Correction and evaluation of the effect due to parasitic motion on primary accelerometer calibration

Primary accelerometer calibration is carried out under the assumption that a vibration exciter gives a rectilinear motion to an accelerometer to be calibrated. However practical vibration given by the vibration exciter includes parasitic motion such as transverse, rocking, and bending motion. Such parasitic motion would give two serious effects on primary calibration results, transverse motion effect and vibration distribution effect. Transverse motion effect is caused by an inner product of the vectors of both transverse motion and transverse sensitivity. On the other hand, the vibration distribution effect is caused by relative motion between a sensing point of accelerometer and a spot sensed by the interferometer. As these effects have close interaction between parasitic motion and measuring instruments, it would be very difficult to evaluate them by measuring independently each component.     

Effects of Sampling Tube Geometry on Soft Clayey Sample Quality Evaluated by Nondestructive Methods

Sample disturbance caused by difference in sampling tube geometry was evaluated by two nondestructive methods: the measurement of the residual effective stress (p_r') by ceramic disc; and the use of the bender element to ascertain the shear wave velocity (V_s), and thus the maximum shear modulus (G_BE). Samples were measured under atmosphere, i.e., not under confined stress conditions. The soil samples were obtained from two sources: reconstituted Kasaoka clay prepared in the laboratory, and at the test site at Takuhoku, Hokkaido, Japan. Samplers with different geometrical designs, referring to the Japanese standard stationary piston sampler, were used for the model ground and field sampling. The geometrical effects of the sampling tube, for example, the thickness of the tube wall, the edge angle, and the existence of a piston were carefully examined. The quality of the samples taken with different samplers was evaluated by p_r' and G_BE, values which were normalized by the in situ vertical effective stress (σ'_vo) and G_f measured by the seismic cone test in the field. It was found from these studies that p_r'/σ'_vo and G_BE/G_f vary considerably due to the geometry of the sampler, with the edge angle of sampling tubes being the most important feature in obtaining high quality samples. The wall thickness, and thus, the area ratio of the sampler is not critical to the sample quality if the edge angle is sharp enough. The existence of the piston does not significantly influence the sample quality in field samples. Furthermore, the correlation between G_BE and p_r' was also investigated, and it was found that the two parameters are strongly dependent.     

GPC Profile Change of Potato Starch with Extrusion Processing

Native potato starch (moisture content 15%) was treated by twin screw extruder under four operating conditions with varying barrel temperatures (110°C–230°C). These modified starch samples were compared to native and drum-dried starch. Starch sample solution for gel chromatography was prepared by the three methods (acidic, alkaline, and neutral methods). They were subjected to gel chromatography on Toyopearl HW-75, and some difference was found among the three gel chromatographic patterns obtained from the same starch solution. This discrepancy among GPC patterns suggests formation of some types of anhydro-bonds between chains of amylopectin and or amylose in the extrusion process. Elevating barrel temperature increases degree of depolymerization. The size of fragments formed with the treatment is bigger than that of oligosaccharides but smaller than that of amylose.     

Explanation of impact load curve in ball impact test in relation to thermal aging

Solder joints are required to have high impact strength for use in portable electronic products. To make solder joints with high impact strength, qualitative evaluation methods of impact strength are required. Ball impact tests have been widely adopted in evaluating the impact strength of solder joints because of their easy implementation. Impact load curves obtained from ball impact tests are used as an evaluation indicator of impact strength of solder joint. However, a relation between fracture behavior and impact load curve has not yet been clarified, and an explanation of the impact load curve has not yet been provided in detail. In addition to this, detailed study about the relation between IMC layer thickness and impact strength has not been performed, although the IMC layer thickness formed at the interface would significantly affect the impact strength of the solder joint. This study aimed to explain the impact load curve in the ball impact test and to reveal the effect of the IMC layer thickness on the impact strength of the solder joint. Sn–3.0Ag–0.5Cu solder was reflowed on an electroless Ni–P plated Cu substrate (Ni–P), and a ball impact test was then carried out to evaluate the impact strength. This study found that the ball impact test is effective to evaluate the interfacial strength of solder joints. In the impact load curve, it is estimated that the solder bump keeps deforming until the interfacial crack initiates (maximum load), and the interfacial crack initiates after the maximum load and propagates along the interface between the solder and Ni–P. The suitable evaluation of impact strength became possible by measuring the correspondence relation between the deformation distance of the solder bump after fracture and the energy until maximum load and the relation between the area fraction of the residual solder on the fractured pad and the energy after maximum load. And, it is proved that the impact strength decreased with increasing aging time because the growth of the IMC layer remarkably degraded the interfacial strength of the solder joint.     

