糖种类和温度对牛肉美拉德反应产物的影响

为了得到更好的牛肉美拉德反应产物,采用析因试验设计,以牛肉美拉德反应物的吸光度、色泽和感官评定为指标对D-木糖、D-葡萄糖和蜂蜜在反应温度92℃和121℃时进行筛选。结果表明:当添加D-木糖在92℃反应时,有利于美拉德反应产物的形成,得到的牛肉美拉德反应物具有较好的增香发色效果。因此,在所考察的糖种类中牛肉美拉德反应最佳糖为D-木糖,最佳反应温度为92℃。     

Effects of light exposure on chlorophyll,sugars and vitamin C content of fresh‐cut celery (Apium graveolens var. dulce) petioles

Effects of light exposure (24 μmol m^?2 s^?1) on fresh‐cut celery nutritional quality were evaluated during 8‐day storage at 7 °C using darkness as control. Light exposure preserved 47% chlorophyll a and 48% chlorophyll b contents more than darkness at the end of storage. Sucrose, reducing sugar and glucose contents in light‐stored petioles were 17%, 25% and 67% higher than those in dark‐stored petioles after 8‐day storage, respectively, thus resulting in higher total soluble solids content in light condition. Moreover, l ‐ascorbic acid content increased at 2‐day storage in light condition and was 46% more than in darkness at the end of storage. The fresh weight loss significantly increased in all petioles, and this increase was markedly accelerated by light exposure with a maximum of 1.43% at the end of storage. Dry matter content was induced more by light exposure than by darkness at 2‐day storage.     

气相色谱法测定10种土壤有机磷农药残留

目的:制订10种土壤中有机磷农药的残留测定方法.方法:微波萃取方法提取,固相小柱净化获得土壤的样品溶液,采用安捷伦DB-608毛细管色谱柱,检测器是火焰光度检测仪器,分析土壤中速灭磷、甲拌磷、二嗪磷、异稻瘟净、甲基对硫磷、杀螟硫磷、溴硫磷、水胺硫磷、稻丰散和杀扑磷十种有机磷农药残留.结果:上述建立的气相色谱方法测定10...     

危废填埋场地下水环境影响评价研究

危险废物具有各种危害性,不仅对人体健康有着威胁,对于环境治理来说也有着极大的消极影响.就目前来说,虽然安全填埋技术已经较为成熟,但在实际实施过程中还是容易出现渗漏事故,渗漏液在地下容易穿透防渗层,从而影响地下水,所以这也是我们需要重视的问题之一.     

Quantification of Se-Methylselenocysteine and Its γ-Glutamyl Derivative from Naturally Se-Enriched Green Bean (Phaseolus vulgaris vulgaris) After HPLC-ESI-TOF-MS and Orbitrap MS n -Based Identification

Orthogonal liquid chromatographic (ion exchange, reversed phase, and ion pairing) and mass spectrometric [electrospray ionization (ESI)-TOF-MS, ESI-Orbitrap MS, and inductively coupled plasma mass spectrometry (ICP-MS)] methods were addressed to identify and quantify selenium species from a naturally Se-enriched green bean (Phaseolus vulgaris vulgaris) sample after proteolytic digestion. While selenomethionine (10.1 mg/kg as Se) and selenate (9.5 mg/kg as Se) could be quantified in a straightforward way by anion exchange LC-ICP-MS technique, a multistep purification protocol was required to identify Se-methylselenocysteine and γ-glutamyl-Se-methylselenocysteine in an unambiguous way prior to quantification by using either in-source fragmentation (LC-ESI-TOF-MS) or collision-induced dissociation (LC-ESI-Orbitrap MS). Finally, Se-methylselenocysteine (2.6 mg/kg as Se) and γ-glutamyl-Se-methylselenocysteine (1.2 mg/kg as Se) could contribute to the overall selenium recovery of 72 %. This sample is the first of the Faboideae subfamily and Phaseolus ssp. to be speciated to such an extent for selenium including γ-glutamyl-Se-methylselenocysteine, a highly potential selenium species, which makes this bean material an ideal candidate for functional food purposes.     

桂皮醛与β-环糊精分子微胶囊的研究

研究了β-环糊精对桂皮醛UV-vis光谱的影响,结果表明:被β-环糊精包结后,桂皮醛的最大吸收波长不变,但吸光度值有规律的下降。Hildebrand-Benesi方程表明二者包结反应的摩尔比为1∶1,结合常数为533.6 L/mol。以桂皮醛为客体,β-环糊精为主体,研究了乙醇体积分数、温度、振荡时间对悬浮液法制备微胶囊中桂皮醛含量的影响。结果表明:桂皮醛含量随乙醇体积分数、温度的升高而降低,随振荡时间延长而增加,但4 h后桂皮醛含量基本不再发生变化。在优化条件下,微胶囊中桂皮醛含量为103.6 mg/g包结物。最后以红外吸收光谱为检测手段证明了β-环糊精对桂皮醛的包结。     

主导烤烟香型风格及感官质量差异的主要化学指标分析

应用方差分析,比较了国内外不同香型风格和感官质量档次的烤烟64种化学指标的差异。结果表明,烟碱、总糖、还原糖、总氮、两糖差、糖碱比、氮碱比、K/(S+Cl)、棕榈酸、亚油酸和油酸、高级脂肪酸总量、二氢大马酮、香叶基丙酮、中性挥发性香味成分总量在不同香型风格和感官质量档次的烤烟间均存在显著或极显著差异;苯甲醛、苯乙醛、4-邻-咖啡基奎宁酸含量主要影响烤烟的香型风格,在不同质量档次的烤烟间差异不显著;氯、硫、有机钾、草酸、丙二酸、苯乙醇、茄酮、苹果酸/柠檬酸、钙/苹果酸、酸碱比主要影响烤烟的感官质量,在不同香型风格烤烟间差异不显著。     

上面发酵青稞啤酒糖化工艺研究

主要研究了青稞啤酒糖化过程中不同的辅料比、料水比以及β-葡聚糖酶添加量对青稞麦汁质量的影响,同时对青稞啤酒的感官及理化指标进行了测定,结果表明,辅料比为30%,β-葡聚糖酶添加量为8μg/mL,料水比为1∶4.0时所得青稞麦汁比较理想,而且加快了麦汁的过滤速度。     

不锈钢金属纤维混纺织物的防微波辐射性能

文中就不同比例的不锈钢金属纤维 涤纶纤维混纺织物的微波屏蔽性进行了测试分析 ,探讨了影响混纺织物屏蔽效果的各种因素 ,为此类功能性产品的设计开发提供了参考。     

BAM网络在车型识别中的应用

设计了一种采用双向联想记忆网络 (BAM) ,仅以车型的轮廓曲线序列作为特征参数 ,能在高速公路不停车收费系统中 ,按照高速公路收费标准对不同车型进行分类的系统 .训练时 ,选择合适的权矩阵 ,把相应的参数训练成网络的稳定状态 ;识别时 ,输入用于区分车型的曲线序列 ,通过对车辆图像进行预处理及图像分析即可利用BAM神经网络识别出车辆的类型 .