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排序方式: 共有253条查询结果,搜索用时 15 毫秒
41.
Ramazan Citak Kirk A. Rogers Ken H. Sandhage 《Journal of the American Ceramic Society》1999,82(1):237-240
BaAl2 O4 /aluminum-bearing composites have been synthesized via the low-temperature oxidation of Ba-Al precursors. Ba-Al powder mixtures that were prepared via high-energy vibratory milling were uniaxially pressed into bar-shaped specimens that were then exposed to a series of heat treatments in pure, flowing oxygen at temperatures up to 640°C. Oxidation at a temperature of 300°C resulted in the formation of barium peroxide (BaO2 ). Additional heat treatment at a temperature of 550°C resulted in the consumption of BaO2 and some aluminum to yield BaAl2 O4 and Al4 Ba. The oxidation of Al4 Ba at a temperature of 640°C yielded additional BaAl2 O4 . Microstructural analyses revealed that a well-dispersed, co-continuous mixture of Al2 O3 -excess BaAl2 O4 and 99.5% pure aluminum was produced. 相似文献
42.
The adsorption behavior of methacrylic acid‐grafted poly(ethylene terephthalate) fibers was studied toward the copper(II) ion in aqueous solutions by a batch equilibriation technique. The influence of treatment time, temperature, pH of the solution, metal ion concentration, and graft yield were considered. One hour of adsorption time was found sufficient to reach adsorption equilibrium for the copper(II) ion. It was found that the adsorption isotherm of Cu(II) fits Langmuir‐type isotherms. The adsorption process is not affected by the temperature when treated with low ion concentration, but is remarkably decreased at a high ion concentration. The heat of adsorption value was calculated as 0.71 kcal/mol. It was found that the reactive fibers are stable and regenerable by acid without losing their activity. © 2000 John Wiley & Sons, Inc. J Appl Polym Sci 75: 766–772, 2000 相似文献
43.
Khurram A. Khan Ramazan Kahraman Esam Z. Hamad Shaikh A. Ali Syed H. Hamid 《应用聚合物科学杂志》1997,64(4):645-652
A liquid crystalline polymer (LCP) was synthesized by an interfacial polycondensation reaction at room temperature from terephthaloyl chloride and p,p′-dihydroxydiphenyl sulfone. The LCP synthesized was so stable and molecularly rigid that it did not show any phase transition until it degraded at about 320°C. Composites of the LCP with polycarbonate (PC), polystyrene (PS), and sulfonated polystyrene (SPS) were formed by compression molding at a temperature at which the thermoplastic matrix was in the melt state. They were thermally analyzed by differential scanning calorimetry. Tensile specimens were cut from the compression-molded plates, and mechanical tests were performed. The morphology of the material systems was studied by performing scanning electron microscopy analysis on cryogenically fractured specimens. For LCP/PS and LCP/SPS systems, a sharp two-phase morphology was formed, which suggested poor interfacial adhesion. The tensile strength of both systems decreased with LCP addition. The LCP/PC system also revealed a two-phase morphology; however, the interfaces between the LCP domains and the PC matrix were not so well defined, showing better interfacial adhesion than the two previous systems studied. Stronger bonding between the LCP and PC resulted in a significant improvement in the mechanical behavior of PC by LCP addition. © 1997 John Wiley & Sons, Inc. J Appl Polym Sci 64: 645–652, 1997 相似文献
44.
Artificial neural network (ANN) based maximum power point tracking (MPPT) algorithm makes use of the advantages of ANNs such as noise rejection capability and not requiring any prior knowledge of the physical parameters relating to PV system. This paper proposes a genetic algorithm (GA) optimized ANN-based MPPT algorithm implemented in a stand-alone PV system with direct-coupled induction motor drive. The major objective of this design is to eliminate dc–dc converter and its accompanying losses. Implementing off-line ANN in DSP needs optimization of ANN structure to obtain an ideal size. GA optimization was used in this study to determine neuron numbers in multi-layer perceptron neural network. Another objective of this work is to prevent the necessity of the trade-off between the tracking speed and the oscillations around the maximum power point. Hence, varying step size is used in MPPT algorithm and PI-controller is adopted for simple implementation. Simulation and experimental results have been used to demonstrate effectiveness of the proposed method. 相似文献
45.
Gokhan Zengin Srinivasan Nithiyanantham Cengiz Sarikurkcu Sengul Uysal Ramazan Ceylan Karnam Satya Ramya 《International Journal of Food Properties》2017,20(10):2373-2382
In the present article, seven wheat cultivars (Ahmetaga, Bezostaya, Dagdas-94, Ekiz, Karahan-99, Konya-2002, and Tosunbey) grown in Turkey were compared for their phytochemical composition, antioxidant, and enzyme inhibitory activities. Antioxidant capacities and enzyme inhibitory effects were investigated with colorimetric methods. Total phenolic content ranged from 40.71 to 86.34 mg of gallic acid equivalent/100 g wheat grain. Tosunbey (92 mg Trolox equivalent/100 g wheat grain) and Ahmetaga (114.56 mg Trolox equivalent/100 g wheat grain) cultivars exhibited strong 2,2 azino-bis (3-ethylbenzothiazloine-6-sulfonic acid) and 1,1-diphenyl-2-picrylhydrazyl free radical scavenging activities. As compared to other wheat cultivars, Tosunbey cultivar had remarkable both antioxidant and enzyme inhibitory effects with the highest level of phenolics. Ferulic acid, chlorogenic acid, and apigenin were the major phenolics in extracts tested. This study suggested that an increased intake of wheat derived products could represent an effective strategy for the management of oxidative stress related chronic and degenerative diseases such as Alzheimers and diabetes mellitus. 相似文献
46.