Three replacement models with two kinds of damage

This paper proposes three replacement policies for a modified cumulative damage model. An item receives shocks and suffers two kinds of damage: one is produced by shocks and the other increases with time at constant rate a. It fails only when the total damage exceeds a failure level K at some shock and is replaced before failure at time T, at shock N, or at damage k. The expected cost rates of three replacement policies are obtained. When shocks occur in a Poisson process, optimal T^*, N^* and k^* which minimize them are computed numerically. Finally, two extended cases where a is a function of time and K is a random variable are also considered.     

Photovoltaic characteristics of phosphorus-doped amorphous carbon films grown by r.f. plasma-enhanced CVD

The phosphorus-doped amorphous carbon (n-C:P) films were grown by r.f. power-assisted plasma-enhanced chemical vapor deposition at room temperature using solid phosphorus target. The influence of phosphorus doping on material properties of n-C:P based on the results of simultaneous characterization are reported. Moreover, the solar cell properties such as series resistance, short circuit current density (J_sc), open circuit current voltage (V_oc), fill factor (FF) and conversion efficiency (η) along with the spectral response are reported for the fabricated carbon based n-C:P/p-Si heterojunction solar cell were measured by standard measurement technique. The cells performances have been given in the dark I–V rectifying curve and I–V working curve under illumination when exposed to AM 1.5 illumination condition (100 mW/cm², 25 °C). The maximum of V_oc and J_sc for the cells are observed to be approximately 236 V and 7.34 mA/cm², respectively for the n-C:P/p-Si cell grown at lower r.f. power of 100 W. The highest η and FF were found to be approximately 0.84% and 49%, respectively. We have observed the rectifying nature of the heterojunction structures is due to the nature of n-C:P films.     

Detection and Quantitation of Left-to-Right Shunts from Radionuclide Angiocardiography Using the Homomorphic Deconvolution Technique

The homomorphic filtering method is described for the detection and quantitation of left-to-right shunts from radionuclide angiocardiography. First, the method is investigated theoreticatly and numerically using a realistic model with systemic recirculation. It is demonstrated that even in a noisy situation the shunt flow fraction can be relatively well estimated, if only the characteristics of the fiters used are suitable. Second, the method is applied to real data, i.e., the pulmonary time-activity curves from radionucUde anglocardiography. The presence or absence of a left-to-right shunt is determined using the ratio AT/MTT. The pulmonary-to-systemic flow ratios calculated from the areas of the two decomposed curves are compared with those from oximetry at cardiac catheterization. Good agreement between the Qp/Qs ratios calculated by oximetry and radionucUide angiocardiography is obtained.     

Capillary gas-liquid chromatographic separation of oxo and oxo-hydroxy bile acid isomers of theallo and normal series

Capillary gas-liquid chromatographic separation was studied for 60 oxo and oxo-hydroxy bile acids of theallo (5α-H, A/B-trans) and normal (5β-H, A/B-cis) series, which differ from one another in the number, position, and configuration of oxo and hydroxy groups at positions C−3, C−4, C−6, C−7, and/or C−12. Good separation of the isomers was achieved by the use of an aluminum-clad fused-silica capillary column coated with bonded and cross-linked methyl polysiloxane.     

Liver phosphatidylcholine hydroperoxidation provoked by ethionine-containing choline-deficient diet in mice

It is shown that peroxidation of phosphatidylcholine (PC) is enhanced in liver of mice fed a hepatocarcinogenic choline-deficient diet containing 0.1% w/w ethionine. Mice were divided into 4 groups and fed for 3 weeks one of the following diets: choline-supplemented; choline-supplemented containing ethionine; choline-deficient; and choline-deficient containing ethionine. Phosphatidylcholine hydroperoxide (PCOOH) of liver lipids was measured by high performance liquid chromatography using a chemiluminescence detector. Mice fed a choline-deficient diet containing ethionine showed 6-fold higher PCOOH levels than the choline-supplemented control mice: the PCOOH/PC molar ratios of liver lipids were 32.3×10⁻⁵ and 5.6×10⁻⁵, respectively. In addition to this remarkable degree of lipid peroxidation in liver of mice fed the choline-deficient diet containing ethionine, we also observed a significant liver fatty infiltration, a decrease in plasma and liver α-tocopherol, and an increase in liver injury-indicative enzyme activities. Also, marker enzymes for hepatocarcinogenesis, glucose-6-phosphatase and γ-glutamyl transpeptidase were affected. These data suggest that enhanced hydroperoxidation of phosphatidylcholine may participate in hepatocarcinogenesis provoked by choline deficiency in the presence of ethionine.