Thermal and mechanical properties of the polymers synthesized by the sequential polymerization of propylene and 1‐hexadecene

The block copolymer of poly(1‐hexadecene) (PHD) and polypropylene (PP) was effectively synthesized by the sequential polymerization of propylene and 1‐hexadecene by using highly isospecific TiCl₃/Cp₂Ti(CH₃)₂ (Cp = cyclopentadienyl). The block copolymers had two separate melting temperatures of constituent blocks. The modulus of PHD–PP block copolymer was enhanced as the content of sequentially polymerized PP block was increased. The elongation at break showed positive deviation at the intermediate compositions from the simple additive values of constituent homopolymers. Shape memory effect which utilizes the crystalline PHD block as a reversible phase and the crystalline PP block as a fixed structure was examined. © 2002 Wiley Periodicals, Inc. J Appl Polym Sci 84: 1709–1715, 2002; DOI 10.1002/app.10551     

网络安全评估方法分析

近年来,网络攻击事件时有发生,给社会和企业带来巨大威胁和损失,对于网络安全评估方法的研究成为了热点,文中介绍了网络安全评估方法的研究现状,分析了网络安全评估相关技术,进而探析了网络安全评估方法。     

有效开展Java程序设计线上教学方法探索

2020年初,为应对疫情并保证教学进度,各校纷纷开展线上教学以满足学生在家学习的需求.文章通过分析Java程序设计课程线上教学的特点及困难,借助"雨课堂"和传智播客教辅平台,在授课形式和考核指标等方面进行调整和探究.教学实践表明,调整后的教学模式能有效地保证各环节的教学效果,提高了师生互动性.该模式可为其他课程的在线教学提供参考.     

对分课堂在人机交互设计课程中的应用

人机交互设计课程涉及的知识面广、涵盖领域众多,采用传统授课方式很难激发学生的兴趣,导致授课效果不理想.对分课堂的授课方式将传统的讲授与课堂讨论相结合,将课堂时间一分为二,通过先讲授,再布置作业,最后展开隔堂讨论,进而达到内化吸收、巩固知识的效果.对分课堂可逐步改善人机交互设计课程中教师讲授和学生学习过程中所面临的困境,激发学生自主学习的动力,增强学生探索新知识的欲望和信心,达到授人以渔的目的.     

RLINK: Deep reinforcement learning for user identity linkage

World Wide Web - User identity linkage is a task of recognizing the identities of the same user across different social networks (SN). Previous works tackle this problem via estimating the pairwise...     

智能电能表质量数据采集与质量监控技术研究

针对智能电能表非常容易发生开关跳闸、断电无法工作等故障问题,研究出了一种完善的解决方法;通过调研智能电能表生产企业的信息化系统和生产过程数据,发现生产企业的信息化系统在不同企业间都存在各个信息系统之间分割严重的问题,导致企业内部的数据分布在各个数据仓库内,数据分散,需要对每个生产企业采集装置的采集功能进行定制化对接,基于边缘计算技术的业务系统能够更加切合采集终端,并进行数据处理;本研究将SVG技术和Ajax技术结合使用,构成智能电能表质量监控系统方案框架;经过实验结果表明,通过SVG技术和Ajax技术对智能电力表各项数据信息处理,得到了很好的效果.     

Effect of wafer size on the film internal stress measurement by wafer curvature method

Wafer curvature method has been applied to determine the internal stress in the films using Stoney’s equation. During the film deposition, the wafer fixation on the sample holder will restrict the deformation of the rectangle-shaped wafer, which may result in the stress datum difference along length and width direction. In this paper, the effect of wafer size and the wafer fixation on the TiN film internal stress measured by wafer curvature method was discussed. The rectangle-shaped wafers with different length/width ratios (L/W=1:1, 2:1, 3:1 and 4:1) were fixed as a cantilever beam. After the TiN films deposition, the profiles of the film/wafer were measured using a stylus profilometer and then the internal stress was calculated using the Stoney equation in the film. The results showed that the fixed end of the wafers limited to some degree the curvature of the wafers along the width direction. For film internal stress measured by wafer curvature method, the wafer profile should be scanned along the length direction and the scan distance should be greater than or equal to half of wafer length. When the length/width ratio of the wafer reached 3:1, the wafer curvature and the calculated stress were basically the same at different positions along the length direction. For film internal stress measured by wafer curvature method, it was recommended that the length/width ratio of wafer should be considered to be greater than or equal to 3:1, and the deformed profile was scanned along the length direction.     

对水利工程项目建议书阶段设计取费问题的讨论与建议

通过相关规范、法规进行分析,对于实行立项简化程序未编制项目建议书的水利工程,项目建议书阶段的设计工作应该取费,但不宜直接套用现行设计取费标准;建议根据项目特点在计算的设计费基础上按0.5～0.8的折扣系数取费。     

聚羧酸助磨剂合成及其性能

利用水泥粉磨过程中的机械力促使水解聚马来酸酐（HPMA）与聚乙二醇单甲醚（MPEG）进行酯化反应形成聚羧酸助磨剂。试验研究了HPMA、MPEG、HPMA与MPEG的混合物、HPMA与MPEG的反应合成物对水泥助磨效果以及对砂浆性能的影响。结果表明,HPMA与MPEG都有一定的助磨性,HPMA与MPEG的混合物和反应合成物具有更佳的助磨性能,且可以改善水泥砂浆的流动性能和显著提高水泥砂浆的早期强度。激光拉曼光谱测试表明HPMA与MPEG的混合物和反应合成物与水泥共同粉磨后吸附在水泥颗粒表面,具有相似的拉曼位移图谱。     

响应面分析法优化山楂叶中黄酮的提取工艺

响应面分析法优化山楂叶中黄酮的提取工艺,以黄酮粗提取率为指标,采用乙醇回流法提取。通过单因素试验及响应面分析,研究了提取温度、液固比、乙醇体积分数和提取时间4个主要因素对山楂叶中黄酮粗提取率的影响。采用Box-Behnken中心组合设计和响应面分析法,建立了回归方程的预测模型,确定最佳提取条件为液固比29 mL/g ,乙醇体积分数68％,提取温度64℃,提取时间34 min ,在此条件下黄酮粗提取率为3．07％。试验结果与模型预测值基本相符,因此,该工艺可应用于山楂叶中黄酮的提取。