熔融缩聚法制备聚乳酸

通过熔融缩聚法制备了聚乳酸。探讨了反应温度、催化剂类型及用量、反应时间对聚乳酸的影响，并用红外光谱和1↑H NMR对聚合物进行了表征。结果表明，最佳的反应条件为：聚合时间30h左右、聚合温度160℃、以O．2％的对甲苯磺酸作为酸催化剂、O．5％的氯化亚锡为催化剂、真空度为O—1333Pa；而提高乳酸纯度是制备高摩尔质量聚乳酸的关键条件之一。     

Preparation,characterization, and adsorption properties for metal ions of a novel chelating resin containing sulfoxide and diethylene glycol

A novel chelating resin containing sulfoxide and diethylene glycol, poly{4‐vinylbenzyl‐[2‐2‐(hydroxyethyl)ethoxyl]sulfoxide} (PVESO) was synthesized using chloromethylated polystyrene (PS‐Cl) as material. Its structure was characterized by elemental analysis, infrared spectra, and scanning electron microscopy (SEM). The adsorption capacities of the resin for Hg²⁺, Ag⁺, Cu²⁺, Zn²⁺, and Pb²⁺ at various pH values were determined. The maximum adsorption capacities for Hg²⁺ and Ag⁺ were 1.56 and 0.75 mmol g^?1 respectively. The resin had high selectivity for Hg²⁺ and Ag⁺ over the pH range 1.0–7.0. The adsorption capacities for Hg²⁺ and Ag⁺ under competitive condition were also determined by batch experiment method. In addition, the adsorption kinetics of the resin towards Hg²⁺ at different temperatures was also investigated. The results showed that the adsorption rate was governed by film diffusion at 20°C and 25°C, by particle diffusion at 30°C and 35°C. © 2006 Wiley Periodicals, Inc. J Appl Polym Sci 102: 6054–6059, 2006     

浅析呼和浩特市大气SO2发展趋势及防治对策

本文通过对二氧化硫的形成及危害的阐述，以及对我市近几年大气中二氧化硫监测结果的分析，针对发展趋势和存在的问题，根据实际情况提出相应的建议。     

Soap‐free emulsion copolymerization of perfluoroalkyl acrylates in the presence of a reactive surfactant

Soap‐free emulsion copolymerization of perfluoroalkyl acrylate (FA)/methyl methacrylate (MMA)/n‐butyl acrylate (n‐BA) was carried out in the presence of sodium 2‐acrylamide‐2‐methyl propanesulfonate (AMPSNa) as a reactive surfactant and potassium persulfate (KPS) as an initiator. An analysis of the effects of concentration of AMPSNa, KPS, FA as well as polymerization temperature on the kinetic features (rate of polymerization) and colloidal characteristics (mean particle diameter, particle disperse index, particle numbers, and surface charge density) was followed. NMR, FTIR, AFM, and fluorine‐selective electrode analysis were used to characterize the composition and morphology of the FA copolymers. Both AFM analysis and contact angle measurements strongly implied that the fluorinated segments migrated to the outmost surface and created films with lower surface energy. © 2007 Wiley Periodicals, Inc. J Appl Polym Sci 104: 2438–2444, 2007     

快速高效隔膜压滤机在鹤壁四矿选煤厂的应用

介绍了快速高效隔膜压滤机的主要性能参数和特点 ;分析了压滤机在煤泥水处理系统中的应用情况和运行结果 ;应用快速高效隔膜压滤机对煤泥水处理系统进行改造后获得了较好的经济及社会效益     

新型聚丙烯接枝物的制备及应用

为制备强韧的共混材料,利用熔融接枝法研制了含有两种接技单体的新型聚丙烯接枝物,讨论了第二单体在接枝过程中的作用,并将其应用于尼龙6/聚丙烯(PA6/PP)共混体系,获得了使分散相粒径更细小、界面更模糊的增容效果。     

庙宇平坝防洪治理方案研究

庙宇平坝地处大溪河右岸支流庙宇沟上游山间盆地内,仅靠一条人工开凿的排洪洞和天然消坑排泄洪水,过流能力不足致使每年都遭受洪涝灾害。根据庙宇平坝地形条件及防洪现状,复核现有排洪设施泄流能力,分析存在的问题,结合庙宇平坝地形条件及区内实际情况,采取整个消水洞的扩建及进口前100 m的河道支护,从而提高泄洪能力,降低庙宇平坝水位,有效减少洪水淹没历时及淹没深度。     

广西田阳县生态扶贫产业核心示范区一期工程补水泵站设计

结合广西田阳县生态扶贫产业核心示范区一期工程补水泵站实际情况,通过方案比选,采用河流入江口东岸布置方案,并对泵站进行了设计介绍,总结技术特点,为类似工程提供参考。     

基于SOAP的企业异构信息系统集成

阐述了SOAP通信协议的构成和实现机制以及与相似协议的比较。基于它的跨平台的能力,将其运用于企业的分布式环境中,实现了异构信息系统间的互操作和跨部门的数据处理,提高企业数据处理的效能,同时为企业异构信息系统集成提供了新的方法。     

A noisy-smoothing relevance feedback method for content-based medical image retrieval

In this paper, we address a new problem of noisy images which present in the procedure of relevance feedback for medical image retrieval. We concentrate on the noisy images, caused by the users mislabeling some irrelevant images as relevant ones, and a noisy-smoothing relevance feedback (NS-RF) method is proposed. In NS-RF, a two-step strategy is proposed to handle the noisy images. In step 1, a noisy elimination algorithm is adopted to identify and eliminate the noisy images. In step 2, to further alleviate the influence of noisy images, a fuzzy membership function is employed to estimate the relevance probabilities of retained relevant images. After noisy handling, the fuzzy support vector machine, which can take into account different relevant images with different relevance probabilities, is adopted to re-rank the images. The experimental results on the IRMA medical image collection demonstrate that the proposed method can deal with the noisy images effectively.