全文获取类型
收费全文 | 1605篇 |
免费 | 104篇 |
国内免费 | 6篇 |
专业分类
电工技术 | 22篇 |
综合类 | 3篇 |
化学工业 | 359篇 |
金属工艺 | 39篇 |
机械仪表 | 57篇 |
建筑科学 | 30篇 |
能源动力 | 111篇 |
轻工业 | 189篇 |
水利工程 | 12篇 |
石油天然气 | 9篇 |
无线电 | 207篇 |
一般工业技术 | 299篇 |
冶金工业 | 82篇 |
原子能技术 | 3篇 |
自动化技术 | 293篇 |
出版年
2024年 | 3篇 |
2023年 | 36篇 |
2022年 | 85篇 |
2021年 | 130篇 |
2020年 | 93篇 |
2019年 | 82篇 |
2018年 | 122篇 |
2017年 | 93篇 |
2016年 | 93篇 |
2015年 | 62篇 |
2014年 | 89篇 |
2013年 | 136篇 |
2012年 | 78篇 |
2011年 | 92篇 |
2010年 | 73篇 |
2009年 | 61篇 |
2008年 | 49篇 |
2007年 | 44篇 |
2006年 | 37篇 |
2005年 | 34篇 |
2004年 | 11篇 |
2003年 | 19篇 |
2002年 | 8篇 |
2001年 | 15篇 |
2000年 | 10篇 |
1999年 | 6篇 |
1998年 | 25篇 |
1997年 | 14篇 |
1996年 | 9篇 |
1995年 | 14篇 |
1994年 | 11篇 |
1993年 | 6篇 |
1992年 | 4篇 |
1991年 | 3篇 |
1990年 | 5篇 |
1989年 | 7篇 |
1988年 | 3篇 |
1987年 | 7篇 |
1986年 | 4篇 |
1985年 | 7篇 |
1984年 | 6篇 |
1983年 | 3篇 |
1982年 | 2篇 |
1981年 | 8篇 |
1980年 | 2篇 |
1979年 | 5篇 |
1978年 | 2篇 |
1975年 | 2篇 |
1974年 | 2篇 |
1967年 | 1篇 |
排序方式: 共有1715条查询结果,搜索用时 15 毫秒
81.
Enhancement of electroconductivity of polyaniline/graphene oxide nanocomposites through in situ emulsion polymerization 总被引:1,自引:0,他引:1
Syed Muhammad Imran YouNa Kim Godlisten N. Shao Manwar Hussain Yong-ho Choa Hee Taik Kim 《Journal of Materials Science》2014,49(3):1328-1335
The present study introduces a systematic approach to disperse graphene oxide (GO) during emulsion polymerization (EP) of Polyaniline (PANI) to form nanocomposites with improved electrical conductivities. PANI/GO samples were fabricated by loading different weight percents (wt%) of GO through modified in situ EP of the aniline monomer. The polymerization process was carried out in the presence of a functionalized protonic acid such as dodecyl benzene sulfonic acid, which acts both as an emulsifier and protonating agent. The microstructure of the PANI/GO nanocomposites was studied by scanning electron microscopy, transmission electron microscopy, X-ray diffraction, UV–Vis spectrometry, Fourier transform infrared, differential thermal, and thermogravimetric analyses. The formed nanocomposites exhibited superior morphology and thermal stability. Meanwhile, the electrical conductivities of the nanocomposite pellets pressed at different applied pressures were determined using the four-probe analyzer. It was observed that the addition of GO was an essential component to improving the thermal stability and electrical conductivities of the PANI/GO nanocomposites. The electrical conductivities of the nanocomposites were considerably enhanced as compared to those of the individual PANI samples pressed at the same pressures. An enhanced conductivity of 474 S/m was observed at 5 wt% GO loading and an applied pressure of 6 t. Therefore, PANI/GO composites with desirable properties for various semiconductor applications can be obtained by in situ addition of GO during the polymerization process. 相似文献
82.
