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951.
Zhe-Feng Zhang Zheng Ming Sun Hitoshi Hashimoto Toshihiko Abe 《Journal of the American Ceramic Society》2003,86(3):431-436
Ti/Si/2TiC powders were prepared using a mixture method (M) and a mechanical alloying (MA) method to fabricate Ti3 SiC2 at 1200°–1400°C using a pulse discharge sintering (PDS) technique. The results showed that the Ti3 SiC2 samples with <5 wt% TiC could be rapidly synthesized from the M powders; however, the TiC content was always >18 wt% in the MA samples. Further sintering of the M powder showed that the purity of Ti3 SiC2 could be improved to >97 wt% at 1250°–1300°C, which is ∼200°–300°C lower than that of sintered Ti/Si/C and Ti/SiC/C powders using the hot isostatic pressing (HIPing) technique. The microstructure of Ti3 SiC2 also could be controlled using three types of powders, i.e., fine, coarse, or duplex-grained, within the sintering temperature range. In comparison with Ti/Si/C and Ti/SiC/C mixture powders, it has been suggested that high-purity Ti3 SiC2 could be rapidly synthesized by sintering the Ti/Si/TiC powder mixture at relatively lower temperature using the PDS technique. 相似文献
952.
Summary A melt-grafting approach was employed to prepare a novel functional polypropylene(FPP)—amino-terminated polyurethane grafted
polypropylene (PP-g-ATPU). The crystallization behaviors of PP and PP/FPP blends were characterized using differential scanning
calorimetry (DSC), wide angle X-ray scattering (WAXS) and polarized optical microscopy (POM). The effects of FPP composition
on crystallization behavior, crystal transformation, and morphology of PP/FPP crystalline were investigated. The results showed
that at a low dosage (<2.0 wt%) ATPU acted as a heterogeneous nucleation agent during the crystallization of PP/FPP blends.
However, when the content of ATPU reached 2.0 wt% or higher, ATPU deteriorated the crystallization of PP or PP/FPP blends.
The crystallite size decreased and the number of crystallites increased as the ATPU content increased. The Avrami analysis
was adopted to describe the isothermal crystallization process. The difference in the exponent n between PP and PP/FPP suggested that the isothermal crystallization kinetics of PP/FPP blends followed a three-dimensional
growth via heterogeneous nucleation. In terms of the half-time of the crystallization, t1/2, the crystallization rate of functional PP blends was faster than that of PP homopolymer at a given crystallization temperature. 相似文献
953.
纳米级无机粒子对聚乙烯的增强与增韧 总被引:50,自引:2,他引:50
对μm级CaCO3、TiO2和nm级SiC/Si3N4粒子填充LDPE的性能进行了研究。实验证明,μm级粒子对LDPE虽无明显的增强增韧作用,但也未使基体的机械性能大幅度下降。nm级SiC/Si3N4对LDPE有较大的增强增韧作用,在5%质量分数时冲击强度出现最大值,缺口冲击强度达55.7kJ/m2为纯LDPE的203%;伸长率到625%时仍未断裂,为纯LDPE的500%,但熔体流动速率急剧下降,仅为纯LDPE的26%,当含量在3%和15%质量分数时,熔体流动速率分别为纯LDPE的337%和151%。 相似文献
954.
955.
STM32和OV2640的嵌入式图像采集系统设计 总被引:1,自引:0,他引:1
基于STM32嵌入式系统及200万摄像头OV2640设计了图像采集系统,分析了系统的基本硬件架构,分别对不同模块的功能特点作出了简单的介绍;对系统的软件设计给出了详细的说明,介绍了系统初始化的基本思路和流程,以及相关外围设备模块在程序中的使用;并给出了系统的整体设计思路,实现了系统的稳定运行。 相似文献
956.
On the use of graphical method to determine the targets of single-contaminant regeneration recycling water systems 总被引:2,自引:0,他引:2
Water system integration with regeneration recycling can reduce freshwater consumption and wastewater discharge to the maximum extent. In this paper, by analyzing the limiting composite curve of a single-contaminant water system, a method is proposed to construct the optimal water supply line for regeneration recycling. Accordingly the targets for regeneration recycling water systems are obtained. The targets in sequence are the minimum freshwater consumption (the minimum wastewater discharge), the minimum regenerated water flowrate, and the optimal regeneration concentration. The post-regeneration concentration is taken to be fixed in the sequential targeting procedure. The interactions of these targets are analyzed, and formulas for calculating these targets are proposed. The results show that for a single-contaminant regeneration recycling water system, the minimum freshwater consumption is determined by the shape of the limiting composite curve below the post-regeneration concentration. The optimal regeneration concentration is defined as the minimum regeneration concentration at the minimum freshwater consumption and the corresponding minimum regenerated water flowrate. The minimum regenerated water flowrate and the optimal regeneration concentration are both related to the geometrical features of the limiting composite curve of the water-using system and to the post-regeneration concentration. The optimal regeneration concentration has no direct relationship with the pinch concentration. 相似文献
957.
CC1101在工业及实验室均有着广泛的应用,本文完成了基于ARM9硬件平台和嵌入式Linux系统的CC1101驱动开发,并以此为基础提出一种简单面向连接的通信模型。经验证,这种通信模型能够保证CC1101的通信质量。 相似文献
958.
高吸水性树脂与PVC共混的研究 总被引:5,自引:0,他引:5
用高吸水性树脂与PVC共混制备了吸水膨胀性PVC共混物。实验证明,部分水解丙烯酸甲酯—醋酸乙烯酯HP(MA—VAC)和丙烯酸甲酯—醋酸乙烯酯—甲基丙烯酸甲酯HP(MA—VAC—MMA)共聚物与PVC共混效果更好。研究了影响共混物吸水率和力学性质的各种因素。结果表明,随高吸水性树脂用量增加,共混物吸水率显著增加。当吸水树脂用量大于40%时,共混物的拉伸强度和断裂仲长率下降。共混物最大吸水率达22.17克水/克共混物,最大膨胀度为15倍。 相似文献
959.
960.