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101.
为验证一氧化碳(CO)和二氧化碳(CO2)加氢制乙醇的可行性,并为相关实验研究提供理论依据,采用HSC Chemistry软件对CO和CO2加氢制乙醇反应进行热力学分析,考察反应压力、反应温度和氢碳摩尔比对原料转化率和产物选择性等指标的影响.结果表明:该反应在最佳条件压力3 M Pa、温度150℃、氢碳摩尔比3:1(CO/CO2比1/1)时,乙醇选择性为60.87%,甲醇选择性26.33%,氢气转化率50%,CO2转化率100%,CO转化率100%.实验表明:乙醇选择性与热力学理论值还存在差距,后续对催化剂进行改性是下一步研究的重点. 相似文献
102.
塔河碳酸盐岩油藏单井注水吞吐替油机理研究 总被引:1,自引:0,他引:1
目前塔河碳酸盐岩油藏存在着油藏产能下降快,地层压力保持水平低的问题。从分析缝洞型碳酸盐岩油藏的微观孔隙结构着手,通过地应力分析和岩心试验的方法来研究塔河油田部分油井初期产能很高,但很快就能量衰竭、产量递减快的原因。进一步探讨了这部分井注水、升压、闷井、回采机理。为研究缝洞型碳酸盐岩油藏提供一种思路,为合理制定进一步开发方案作参考。 相似文献
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Formation of Gold and Silver Nanoparticle Arrays and Thin Shells on Mesostructured Silica Nanofibers
S. Zhang W. Ni X. Kou M. H. Yeung L. Sun J. Wang C. Yan 《Advanced functional materials》2007,17(16):3258-3266
Mesostructured silica nanofibers synthesized in high yields with cetyltrimethylammonium bromide as the structure‐directing agent in HBr solutions are used as templates for the assembly of Au and Ag nanoparticles and the formation of thin Au shells along the fiber axis. Presynthesized spherical Au and Ag nanoparticles are adsorbed in varying amounts onto the silica nanofibers through bifunctional linking molecules. Nonspherical Au nanoparticles with sharp tips are synthesized on the nanofibers through a seed‐mediated growth approach. The number density of nonspherical Au nanoparticles is controlled by varying the amount of seeded nanofibers relative to the amount of supplied Au precursor. This seed‐mediated growth is further used to form continuous Au shells around the silica nanofibers. Both the Au‐ and Ag‐nanoparticle/silica‐nanofiber hybrid nanostructures and silica/Au core/shell fibers exhibit extinction spectra that are distinct from the spectra of Au and Ag nanoparticles in solution, indicating the presence of new surface plasmon resonance modes in the silica/Au core/shell fibers and surface plasmon coupling between closely spaced metal nanoparticles assembled on silica nanofibers. Spherical Au‐ and Ag‐nanoparticle/silica‐nanofiber hybrid nanostructures are further used as substrates for surface‐enhanced Raman spectroscopy, and the enhancement factors of the Raman signals obtained on the Ag‐nanoparticle/silica‐nanofiber hybrid nanostructures are 2 × 105 for 4‐mercaptobenzoic acid and 4‐mercaptophenol and 7 × 107 for rhodamine B isothiocyanate. These hybrid nanostructures are therefore potentially useful for ultrasensitive chemical and biological sensing by using molecular vibrational signatures. 相似文献
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Yui Tanaka Tadao Nakagomi Itaru Suzuki Kou Matoba Keiji Murayama 《Welding International》2013,27(6):422-430
We conducted the welding experiment using three kinds of test piece, actual size, diaphragm and butt joint. Then, we examined the influence on strength, cooling time and carbon equivalent of weld metal by welding conditions on the different test pieces. We calculated an estimate of cooling time and chemical components. Consequently, we concluded that the strength of weld metal can be estimated by heat input, interpass temperature, carbon equivarent of welding wire and shape of test piece. 相似文献
109.
Abstract A method is developed to eliminate the influence of the perturbed reference wave when long-range electromagnetic fields are investigated by electron holography. Based on phase relationships between the reference wave and the object wave, with digital reconstruction and data processing, we can extract the phase of an object wave from the phase difference between the object wave and the perturbed wave, which is always obtained in normal reconstruction. An example of one-dimension electromagnetic fields is given to verify this method. 相似文献
110.
W.L. Lai S.C. Kou C.S. Poon W.F. Tsang C.C. Lai 《Construction and Building Materials》2009,23(10):3152-3160
This paper reports the results of a durability study of the effects of exposing externally-bonded CFRP-concrete beams to three elevated water temperatures (25 °C, 40 °C and 60 °C). The effects of the heated water environments on the adhesive bonding layer between the CFRP and concrete beams were evaluated by quantifying: (1) the changes of delaminations within the adhesive bonding layer, (2) the changes in resistance to direct shear force and (3) the changes of failure mode distribution. Before the exposure, the condition of the adhesive bonding layer was inspected by infrared thermography (IRT). After exposure, the deterioration of the same bonding layer and failure mode distributions were measured by analyzing the visual photos on the failed CFRP strips. The failure modes were found to be affected largely by the combined effect of elevated temperature and moisture ingress, in which three types were identified: failure at concrete beams, at adhesive bonding layer and interface between CFRP strip and concrete. With these methods, results of 54 specimens show that the adhesive bonding layers of all the specimens had gradually deteriorated in the 40 °C and 60 °C water baths. This deterioration was due to the weakening of the adhesive bonding layers when the glass transition temperature (Tg) or the heat distortion temperature (HDT) was approached or even exceeded, and gradual development of delaminations at adhesive bonding layer. 相似文献