Ramazan Gürkan 《Food additives & contaminants. Part A, Chemistry, analysis, control, exposure & risk assessment》2016,33(7):1127-1138
A simple and efficient ultrasonic-assisted extraction (UAE) procedure has been proposed for the pre-concentration of (2S)-2-[(4-{[(2-amino-4-hydroxypteridin-yl)methyl]amino}phenyl)formamido]pentanedioic acid (folic acid) in vegetables, pharmaceuticals and foods prior to determination at 540 nm using UV-Vis spectrophotometry. The method is based on hydrophobic ternary complex formation of folic acid with silver ions in the presence of cetyltrimethylammonium bromide (CTAB) as a sensitivity enhancer counter ion at pH 7.0, and then extraction into a micellar phase of polyethylene glycol monoalkyl ether (Genapol X-080). The impacts on the extraction efficiency and complex formation of analytical parameters such as sample pH, concentration of silver, concentration of surfactants and extraction time, ultrasonic time and sample volume, were investigated and optimised in detail. The matrix effect on the pre-concentration and determination of folic acid was investigated, and it was observed that the proposed method was highly selective against possible matrix co-extractives. Under optimised conditions, a good linear relationship between the analytical signal and folic acid concentration was obtained in the range of 0.6–180 μg l?1 with a detection limit of 0.19 μg l?1 and quantification limit of 0.63 μg l?1. The applicability was evaluated using samples fortified at different concentration levels, and recoveries higher than 94.1% were obtained. The precision as the percent relative standard deviation (RSD%) was in range of 2.5–3.8% (10 and 40 μg l?1, n = 5). The proposed method was validated by analysis of two standard reference materials (SRMs) and various real samples, and satisfactory results were obtained. 相似文献
47.
The effect of crystallinity and particle morphology of the submicron barium hexaferrite (BaFe12O19) powders on the magnetic properties was investigated on powders synthesized by solid-state calcination (BHF-c) and molten salt synthesis (BHF-m) methods. Solid-state calcination route was found to yield agglomerated powders with poor crystallinity, whereas molten salt synthesis resulted in well crystallized powders with an anisometric morphology. The saturation magnetization of the BHF-m and BHF-c samples is 59 emu/g, and 56 emu/g at 300 K, and 90 emu/g, and 86 emu/g at 10 K. The temperature dependence of magnetization of the BHF-m is higher and the increase in magnetocrystal anisotropy with decreasing temperature is also steeper than that of the BHF-c due to the higher crystallinity. The magnetocrystalline anisotropy constant, K, calculated from the Stoner–Wohlfarth theory, of the BHF-m and BHF-c powders is 14.24 and 10.14 HA2/kg, respectively. The higher effective anisotropy, Keff of the BHF-m is also confirmed through ferromagnetic resonance measurements. In conclusion, the higher crystallinity, slightly higher particle size and anisometric morphology of the BHF-m particles translated into higher magnetic properties and magnetocrystalline anisotropy. 相似文献
48.
Halil İbrahim Ulusoy Ramazan Gürkan Özlem Demir Songül Ulusoy 《Food Analytical Methods》2012,5(3):454-463
A new method has been developed for preconcentration of cobalt at trace levels in beverage samples using calcon carboxylic
acid as chelating agent and cetyl pyridinium chloride as an auxiliary ligand and entrapped into Triton X-114 prior to its
determination by flame atomic absorption spectrometry (FAAS). The main parameters affecting cloud point extraction (CPE) efficiency
such as pH, concentration of the complexing agent, cationic and nonionic surfactant concentration, salt effect, the equilibrium
time, and temperature were investigated and optimized. After optimization of the CPE conditions, a preconcentration factor
of 60, an enhancement factor of 106, and a detection limit of 0.20 μg L−1 by (R
2 = 0.9978) were obtained from a calibration curve constructed in the range of 0.7–100 μg L−1. The proposed preconcentration procedure was successfully applied to the determination of cobalt ions in some real samples
including natural drinking water, tap water, and beer and wine samples. The accuracy and validity of the proposed CPE/FAAS
method was tested by means of five repeated analysis of reference standard materials (TM-253, a low level fortified water
standard for trace elements). A good agreement between analytical results (28.8 and 28.5 μg L−1 with calibration curve and standard addition curve method, respectively) and certified value (27.9 μg L−1) for Co (p < 0.05) were obtained and verified by means of calibration curve and standard addition curve method using CPE procedure. 相似文献
49.
The histamine contents of Turkish style fermented sausages were determined on 46 samples of five different brands obtained from retail stores in Van in Turkey. Histamine was found in all samples in the range 19.64-87.47 mg/kg (mean 32.13 mg/kg). Histamine levels in the brands differed significantly (P<0.01). The results suggest that the histamine levels in the sausages were not hazardous in terms of public health although they may be a potential risk to sensitive individuals. 相似文献
50.
Food Analytical Methods - In the present study, an inexpensive, selective, and micellar sensitive spectrophotometric method for Sn(IV) was developed at 537 nm. The method is based on the... 相似文献