In-situ monitoring of decane-in-water emulsion during microwave irradiation

Microwave (MW)-assisted de-emulsification has been attractive in processes of petroleum production and refining. However, the mechanism and optimal operation remain poorly understood. In this study, the behaviour of decane-in-water emulsion under MW irradiation was monitored in-situ through a size measurement system equipped with the reactor and surface tension profiles. The results indicated that the bubble was formed around the oil droplet during MW irradiation. The MW-induced bubbles can enhance de-emulsification in a similar mechanism as the flotation column. The efficiency of MW de-emulsification depends on emulsion content and MW power. Although a higher MW power is more effective, boiling caused by excessive energy must be considered due to the higher local heating. As a result, moderate power is more desirable. For the decane-in-water emulsions in this study, the optimal condition was determined to be around 500 W.     

Influencing factors on nugget formation during multipoint welding by single-side resistance spot welding

ABSTRACT

Recently, weight reduction and improvement of crashworthiness of auto bodies have become important issues. At the same time, stiffness of auto bodies is also needed to ensure a smooth ride. Using hollow parts, such as bended pipes and hydroformed parts, is one of the solutions to the demand for both rigidity and light weight.

To weld hollow parts and sheet panels together, welding methods which allow us to access from one side are required. Single-side resistance spot welding (single-side RSW) process is one of those, and has recently been attracting attention.

However, because of the long current path and small electrode force, it is difficult to concentrate the electric current in the welding spot compared with conventional direct resistance spot welding (direct RSW). Furthermore, in multipoint welding, shunt current will occur easily, and the nugget formation will be inhibited.

To obtain a guideline for making sound nuggets, influencing factors for shunt current were investigated. In addition, a numerical study was carried out to discuss the difference between direct RSW and single-side RSW.

According to the CAE analysis, the shunt current of single-side RSW will be higher rate than direct RSW. The rate of shunt current was influenced by the electrical resistance of its current path. For this reason, with shorter distance between welding points, or with lower electrical resistance of material, it is difficult to get large nuggets. By enhancing the electrical resistance of shunt current path, shunt current could be reduced and a larger nugget would be obtained.     

Lubrication using porous surface layer for cold drawing of steel wire

As a lubricant for steel cold working, metal soap on zinc phosphate coating is widely used. However the lubrication causes hazardous wastes, and hence an alternative system is demanded. The authors proposed to utilize porous layer on workpiece surface as a reservoir of liquid lubricant. In this study, 0.64%C steel wires were oxidized at 923 K under air and chemically reduced by pure hydrogen to form porous surface layer with pores 1–2 μm in diameter. In cold drawing with machine oil, the friction coefficient on the porous surface was 0.06, while that on normal surface was 0.11. The lubrication mechanism with porous surface is discussed.     

Effect of ion implantation layer on adhesion of DLC film by plasma-based ion implantation and deposition

High adhesive diamond-like carbon (DLC) film on SUS304 was obtained using carbon ion implantation between DLC film and substrate material by plasma-based ion implantation and deposition (PBIID). Implantation of mixed silicon and carbon ions to the substrate resulted in much higher adhesion strength than that of the epoxy resin. Effect of ion implantation on adhesion of DLC film was studied by cross sectional STEM observation and EDS element analysis. Enhancement in adhesive strength by ion implantation of mixed carbon and silicon was ascribed to the formation of the multilayer interface consisting of mixed carbon and silicon ion implanted layer and the amorphous layer of carbon and silicon.     

Multi-color light-emitting transistors composed of organic single crystals

We report a novel concept for multi-color light emission from an ambipolar organic single-crystal transistor using natural optical waveguides, the self-absorption effect, Davydov splitting and the unique alignment of the transition dipole moments. We used 9,10-bis-(2,2-diphenylvinyl)-anthracene single crystals to produce blue and green light from identical single-crystal transistors. We also observed red light, which corresponds to the emission from in-gap states that are caused by impurities. Importantly, each of these different colors corresponds to a distinguishable light polarization, which enables us to tune the emission color by using a light polarizer.     

Wavefield characterization of nearly diffraction-limited focused hard x-ray beam with size less than 10 nm

In situ wavefront compensation is a promising method to realize a focus size of only a few nanometers for x-ray beams. However, precise compensation requires evaluation of the wavefront with an accuracy much shorter than the wavelength. Here, we characterized a one-dimensionally focused beam with a width of 7 nm at 20 keV using a multilayer mirror. We demonstrate that the wavefront can be determined precisely from multiple intensity profiles measured around the beamwaist. We compare the phase profiles recovered from intensity profiles measured under the same mirror condition but with three different aperture sizes and find that the accuracy of phase retrieval is as small as λ∕12.     

High-pressure behavior and tribological properties of wind turbine gear oil

Different types of synthetic polyalphaolefin (PAO) oils and a mineral oil are considered in this study. High-pressure viscosity test was done and pressure-viscosity coefficient was measured for all sample oils. Results showed the better performance of PAO oils than the mineral oil. Authors also tested some other tribological properties such as low-temperature behavior, bulk property, frictional coefficient, and wear behavior, which are important for wind turbine gear oil. Low-temperature behavior and frictional property of PAO oils exhibited the better results. Study also showed that the prediction of low-temperature fluidity is possible using the sound velocity in the oil. Finally, the presence of polymethakrylate (PMA) absorbent in PAO oil exposed comparatively better results among all PAO oils.     

Optimal energy consuming planning for a home-based microgrid with mobility constraint of electric vehicles and tractors

This research deals with the energy management problem to minimize the cost of non-renewable energy for a small-scale microgrid with electric vehicles(EV)and el...