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31.
Cypriano G da Trindade Neto Ana LP Fernandes Ana IB Santos Waldenice A Morais Marcos VM Navarro Tereza NC Dantas Mrcia R Pereira Jos LC Fonseca 《Polymer International》2005,54(4):659-666
Complexation of chitosan in aqueous solutions by low molecular weight electrolytes is one of the simplest methods for the preparation of aqueous chitosan dispersions. In this work, the influence of storage time, sulfate concentration, method of preparation and surfactant content on some properties of the resultant chitosan dispersions (turbidity, viscosity and zeta potential) was analyzed. Turbidimetry was adequate to monitor the formation of particles, while viscometry was suitable to monitor changes in the dispersing phase. An analysis of the properties of these systems, mainly in terms of particle–particle and macromolecule–macromolecule interactions was carried out. Copyright © 2004 Society of Chemical Industry 相似文献
32.
V. Anjos M.J.V. Bell E.F. da Silva Jr. R.W.A. Franco I.A. Esquef 《Microelectronics Journal》2005,36(11):977-980
In this paper we report the use of photothermal techniques such as Thermal lens (TL) spectrometry, Photoacoustic and heat capacity, ρcp, to determine the thermo-optical parameters, such as thermal conductivity (K), thermal diffusivity (D), specific heat (cp) and the optical path dependence with temperature (ds/dT), of an undoped polycrystalline 3C-SiC. To our knowledge, this is the first time that Thermal lens technique is used for wide band-gap systems. Results obtained for the polycrystalline sample with TL technique indicates that ds/dT is negative at room temperature. Moreover, the obtained values of thermal diffusivity and thermal conductivity are in good agreement with that found in the literature, indicating that the phototermal techniques can be used to obtain the referred parameters in circumstances where other techniques cannot be used, for example, in harsh environments. 相似文献
33.
Daniel X. Gouveia Odair P. Ferreira Antonio G. Souza Filho M. G. da Silva J. A. C. de Paiva Oswaldo L. Alves Josué Mendes Filho 《Journal of Materials Science》2007,42(2):534-538
The thermal decomposition properties of Mg–Fe hydrotalcites were studied through in situ 57Fe Mössbauer spectroscopy and in situ X-ray diffraction. Abrupt changes in the quadrupolar splitting measured in the Mössbauer spectra revealed a phase transition from the starting lamellar structure to a new crystalline arrangement. By analyzing the Mössbauer parameters we show that the material is highly disordered in the 300–400 °C temperature range. This hypothesis is confirmed by the X-ray results whose diffractograms indicated the collapse of the lamellar structure and the formation of a solid solution. 相似文献
34.
35.
Artem Sokolov Darrell Whitley Andre’ da Motta Salles Barreto 《Genetic Programming and Evolvable Machines》2007,8(3):221-237
This paper evaluates different forms of rank-based selection that are used with genetic algorithms and genetic programming.
Many types of rank based selection have exactly the same expected value in terms of the sampling rate allocated to each member
of the population. However, the variance associated with that sampling rate can vary depending on how selection is implemented.
We examine two forms of tournament selection and compare these to linear rank-based selection using an explicit formula. Because
selective pressure has a direct impact on population diversity, we also examine the interaction between selective pressure
and different mutation strategies. 相似文献
36.
37.
M. D. Kannan Sa. K. Narayandass C. Balasubramanian D. Mangalaraj 《Journal of Materials Science》1992,27(18):5040-5044
Aluminium-neodymium oxide-aluminium thin film capacitors have been prepared by thermal evaporation and the d.c. conduction properties of these films have been studied. The thicknesses of the films have been determined by a multiple beam interferometer. The current-voltage power-law dependence showed that the conduction in these films is space-charge limited. The linear dependence of the current density on the square root of the applied field confirmed the exponential trap distribution. The trap density has been found to be of the order of 1026 m–3. It has also been observed that the Schottky type of conduction is predominant in the high-field region and the height of the Schottky barrier has been determined. It is seen that the conduction mechanism is an activated process with the activation energy decreasing with increasing field. 相似文献
38.
Fbio Gomes Costa Elias Andrade Braga Soraia Teixeira Brando Alexandre de Freitas Espeleta Zênis Novais da Rocha Lílian Maria Tosta Simplício Emerson Andrade Sales 《Applied Catalysis A: General》2005,290(1-2):221-226
Infrared and UV–vis studies of metallocene immobilization on silica are reported here. The results have indicated changes in the Zr coordination sphere of metallocene depending on the immobilization route used. The reaction of [(Cp)2ZrCl2] with silica formed [(Cp)2ZrCl]+[SiO]− species. The same metallocene, reacting with TMA modified silica, formed monomethylated and dimethylated species by the substitution of chloro for methyl ligands, stabilized on the surface by interaction with “MAO-like” species (methylaluminoxane, MAO). These monomethylated and dimethylated cationic zirconium species are the active centers for the polymerization reaction. Different order of TMA addition in the silica modification step generated surface species of a similar nature, differing in their relative quantities. The highest amount of these active species was obtained when the support was added to the TMA solution rather than adding the TMA solution to the silica support. This was the most significant parameter affecting catalytic activity in ethylene polymerization. 相似文献
39.
Nguyen-Huy Dung Pardo Marie-Paule Dogguy.Smiri Leïla 《Materials Research Bulletin》1982,17(3):293-300
The Mn0.23Ga1.85S3 phase belongs to the solid solution , stable at low temperature in the Ga2S3MnS system. It is hexagonal superstructure of the wurtzite, with the Ga2S3α′ type (; Z = 6; space groupe P61 or P65). Its crystal structure has been refined by the least squares method to a final R = 0.06 with 323 independant reflections. This structure is closely related to Ga2S3 α described by Hahn and Frank, and differs only by the partial occupation of the vacant metal site of Ga2S3 by Mn atoms in statistical disorder. 相似文献
40.