Hydrothermal Synthesis of Acicular Lead Titanate Fine Powders

A pure, acicular lead titanate (PbTiO₃) fine powder with a white color has been prepared by hydrothermal synthesis. It is a new phase of PbTiO₃ with I 4 symmetry, cell parameters of a = 12.358 Å and b = 14.541 Å, and a density of 6.80 g.cm⁻³. The influences of pH (12.5 to 14.4), Pb/Ti ratio (1.0 to 1.6) in the feedstock, reaction temperature (130° to 230°C), time (0.25 to 4 h), starting materials, and additives on the formation of acicular PbTiO₃ under hydrothermal conditions have been investigated. The acicular PbTiO₃ with I 4 symmetry, referred to as the PX phase, can be converted to the perovskite-type (PE phase) of PbTiO₃ at about 605°C while its acicular morphology is essentially unchanged. The preferable conditions for preparing pure acicular PX-phase PbTiO₃ are that the pH is 13.0 to 14.0, Pb/Ti ratio is >1.3, reaction temperature is 170° to 200°C, time is 0.5 to 1.0 h, titanium butoxide (Ti[O(CH₂)₃CH₃]₄) is the starting material, and poly(vinyl alcohol) is an additive. The acicular grain of the PX phase is usually less than 100 nm in diameter and more than 1000 nm in length.     

单相电焊机计量异常分析

针对单相电焊机采用单相感应式电能表进行计量中出现的圆盘反转现象 ,从理论和试验 2个方面分析和验证了 :由于单相电焊机本身的特点 ,无论它在负载还是空载状态 ,总会有 1块电能表出现圆盘反转 ,这是正常的     

Dipole radiation in the proximity of a chiral slab

Radiation of an electric dipole located along an arbitrary direction in the presence of a chiral slab is formulated using matrix analysis in conjunction with Fourier transform techniques. Moreover, dyadic Green's function of such a structure may be determined for further investigation porpose.     

济钢中板厂加快技术创新的对策

本文通过对中板厂近年来技术改造后工艺装置和技术水平的分析，并结合中国加入WTO后对中国钢铁企业面临全球化市场竞争严峻性的认识，提出了中板厂在实现高产生产模式后，应加快技术创新的步伐，尽快完成由高产向优质、多品种、低消耗的高效化生产模式转化的主导思想、措施及建议。     

我国小水电技术发展路线的探讨

根据国际小水电技术发展新动向以及国内政治、政策和市场化经济新发展等情况，讨论确定小水电技术发展路线的原则，提出技术路线的框架和重点，供决策部门参考。表1个。     

U(Ⅳ)-U(Ⅵ)同位素交换反应动力学研究 Ⅰ.Fe~(2+)对U(Ⅳ)-U(Ⅵ)同位素交换反应的催化作用

一、前言由于U(IV)-U(VI)同位素交换体系具有相当大的同位素效应和很好的稳定性,并且容易实现两相回流,这对于分离U同位素的工业应用都是十分有利的。但是,U(IV)-U(VI)同位素交换反应速度非常慢,常温下H~+浓度为1.0—4.0 mol/l时,速度常数为1.0×10~(-4)l~2/mol·s。因此要用U(IV)-U(VI)交换体系浓缩铀同位素,必须研究U(IV)-U(VI)交换反应动力学,找到加快交换反应的方法。     

堤坝渗漏防治技术在社岗防护堤的应用

该文从设计、施工和运行管理等方面介绍了高喷板墙、减压井、充填灌浆以及开挖导渗等技术在飞来峡水利枢纽社岗防护堤中的应用情况,探讨了堤坝渗漏综合防治的技术措施和有关问题。     

Patient thermal comfort requirement for hospital environments in Taiwan

This study examines the comfort criteria of ASHRAE Standard 55-2004 for their applicability in hospital environments. Through an extensive field survey conducted in a university hospital in Taiwan, 927 sets of data have been collected. Above half of the measured samples failed to meet the specifications of Standard 55 comfort zone due to improper humidity control. Acceptability votes by patients exceeded the Standard's 80% criterion, regardless of whether the physical conditions were in or out of the comfort zone. Thermal neutrality, preference and comfort range are compared with other studies conducted in office environments and Standard 55 criteria. Results of chi-square tests revealed that patients’ physical strength significantly effected their thermal requirements. The net effect of health yields a marked difference in thermal neutrality and preference, and also in the comfortable temperature range.     

Highly active lanthanum doped nickel anode for solid oxide fuel cells directly fuelled with methane

Lanthanum doped nickel and YSZ composite anode (LaNi–YSZ) exhibited a greatly reduced polarization resistance and high performance for electrochemical oxidation of hydrogen and methane, which resulted from a fine anode structure with a high dispersion of nickel catalyst and a high catalytic activity towards methane.     

影响长廊阻抗式调压室配筋的几个因素分析

采用三维非线性有限元方法,对四川天全县干溪坡水电站调压室结构特性进行研究,并对几个影响配筋的因素进行敏感性分析,得出各个因素对配筋结果的影响,为调压室结构设计提供科学依据。