Influence of equal channel angular pressing in an acute angle die with a back pressure notch on grain refinement,torsion and mechanical properties of aluminium

Severe plastic deformation improves the strength of a metal by strain hardening. Of the various severe plastic deformation processes, equal channel angular pressing proves to be the right candidate for bulk metal processing. Extensive works were carried out on equal channel angular pressing with channel angle ranging from 90° to 120 ° with or without back pressure on the exit channel. Numerical analyses suggest that reducing the channel angle below 90° would enhance the magnitude of strain imparted and, with prediction of a lesser strain homogeneity in such cases. Hence an acute angled equal channel angular pressing die with a back‐pressure notch sunken into the roof of the exit channel was designed, fabricated and was used for processing pure aluminium. Various mechanical properties of the processed materials were tested and acute angle processing imparted superior tensile strength to the work pieces in a single pass that would require several passes in a conventional equal channel angular pressing die. Substantial improvement in grain refinement and torsional properties was identified.     

Correction to: Comparative Analysis of Processing Techniques’ Effect on the Strength of Carbon Black (N220)-Filled Poly(Lactic Acid) Composites

Strength of Materials - We apologize to the authors and readers for these technical lapses made by the journal staff.     

Development of highly soluble and functional buffalo milk protein concentrate 60 by modifying ionic environment and characterisation thereof

The ionic and protein environment of buffalo skim milk was modified by instant pH drop and its restoration for the development of highly soluble milk protein concentrate-60 (BuMRate–60^@), which resulted in depletion of 88.64% calcium, 89.18% magnesium, 91.69% potassium and 93.96% phosphorous. BuMRate–60^@ displayed excellent wetting, rehydration and solubility (97.76%). The Fourier transform infrared spectrometer spectra revealed significant stretching (C-H and O-H), N-H bending and a large extent of H-bonding. Scanning electron microscopy micrographs presented particles with porous nature and dimples, while transmission electron microscopy confirmed a greater release of minerals with altered casein micelles.     

Fruit and Vegetable Waste: Bioactive Compounds,Their Extraction,and Possible Utilization

Fruits and vegetables are the most utilized commodities among all horticultural crops. They are consumed raw, minimally processed, as well as processed, due to their nutrients and health‐promoting compounds. With the growing population and changing diet habits, the production and processing of horticultural crops, especially fruits and vegetables, have increased very significantly to fulfill the increasing demands. Significant losses and waste in the fresh and processing industries are becoming a serious nutritional, economical, and environmental problem. For example, the United Nations Food and Agriculture Organization (FAO) has estimated that losses and waste in fruits and vegetables are the highest among all types of foods, and may reach up to 60%. The processing operations of fruits and vegetables produce significant wastes of by‐products, which constitute about 25% to 30% of a whole commodity group. The waste is composed mainly of seed, skin, rind, and pomace, containing good sources of potentially valuable bioactive compounds, such as carotenoids, polyphenols, dietary fibers, vitamins, enzymes, and oils, among others. These phytochemicals can be utilized in different industries including the food industry, for the development of functional or enriched foods, the health industry for medicines and pharmaceuticals, and the textile industry, among others. The use of waste for the production of various crucial bioactive components is an important step toward sustainable development. This review describes the types and nature of the waste that originates from fruits and vegetables, the bioactive components in the waste, their extraction techniques, and the potential utilization of the obtained bioactive compounds.     

Modulation of biochemical activity of hepatocytes in culture by matrix substratum

If critical care nurses and advanced practice nurses could identify patients with an increased risk of an unsuccessful outcome from cardiac arrest resuscitation in the hospital, such patients could be monitored with a heightened vigilance. This is the first nursing study to examine pre-existing variables and outcome of cardiac arrest resuscitation in hospitalized patients. The investigators found that heart rate and respiratory rate increased significantly 8 hours before the cardiac arrest in patients with an unsuccessful outcome of resuscitation.     

