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101.
Photoelectrochemical decomposition of bio-related compounds such as amino acids was investigated with a biophotochemical cell comprising a mesoporous TiO2 thin film photoanode and an O2-reducing cathode. It was concluded that a kind of Schottky junction formed at the surface of the TiO2 (called as liquid junction) induced the photodecomposition followed by generation of photocurrent/photovoltage. Complete photodecomposition was investigated by the CO2 formation yield. The photocurrent-photovoltage (J-V) characteristics of amino acids and other typical bio-related compounds were investigated, and the short circuit photocurrent (Jsc), open circuit photovoltage (Voc), and Fill factor (ff) were exhibited. Effect of pH on the photodecomposition of phenylalanine and cysteine were studied; for cysteine alkaline conditions gave a high efficiency, which was interpreted by the high electron-donating ability of the dissociated -S− group. The incident light-to-current conversion efficiency (IPCE) of cysteine was 25% at 350 nm. It was for the first time shown that organic acids gave high internal quantum efficiency (η′) over 8 (=800%) in the photodecomposition; for oxalic acid it was 9.3 (=930%) and for butyric acid 8.2. The alternating current impedance spectroscopy of glycine showed that the cell performance is determined by the chemical reactions at TiO2 or Pt electrodes. 相似文献
102.
A new inclusions rating method using hydrogen embrittlement of a tensile test specimen is proposed. This method is essentially based on the statistics of extremes for inclusion rating where the maximum inclusion size is determined by simple tensile testing of a hydrogen-precharged (H-precharged) specimen. Tensile tests were conducted using two bearing steels (SAE52100 HV 346, HV 447, HV 559, HV 611, HV 678 and ASTM-A485-1 HV 706, HV 715) and one spring steel (SAE5160, HV 651). Fatigue tests were conducted using SAE52100 bearing steel (HV 682). All H-precharged tensile specimens (SAE52100, ASTM-A485-1 and SAE5160) were fractured from internal inclusions except the SAE52100 tensile specimens with a Vickers hardness of HV 346. It was confirmed that the distribution of extreme values of inclusion sizes obtained by SAE52100 tensile testing with H-precharged specimens coincided with those obtained by SAE52100 fatigue testing. From these results, it is presumed that the inclusion rating method by fatigue testing can be replaced by simple tensile testing with H-precharged specimens. The proposed method is more convenient and reliable than other existing inclusion rating methods, i.e., fatigue testing and optical microscopy. The proposed method can be applied to specimens with a Vickers hardness of higher than HV 447. 相似文献
103.
Isao Kagomiya Shinji Matsumoto Ken-ichi Kakimoto Hitoshi Ohsato Hiroshi Sakai Yukinori Maeda 《Journal of the European Ceramic Society》2013,33(5):985-990
We investigated annealing effects of La1?xSrxMnO3 (x = 0–0.6) on electrical resistivity and the temperature coefficient of resistivity (TCR). The annealed samples’ resistivity was lower than those of non-annealed samples. For example, annealing changed the resistivity of x = 0.3 at 25 °C from 4.50 × 10?5 to 3.71 × 10?5 Ω m. Remarkable difference in TCR was observed after annealing, for x = 0.3, 0.45, and 0.5. For x = 0.3, the TCR after annealing was 4000 ppm/°C, which was 1250 ppm/°C greater than that before annealing. We investigated (1) crystal phase, (2) Mn average valence, (3) Mott insulator–metal transition temperature, and (4) microstructure. The microstructure was remarkably varied for annealed x = 0.3 and 0.5. The average grain size of the x = 0.3 increased from 1.60 up to 2.38 μm. Results show that annealing affects resistivity and TCR because of grain growth during annealing. 相似文献
104.
105.
To develop a quantitative method for predicting shrinkage porosity in squeeze casting 总被引:1,自引:0,他引:1
In order to secure high strength and high elongation of suspension parts, it is critical to predict shrinkage porosity quantitatively. A new simulation method for quantitative predic'don of shrinkage porosity when replenishing molten metal has been proposed for squeeze casting process. To examine the accuracy of the calculation model, the proposed method was applied to a plate model. 相似文献
106.
