The effect of sensitization on the hydrogen-enhanced fatigue crack growth of two austenitic stainless steels

Fatigue crack growth tests were performed to evaluate the susceptibility to hydrogen-enhanced crack growth of AISI 304 and 316 stainless steels (SSs). Sensitization treatment at 650 °C 100 h played little effect on the fatigue crack growth behavior in air, regardless of testing specimens. However, hydrogen accelerated the fatigue crack growth of various specimens to different degrees; sensitized specimens were more susceptible as compared with the un-sensitized ones.

Fatigue fracture appearance of various specimens tested in air exhibited mainly transgranular fatigue fracture together with rarely intergranular fracture and twin boundary separation. Meanwhile, intergranular fracture was found for sensitized specimens tested in hydrogen. Extensive quasi-cleavage fracture related to the strain-induced martensite accounted for the hydrogen-accelerated fatigue crack growth of unstable austenitic SSs. On the other hand, the lower susceptibility of 316H specimens could be attributed to the partial austenite transformation, as evidenced by a mixture of transgranular fracture feature and quasi-cleavage.     

Thermal stress analysis and design optimization of direct chip attach (DCA) and chip scale package (CSP) in flip chip technology

Underfill encapsulation is a technique used to reinforce the solder bumps between the chip and the substrate in flip chip technology. To determine the optimal geometrical parameters and material properties for the package and candidate underfill materials is an important strategy for improving the thermo-mechanical reliability of flip chip packages. In this study, a stress-function-based energy method was developed to evaluate the interfacial peel and shear stress distributions in multilayered packaging structures. The stress functions were expressed in terms of sine and cosine trigonometric series. Simple programming and short CPU time lead to accurate stress distributions. After comparisons with other proposed numerical methods and results, the developed model was then coupled with a Genetic Algorithm to optimize the design of the direct chip attach (DCA) and chip scale package (CSP) in order to diminish the interfacial stresses and the possibility of crack initiation. The results revealed that the maximum peel and shear stress values were productively decreased and their peaks moved toward the center after conducting the optimizations in both cases. Improved geometrical and material parameters of the flip chip package were determined.     

Equations for helical gears with pinion circular arc teeth and gear involute teeth

Abstract

In this paper, the theory of gearing and the concept of differential geometry have been applied to derive equations for helical gears with pinion circular arc teeth and gear screw involute teeth. The paper covers: (a) generation of conjugate gear tooth surfaces with localized bearing contact; and (b) derivation of equations for gear tooth surfaces and their unit normals.     

Laminar forced convection in wedge flow with separation

Abstract

A perturbation method is used to study the steady and unsteady laminar boundary layer heat transfer from a wedge with separation for a step‐discontinuity in the surface temperature. The analytic solutions obtained can be used to calculate the steady and unsteady heat transfer rate with arbitrary surface temperature. The effects of the Prandtl number on the temperature distribution and the heat transfer rate are discussed in detail. The solution is valid for large or moderate Prandtl number.     

Distribution of diamond grains in fixed abrasive wire sawing process

For over 20 years, wire sawing has been the primary method used for slicing ingots of silicon, sapphire, and silicon carbide into wafer substrates. Fixed diamond wire sawing has recently emerged as an alternative to slurry wire sawing as a means to shorten the time required for slicing and reduce the usage of slurry. The distribution of diamond grains on the wires strongly influences slicing performance in terms of material removal, surface topography, and subsurface damage. However, few studies have investigated this topic. This study established a model with which to simulate the distribution of diamond grains. Simulation results demonstrate that a higher density distribution reduces the rate of material removal because the loading is shared by the abrasives, thereby preventing the grains from penetrating deeply enough into the workpiece to facilitate the removal of material. Lower distribution density was shown to increase the loadings on the abrasives. These results demonstrate the importance of distribution density of diamond abrasives on the wire with regard to slicing performance.     

Effect of iron particle addition on the pseudocapacitive performance of sol–gel derived manganese oxides film

Manganese oxide electrodes with promising behavior were prepared successfully by sol–gel process. Manganese oxide films were also modified with the addition of submicron-crystalline iron powders. Effects of post heat treatment and iron submicron-powder addition on the material characteristics and electrochemical capacitance of the manganese oxide electrodes were investigated. The experimental results showed that manganese oxide films composed from metal-organic precursors at 250 °C heat treatment, while formation of MnO₂, Mn₂O₃, Mn₃O₄, Fe₂O₃, and Fe₃O₄ phases were observed after heat treatment at a temperature higher than 300 °C. The specific capacitances were 48.9, 140.1, 212.7, and 81.1 F g⁻¹ for manganese oxide films heat treated at 250, 300, 350, and 400 °C, respectively. The specific capacitances were 75.7, 227.3, 247.9, and 152.9 F g⁻¹ for manganese/iron oxide films (Mn:Fe = 100:1) heat treated at 250, 300, 350, and 400 °C, respectively. The manganese/iron oxide films (Mn:Fe = 100:1) treated at 350 °C exhibited the highest specific capacitance 247.9 F g⁻¹ of the electrodes investigated in the present study. After 1000 cyclic voltammetry tests, the specific capacitance decreased by only 10 percent. The surface morphology of this film exhibited powders with linked nano-sized particles. The number of special particles reached a maximum after heat treatment at 350 °C. The experimental results showed that post heat treatment and iron submicron-particle addition may change the surface morphology and structure, increase the specific capacitance, and improve the electrochemical performances of the manganese oxide electrodes.     