83.
Zahra Shabeh tu Syed Waqar A.A. Rafiq Nouman Shah Wiqar H. Iqbal Zafar 《Protection of Metals and Physical Chemistry of Surfaces》2021,57(2):321-328
Protection of Metals and Physical Chemistry of Surfaces - Chromium oxide thin films were grown on Al2O3 substrates by ablating a pure Cr2O3 target using a KrF excimer laser. The energy density on... 相似文献
84.
V. S. Vendamani Syed Hamad V. Saikiran A. P. Pathak S. Venugopal Rao V. V. Ravi Kanth Kumar S. V. S. Nageswara Rao 《Journal of Materials Science》2015,50(4):1666-1672
We report a detailed study on the synthesis of ultra-small (1–10 nm) colloidal silicon nanoparticles (Si NPs) by ablating porous silicon (pSi) in acetone using femtosecond laser pulses. Porous silicon is considered as a target material for ablation because it contains a large number of light emitting silicon nanoparticles. The pSi samples were prepared by anodic etching of silicon in aqueous HF solution for different etching current densities. Transmission electron microscope measurements confirmed the successful formation of well-isolated spherical silicon nanoparticles. The average size of spherical NPs were estimated to be ~7.6, ~7, and ~6 nm when anodic etching current densities of 5, 10, and 20 mA/cm2 were used respectively for preparing pSi targets. The crystallinity of these Si NPs was confirmed by selective area electron diffraction and Raman spectroscopy measurements. The observed blue shift in the absorption and emission spectra are attributed to reduction in the average particle size with increase in etching current density. These Si NPs may be useful for fabricating low-dimensional microelectronic compatible photonic devices. 相似文献
85.
Frank J. Gaudet Syed R. Qasim 《The International journal of environmental studies》2013,70(1-2):127-135
Industrial wastes containing heavy metals can interfere with the normal operation of municipal wastewater treatment plants utilizing biological treatment processes. It is well known, however, that activated sludge can become acclimated to toxic levels of heavy metals if the dosages are increased gradually. Although such an acclimation procedure could prevent inhibitory effects of slug loads of toxins, the use of toxic heavy metals for normal plant operation is too perilous for consideration. It is, however, acceptable to utilize a nontoxic metal that may give general tolerance to toxic metals. Laboratory experiments were conducted to examine the use of ferric chloride acclimation for treatment against heavy metal toxicity of an activated sludge process. The oxygen uptake of acclimated and unacclimated seed was measured by respirometry to determine the inhibitory effects of Ag and Pb. The toxic effects of Ag and Pb were greatly reduced for acclimated seed. The experimental data area utilized in kinetic rate equations, and families of curves are developed to show the inhibition of Ag and Pb at a range of concentrations when the activated sludge is acclimatized at different concentrations of Fe(III). 相似文献
86.
Brajendra Kumar Singh Jeremy Coulter Mohammad Abdul Ghani Sayani Syed M. Sami Mohammad Khalid Kemal E. Tepe 《The International journal of environmental studies》2013,70(5):765-776
Communication systems are needed to integrate generated power from wind farms with the electrical grid. This paper provides a comprehensive review of available communication technologies, protocols and objectives related to wind energy and electrical grid integration. This paper summarizes the communication system solutions for wind generation. A major obstacle is an absence of unified communication architectures and standards. 相似文献
87.
Aluminium phosphate (AlPO4) was characterized using X-ray diffractometry (XRD), Fourier Transform infrared (FTIR), point of zero charge (PZC) and dissolution studies. XRD showed the sample to be amorphous, FTIR confirmed the presence of OH groups on the surface and PZC was determined at pH 3.45. The dissolution study illustrated a decrease in dissolution with an increase in the pH. Potentiometric titration data were fit to the Gaines–Thomas equation, which showed that AlPO4 is a weakly acidic ion exchanger. Sorption studies were carried out at pH 4–6 and temperatures 293–323 K. The uptake of metal ions was observed to increase with an increase in the pH and temperature. The surface selectivity towards metal ions was found in the order Pb2+> Cu2+> Cd2+. Sorption data were fit to the new equation derived from the proposed mechanism for metal ion uptake. Various parameters such as stoichiometry of the surface H+ ion release, equilibrium constant, standard enthalpy, entropy and free energy changes were evaluated from the plots. The values of all these parameters were found to be closely related to the values reported in the literature. 相似文献
88.