Some tetracycline (TC) antibiotics, including TC and anhydrotetracycline, have been found to enhance specific binding of low
density lipoprotein (LDL) to both LDL receptor-positive and-negative cells at relatively higher concentrations. When incubated
at 37°C, the ability of LDL receptor-negative human fibroblasts to bind 125I-LDL was increased from<2 to 45 ng/mg by 170 μM TC. In normal human fibroblasts and Hep G2 cells, 125I-LDL binding was elevated 1.4- to 2-fold by 113 μM TC. The 125I-LDL binding in the presence of TC was diminished by both heparin and EDTA. The enhancement by TC was not observed when 125I-LDL binding was assayed at 4°C. TC enhanced LDL binding to paraformaldehyde-fixed Hep G2 cells, excluding LDL receptor induction
in the mechanism. These results demonstrated that TC enhanced cellular LDL binding through a process not involving functional
LDL receptors. 相似文献
107.
Shinji Tsuneyuki Hikaru Kitamura Tadashi Ogitsu Takashi Miyake 《Journal of Low Temperature Physics》2001,122(3-4):291-296
Quantum distributions of protons in three high-pressure phases of solid molecular hydrogen are investigated by the first-principles path integral molecular dynamics (FP-PIMD) method, in which interatomic forces are calculated precisely based on the density functional theory. The distributions have entirely different symmetries from those predicted by conventional simulation with classical treatment of protons. Especially in phase II, we found that molecular rotation is hindered by quantum fluctuation of protons, having a strong resemblance to a quantum distribution of impurity muonium in crystalline silicon. The mechanism of this “quantum localization” is clarified by a detailed study of the potential energy surface for the molecular rotation. 相似文献
108.
This letter describes the successful fabrication of a 0.95Sn−0.05Au solder microbump on a compound semiconductor wafer by
reflowing of multi-layer metal film. Since the inherent interdiffusion in Au−Sn phases results in the alloying of multi-layer
films, the composition of micro-bump is well controlled by the thickness of constituent metal films. The micro-bumps melt
at about 220 C, which is close to the lowest eutectic temperature in a Au−Sn system. Solder bonding using 0.95Sn−0.05Au micro-bump
is a very useful technique for the flipchip bonding of compound semiconductor devices. 相似文献
109.
Study on dominant mechanism of high-cycle fatigue life in 6061-T6 aluminum alloy through microanalyses of microstructurally small cracks 总被引:1,自引:0,他引:1
Yoshimasa Takahashi Takahiro Shikama Shinji Yoshihara Tadashi Aiura Hiroshi Noguchi 《Acta Materialia》2012,60(6-7):2554-2567
The mechanism controlling the fatigue life of a precipitation-hardened Al–Mg–Si alloy (6061-T6) at a high-cycle fatigue (HCF) regime of over 107 cycles was investigated in detail. It was found that over 90% of the total fatigue life was occupied by the growth process of a microstructurally small crack at relatively low stress amplitude. The small crack was often found to be arrested and halted for a long period (more than 106 cycles) before it began to grow again, which resulted in a significantly slow growth process. The small crack was then analyzed not only by the conventional fractography but also by the cross-sectional observation of the crack tip region using a focused ion beam and transmission electron microscopy. These observations, supplemented also by a grain orientation analysis using electron backscattered diffraction, explicitly revealed the following points: (i) the small crack growth observed on the specimen surface is primarily related to facet-type cracking that occurs exclusively at the specimen surface; (ii) the growth direction of the small crack has strong anisotropy (i.e. surface-induced growth); (iii) the facet-type cracking is related to the formation of persistent fine slip bands that accompany no structural change of the matrix. On the basis of these results, the micromechanism of small crack growth and its relation to the concept of fatigue limit at the HCF regime is discussed in detail. 相似文献
110.
One of the most important technologies for electric vehicles (EVs) will be drive control technology for the main motor. It is desired that the drive control technology have the following characteristics. (1) It does not require a position/speed sensor for controlling motor drive, which has been mounted on the rotor shaft. (2) It has vector controls that can produce torque quickly, efficiently, and/or precisely. (3) It has wide driving‐range and allows developing EVs with no variable transmission. This paper proposes new drive control technologies for such EVs using a permanent‐magnet synchronous motor as a main motor, and verifies its usefulness through development of an actual EV that can drive on public roads. © 2008 Wiley Periodicals, Inc. Electr Eng Jpn, 165(3): 83–94, 2008; Published online in Wiley InterScience ( www.interscience.wiley.com ). DOI 10.1002/eej.20459 相似文献