A 16-bit 65-MS/s 3.3-V pipeline ADC core in SiGe BiCMOS with 78-dB SNR and 180-fs jitter

The analog-to-digital converter presented in this work demonstrates the efficiency of the straight 2.5 bit-per-stage approach for the implementation of pipelined switched-capacitor architectures targeting up to 16-bit resolution and 65-MS/s sampling rate. The test chip has been fabricated in a 45-GHz f/sub T/, 0.4-/spl mu/m 3.3-V SiGe BiCMOS process that makes it suitable for integration with an RF front-end toward an antenna-to-DSP communication processor. Performance of 78.3 dBFS SNR, 88dBc SFDR at 65 MS/s, 1 MHz input is obtained without trimming or calibration, dissipating 970 mW total with external references. Since the 4 V/sub p-p/ signal range chosen for high SNR could lead to distortion in the Sample/Hold and the pipelined quantizer with only 3.3-V supply, a fast and accurate SPICE simulation technique for INL investigation is described that enabled detailed diagnosis of potential nonlinearity sources. Theoretical analysis and practical implementation of the clock circuit are also discussed allowing the design of a CMOS-based clock featuring 180-fs jitter, which preserves high SNR against input frequency: state-of-the-art 73.5dBFS have been observed at 150 MHz input, popular intermediate frequency (IF) for single-heterodyne BTS receivers. Finally, the figures of merit encompassing power, effective resolution, and speed rank the dynamic performance of the ADC core among the best in its class.     

A bibliometric analysis of hydrogen energy literature, 1965–2005

The present study explores the characteristics of hydrogen energy literature from 1965 to 2005 based on the database of Science Citation Index Expanded (SCIE) and its implication using the bibliometric techniques. The results of this work reveal that the literature on hydrogen energy grows exponentially with an annual growth rate of about 18% for the last decade. Most of document type is in the form of journal articles or meeting abstracts, constituting 90.17% of the total literature and English is the predominant language (94.66%). USA, Japan and China are the three biggest contributing countries on hydrogen energy literature publishing, 25.8%, 14.9%, 7.7%, respectively. The Chinese Academy of Sciences in China is the largest contributor publishing 308 papers. The journal literature on hydrogen energy does not confirm the typical S-shape for the Bradford-Zipf plot, but five core journals, i.e. International Journal of Hydrogen Energy, Journal of Power Source, Journal of the Electrochemical Society, Solid State Ionics, and Electrochimica Act, contributing about 41% can be identified. Journals with highly cited articles and most highly cited articles are also identified, in which the most highly cited article receives more than 1,000 citations.     

Parent influences on adolescent peer orientation and substance use: the interface of parenting practices and values

This study examines how experiences in the family domain may magnify or mitigate experiences in the peer domain, and how processes in both milieus may influence adolescent substance use. The data derived from 666 European American mother-adolescent dyads and 510 European American father-adolescent dyads. Consistent with individuation-connectedness theory, mothers' responsiveness lessened their adolescents' orientation to peers, which, in turn, reduced adolescent substance use. This process was moderated by maternal values regarding adolescent alcohol use; that is, the relation of maternal responsiveness to adolescent substance use depended on the extent of maternal approval or disapproval of adolescent alcohol use. Among fathers, closer monitoring was directly associated with less adolescent substance use, with stronger effects among fathers who held more disapproving values regarding adolescent alcohol use. Theoretical, methodological, and pragmatic implications are given.     

Use of food quotients in human doubly labeled water studies: comparable results obtained with 4 widely used food intake methods

Information on the macronutrient composition of the diet is needed in doubly labeled water studies to convert measured rates of carbon dioxide production into values for total energy expenditure. There is no general consensus, however, about the best method to determine food intake for this purpose. Four common methods of measuring food intake (7-day weighed food intake, 24-hour recall, and Fred Hutchinson Cancer Research Center/Block and Willett food frequency questionnaires) were tested for their ability to provide comparable food quotient and total energy expenditure data in doubly labeled water studies in 10 young and 10 older women. All methods gave mean values for total energy expenditure that were within 1% of each other. Individual values obtained using the 24-hour recall and food frequency questionnaires were within +/- 3% (standard deviation) of values determined using data from the 7-day weighed food record. These results suggest that it is not necessary to use time-consuming and expensive 7-day food records in doubly labeled water studies; instead, food intake data obtained more easily by 24-hour recall or food frequency questionnaire can provide comparable data.