V(苯甲醛):V(甲醇)=3:50,反应温度50℃,反应时间150 min。在此条件下,苯甲醛的平衡转化率达77.49%,安息香甲醚选择性接近100%。为洁净合成安息香甲醚开辟了一条新的途径。     

在未来勘探开发中研发的推动作用

在过去的20年里,尽管油价和经营环境不断发生着变化,但勘探开发的产量和经济效益持续增长着,科学研究和先进技术起了关键作用。未来的勘探开发将更加依赖于先进的技术和科学的研究开发。 随着变化的经营环境和关键的先进科学技术强有力的结合,出现了新的研发模式和发展趋势。在这里我们     

抗窄带干扰宽带中频数字接收机的设计与实现

讨论了存在强干扰条件下MSK中频数字接收机的频域窄带干扰抑制、伪码快速捕获、MSK相干解调等实现方法。具体实现中提出了基于功率估计的码捕获门限实时调整方案，解决了动态干扰条件下的快速码捕获问题。基于FPGA DSP硬件设计和软件可编程数字信号处理算法，接收机具有较强的适应性和稳定性。     

Mapping rule-based systems onto multicomputers using simulated annealing

In this paper, we present a static load balancing method for mapping production rules in an expert system onto processors of a message-passing multicomputer. The method uses simulated annealing to achieve a nearly optimal allocation of production rules onto processor nodes. The approach balances the initial rule distribution to avoid higher communication demand among processor nodes at run time. A formal mapping model is developed and a new cost function is defined for the annealing process. New heuristic swap functions and cooling policies are provided to ensure the quality of the annealing process. A software load balancing package, SIMAL, was implemented on a SUN workstation to carry out the benchmark experiments. The overhead associated with this mapping method is O(m In m), where m is the number of rules in the production system. Two benchmark production systems, Toru-waltz and Tourney, are mapped onto a hypercube computer with 32 nodes. Experimental benchmark results verify the effectiveness of the rule mapping method. The method can be applied for distributed artificial intelligence processing or for the parallel execution of cooperating expert systems on a message-passing multicomputer.     

Acrylonitrile-based copolymers: Synthesis,characterization, and formation of ultrafiltration membranes utilized for the immobilization of proteins

Various high molecular weight copolymers of acrylonitrile and a vinyl comonomer containing an aryl amine, a pyridine, or an aliphatic hydroxyl group were synthesized via slurry polymerization techniques so as to contain from 1 to 15 mol % functional comonomer. The comonomer content was quantitated by ultraviolet absorbance, base titration of acid polymer salts, and/or relative chemical reactivity with trichloro-s-triazine. Thin films were cast from copolymer solutions, coagulated into unsupported ultrafiltration membrances, and characterized with respect to both water permeability and pore size distribution. Analysis by size exclusion chromatography of the membrane permeate of a pool of dextran fractions yielded a continuous distribution curve for membrane pore size over the range 1.5 to 70 nm. The ultrafiltration membranes were used for protein immobilization after appropriate chemical activation. The three distinct types of functional copolymers gave comparable results for α-chymotrypsin, with protein weight loadings of 6–12% and 40–65% retention of enzymatic specific activity.     

新型机载高速数据通信系统设计

为了满足航空电子通信技术发展的需求,提出了基于FDDI标准的机载高速光纤通信网络体系结构,论述了该通信系统的总体设计思想和硬软件实现方案,最后简述机载高速数据通信系统的应用情况.     

Individual and structural origins of friendship and social position among professionals.

Friendship affects individual and organizational well-being through direct relations, social positions, and complex network structures. In this study, the authors use longitudinal data from 2 groups of master's of business administration students to increase understanding of how friendship networks develop. The authors propose and test a dynamic model in which attribute similarity facilitates dyadic friendship ties, as well as similar network centrality and social position; early friendship increases later similarity in structural position and centrality; and early structural similarity enhances the likelihood of future friendship. Findings largely supported the model, demonstrating how homophily and early social contacts can jointly shape maturing friendship networks. (PsycINFO Database Record (c) 2010 APA, all rights reserved)     

Improving Cost Estimates of Construction Projects Using Phased Cost Factors

Central to cost-based competition is the capability to accurately predict the cost of delivering a project. Most literature on cost estimation focuses on specific estimation methods as generic techniques and little attention has been paid to the unique requirements at each project stage. This note attempts to identify the critical factors for effective estimation at various stages of typical construction projects. Drawing from organization control theory and cost estimating literature, this note develops a theoretical framework that identifies the critical factors for effective cost estimation during each project phase of a conventional construction project. The underlying logic is that as a cost estimating effort progresses, both task programmability and output measurability improve. As a result, control effort will shift from input-oriented control to a combination of output and behavior control.