Loss of glucose transport in developing avian red cells

OBJECTIVE: This study aimed to examine the characteristics of intraretinal changes associated with macular holes and epiretinal membranes by scanning retinal thickness analysis. STUDY DESIGN: The study design was a nonconsecutive case series. PATIENTS: Fifty-six eyes of patients who had either a suspected or clinically diagnosed macular hole or epiretinal membrane were recruited. INTERVENTIONS: A commercial prototype of the scanning retinal thickness analyzer (RTA) was used. It projected a laser slit beam onto the retina and scanned it, in 200 or 400 msec, across a 2- x 2-mm area, yielding multiple optical cross sections that were recorded digitally. RESULTS: Epiretinal membranes were detected, and sites of attachment could be identified. Full-thickness holes corresponded to intraretinal cavities in which the inner retinal surface was broken, usually at the center. The majority of eyes with full-thickness macular holes showed increased retinal thickness surrounding the hole. The so-called "cuff of subretinal fluid," however, often was not present by retinal thickness analysis, despite clinical diagnosis to the contrary, even though retinal thickness analysis is capable of detecting such fluid. In 20 (42%) of 47 eyes diagnosed or suspected of having macular holes, scanning retinal thickness analysis showed findings different from those reported by retinal specialists. CONCLUSIONS: Examination of macular holes with the scanning RTA provides useful information in the diagnosis of macular holes in addition to that obtained through conventional techniques. The findings support the idea that many macular holes develop in association with intraretinal cystic changes. The precise chronology of the events remains to be determined.     

Effect of Constraint on Creep Behavior of 9Cr-1Mo Steel

The effect of constraint on creep rupture behavior of 9Cr-1Mo steel has been investigated. The constraint was introduced by incorporating a circumferential U-notch in a plain cylindrical creep specimen of 5 mm diameter. The degree of constraint was increased by decreasing the notch root radius from 5 to 0.25 mm. Creep tests were conducted on plain and notched specimens at stresses in the range of 110 to 210 MPa at 873 K (600 °C). The creep rupture life of the steel was found to increase under constrained conditions, which increased with the increase in degree of constraint and applied stress, and tended to saturate at a higher degree of constraint. The creep rupture ductility (pct reduction in area) of the steel was found to be lower under constrained conditions. The decrease in creep ductility was more pronounced at a higher degree of constraint and lower applied stresses. Scanning electron microscopic studies revealed a change in fracture behavior with stress and degree of constraint. The fracture surface appearance for relatively lower constrained specimens at higher stresses was predominantly transgranular dimple. Creep cavitation-induced intergranular brittle fracture near the notch root was observed for specimens having a higher degree of constraint at relatively lower stresses. The creep rupture life of the steel under constrained conditions has been predicted based on the estimation of damage evolution by continuum damage mechanics coupled with finite element analysis of the triaxial state of stress across the notch. It was found that the creep rupture life of the steel under constrained conditions was predominantly governed by the von-Mises stress and the principal stress became progressively important with increase in the degree of constraint and decrease in applied stress.     

Effect of high pressure treatment on thermal and rheological properties of lentil flour slurry

Thermal characteristics of high pressure (HP) treated lentil flour dispersions were studied as function of pressure level (350-650 MPa) and moisture content (14-58 g per 100 g of flour). Differential scanning calorimeteric (DSC) measurement of pressure treated lentil dispersions indicated incomplete denaturation of lentil proteins. The protein dentauration temperature (T_d) shifted with applied pressure and moisture content non-systematically. No starch gelatinization peak was detected during thermal scanning of lentil slurries (untreated or treated) irrespective of moisture content or heating rate. High pressure treatment of lentil dispersion significantly reduced the retrogradation behavior compared with that obtained from the thermally gelatinized sample. Dynamic rheological measurement indicated pressure treated lentil slurries exhibited a true viscoelastic fluid. Slurries gradually transformed from solid-like behavior to liquid-like behavior as function of moisture content and pressure level. Fourier transform infrared (FTIR) spectroscopy confirmed insignificant change in amide band of pressure treated slurry. This study has provided complementary information of pressure-induced structural changes on both the molecular and the sub-molecular level of lentil protein.     

Polystyrene‐supported polyoxyethylene bound potassium permanganate as a heterogeneous oxidizing agent

Oxidation behavior of a 2 mol % divinylbenzene (DVB)‐crosslinked polystyrene‐supported permanganate function was investigated toward low molecular weight primary and secondary alcohols and aldehydes. The permanganate function was attached to a polystyrene support through cyclic polyoxyethylene (POE) units immobilized on the support. Contrary to the oxidations catalyzed by low molecular weight permanganate reagents, the oxidation of primary alcohol terminated in the aldehyde stage. The secondary alcohols were converted to the respective ketone and aldehyde to acid. The effect of the variable parameters similar to solvent, temperature, and reagent to substrate ratio was followed. Nonpolar cyclohexane was found to be the best solvent for the present study. Also the reactivity increased with increasing temperature. The oxidizing reagent possesses a long shelf life and could be recycled several times without reduction of capacity and mechanical stability. © 2003 Wiley Periodicals, Inc. J Appl Polym Sci 90: 3708–3717, 2003