Syed Jafar Mehdi Hector Rosas-Hernandez Elvis Cuevas Susan M. Lantz Steven W. Barger Sumit Sarkar Merle G. Paule Syed F. Ali Syed Z. Imam 《International journal of molecular sciences》2016,17(9)
Currently, the lack of new drug candidates for the treatment of major neurological disorders such as Parkinson’s disease has intensified the search for drugs that can be repurposed or repositioned for such treatment. Typically, the search focuses on drugs that have been approved and are used clinically for other indications. Kinase inhibitors represent a family of popular molecules for the treatment and prevention of various cancers, and have emerged as strong candidates for such repurposing because numerous serine/threonine and tyrosine kinases have been implicated in the pathobiology of Parkinson’s disease. This review focuses on various kinase-dependent pathways associated with the expression of Parkinson’s disease pathology, and evaluates how inhibitors of these pathways might play a major role as effective therapeutic molecules. 相似文献
89.
Laraib A. Khan Ayesha Kausar Syed Tajammul Hussain Zafar Iqbal Richard J. Day Ahmed Shuja Syed Zaffar M. Khan 《Polymer Engineering and Science》2014,54(4):887-898
In this effort, Quickstep, a relatively a new technique, have been employed for manufacturing of composite materials. The cure schedule provided by a prepreg manufacturer is usually designed for autoclave or other traditional processing techniques and thermosetting resin systems are formulated for ramp rate curing 2–3 K min?1. While in case of Quickstep processing, ramp rates of 15 K min?1 can be achieved, thus changing the chemorheology of resin. The cure process of 977‐2A carbon/epoxy composites was evaluated for Quickstep processing using differential scanning calorimetry (DSC), dynamic mechanical and thermal analysis, and Fourier transformed infrared and results were compared with cure cycle employed for autoclave curing. Optimum hold time for Quickstep processing at upper curing temperature (180°C) was determined using DSC. The hold time of 120 min at 180°C was found to be suitable for Quickstep cure cycle, producing a panel of similar degree of cure to that achieved through autoclave processing schedule. Final degree of cure was dependent on time spent at upper cure temperature and slightly on initial steps of the cure cycle which was used to control the resin flow, fiber wetting, and void removal. Quickstep processed samples exhibited higher Tg and crosslink density and similar molecular network structure to the autoclave cured samples. POLYM. ENG. SCI., 54:887–898, 2014. © 2013 Society of Plastics Engineers 相似文献
90.
Sougata Jana Syed Ansar Ali Amit Kumar Nayak Kalyan Kumar Sen Sanat Kumar Basu 《Chemical Engineering Research and Design》2014
This article describes the development, optimization, and evaluation of Carbopol 940 topical gel containing aceclofenac-crospovidone (1:4) solid dispersion using “Quality by Design (QbD)” approach based on 23 factorial design. The effect of crospovidone, tri-ethanolamine, and ethyl alcohol amount on the drug permeation profile of the topical gel containing aceclofenac-crospovidone solid dispersion was optimized by 23 factorial design. The optimized gel showed improved permeation profile with cumulative drug permeation of 26.262 ± 2.157%, and permeation flux of 0.059 ± 0.011 μg/cm2/h. These gels were characterized by pH, viscosity, gel strength and FTIR study. The in vivo anti-inflammatory activity of the optimized gel was evaluated in rats using carrageenan-induced rat-paw oedema model and found excellent anti-inflammatory comparable with a marketed gel without producing any skin irritation. 相似文献