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241.
Several new isoxazolidines having varying degree of steric environment and hydrophobic chain length, prepared efficiently using single-step nitrone cycloaddition reactions, are tested for corrosion inhibition of mild steel in 1 M and 5 M HCl at 50-70 °C range by gravimetric and electrochemical methods. All compounds have shown very good corrosion inhibition efficiency (IE%) in acidic solution. Steric crowding around the nitrogen centres and hydrophobic chain lengths as well as increase in temperature (in the presence of the inhibitor in the higher concentration range 100-400 ppm) are found to increase the inhibition efficiency of the isoxazolidines. Thermodynamic parameters (ΔG°ads, ΔH°ads, ΔS°ads) for the adsorption process and kinetic parameters for the metal dissolution (or hydrogen evolution) reaction in the presence of one of the isoxazolidines were determined. Experimental results agree with the Temkin adsorption isotherm. The inhibition of corrosion in 1 M HCl, influenced by both physi- and chemi-sorption, was found to be under mixed control, but predominantly under cathodic control. 相似文献
242.
243.
E. Titus N. Ali G. Cabral J. Gracio P. Ramesh Babu M. J. Jackson 《Journal of Materials Engineering and Performance》2006,15(2):182-186
This article reports key findings on the chemical functionalization of carbon nanotubes (CNT). The functionalization of chemical
vapor-deposited CNT was carried out by treating tubes with polyvinyl alcohol through ultrasonication in water with the aid
of a surfactant. The surfactant is expected to promote the unbundling of aggregated CNT. The characterization of functionalized
samples using thermogravimetric analysis, Fourier transform infrared spectroscopy, and Raman spectroscopy revealed that the
CNT were functionalized by the interaction of carboxylic acid and hydroxyl groups. From the characterization studies, it is
apparent that there is a strong interaction between these functional groups and the covalently bonded carbon in the CNT network.
The functionalization process enabled good CNT dispersion in the solution, and the CNT remained in suspension for many days.
To support the effective functionalization of the tubes, the interaction of functionalized CNT with Ni ions is also demonstrated.
This paper was presented at the fourth International Surface Engineering Congress and Exposition held August 1–3, 2005 in
St. Paul, MN. 相似文献
244.
Existing analytical thermal models for predicting surface burns due to grinding have limited use because of their reliance on parameters that are not readily obtainable in practice. This paper presents a practical and consistent fuzzy rule-based model for estimating the grinding conditions at which “burn limits” occur. The model consists of 37 absolute and eight relative rules. It has a wide range of applications over many types of steels, Alundum wheels, and grinding conditions. It is also simple to implement, from a rule-chart mode to an intelligent on-line adaptive control mode. 相似文献
245.
Recently, by defining suitable fuzzy temporal logics, temporal properties of dynamic systems are specified during model checking process, yet a few numbers of fuzzy temporal logics along with capable corresponding models are developed and used in system design phase, moreover in case of having a suitable model, it suffers from the lack of a capable model checking approach. Having to deal with uncertainty in model checking paradigm, this paper introduces a fuzzy Kripke model (FzKripke) and then provides a verification approach using a novel logic called Fuzzy Computation Tree Logic* (FzCTL*). Not only state space explosion is handled using well-known concepts like abstraction and bisimulation, but an approximation method is also devised as a novel technique to deal with this problem. Fuzzy program graph, a generalization of program graph and FzKripke, is also introduced in this paper in consideration of higher level abstraction in model construction. Eventually modeling, and verification of a multi-valued flip-flop is studied in order to demonstrate capabilities of the proposed models. 相似文献
246.
Omar?N.?Al-BoeridiEmail author S.?M.?Syed Ahmad S.?P.?Koh 《Neural computing & applications》2015,26(6):1505-1513
An off-line handwriting recognition (OFHR) system is a computerized system that is capable of intelligently converting human handwritten data extracted from scanned paper documents into an equivalent text format. This paper studies a proposed OFHR for Malaysian bank cheques written in the Malay language. The proposed system comprised of three components, namely a character recognition system (CRS), a hybrid decision system and lexical word classification system. Two types of feature extraction techniques have been used in the system, namely statistical and geometrical. Experiments show that the statistical feature is reliable, accessible and offers results that are more accurate. The CRS in this system was implemented using two individual classifiers, namely an adaptive multilayer feed-forward back-propagation neural network and support vector machine. The results of this study are very promising and could generalize to the entire Malay lexical dictionary in future work toward scaled-up applications. 相似文献
247.
248.
A robust
observer‐based stabilization method for systems with uncertain parameters and Lipschitz nonlinearities
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This paper deals with the robust observer‐based control design for a class of Lipschitz nonlinear discrete‐time systems with parameter uncertainties. Based on the use of a reformulated Lipschitz property combined with the slack variable techniques and some mathematical artifacts, it is shown that the solution of the discrete‐time output feedback stabilization problem is conditioned by a set of bilinear matrix inequalities, which become linear matrix inequalities by freezing some scalars. Furthermore, we show that some existing and elegant results reported in the literature can be regarded as particular cases of the stability conditions presented here. Numerical examples are provided to show the validity and superiority of the proposed method. Copyright © 2015 John Wiley & Sons, Ltd. 相似文献
249.
Ayesha Kulsoom Di Xiao Aqeel-ur-Rehman Syed Ali Abbas 《Multimedia Tools and Applications》2016,75(1):1-23
A novel image encryption algorithm in streaming mode is proposed which exhaustively employs an entire set of DNA complementary rules alongwith one dimensional chaotic maps. The proposed algorithm is highly efficient due to encrypting the subset of digital image which contains 92.125 % of information. DNA addition operation is carried out on this MSB part. The core idea of the proposed scheme is to scramble the whole image by means of piecewise linear chaotic map (PWLCM) followed by decomposition of image into most significant bits (MSB) and least significant bits (LSB). The logistic sequence is XORed with the decoded MSB and LSB parts separately and finally these two parts are combined to get the ciphered image. The parameters for PWLCM, logistic map and selection of different DNA rules for encoding and decoding of both parts of an image are derived from 128-bit MD5 hash of the plain image. Simulated experimental results in terms of quantitative and qualitative ways prove the encryption quality. Efficiency and robustness against different noises make the proposed cipher a good candidate for real time applications. 相似文献
250.
In this paper, metamodeling and five well-known metaheuristic optimization algorithms were used to reduce the weight and improve crash and NVH attributes of a vehicle simultaneously. A high-fidelity full vehicle model is used to analyze peak acceleration, intrusion and component’s internal-energy under Full-Frontal, Offset-Frontal, and Side crash scenarios as well as vehicle natural frequencies. The radial basis functions method is used to approximate the structural responses. A nonlinear surrogate-based mass minimization was formulated and solved by five different optimization algorithms under crash-vibration constraints. The performance of these algorithms is investigated and discussed. 相似文献