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Thermal loading induces modifications of the precipitation microstructure of Al–Si–Cu–Mg alloys. This study focuses on the effect of deformation on precipitation microstructure during thermomechanical loadings. Several specimens were thermomechanically cycled while others were exposed to the same thermal cycles without any mechanical loading. The nature and morphological characteristics of the precipitation microstructure of the thermomechanically cycled specimens are compared to those of the thermally aged ones, using transmission electron microscopy (TEM), in order to assess the effect of deformation on the precipitation microstructure and especially on the kinetics of precipitate growth. The absence of any significant effect of superimposed straining during thermal cycling is discussed. Implications for the prevision of yield strength degradation during service operation are briefly presented.
相似文献Oriented materials are of great importance, but their formation is rarely described. Here, nine Al/Al2O3 systems were designed to identify the dominant factors. Electron back-scattered diffraction indicates that the new Al crystal(s) with one or multiple orientation(s) can be stimulated by one single-crystal Al2O3 substrates. Synchrotron radiation diffraction shows that the preferred orientation(s) is/are determined based on the initial stage of the liquid–solid transition. The nonpreferred orientation can be suppressed through competition.
相似文献TiN coating is provided by reactive magnetron coating on a 304 stainless steel sample with a notch introduced at the edge of the sample. The sample is subjected to a tensile stress close to that of yield strength of the stainless steel. Optical and scanning electron microscopy characterization showed the distribution of buckled and delaminated regions around the notch. The distribution of the size of the partially delaminated regions of the film on the substrate is determined by transient thermo-reflectance. The stress field due to the notch is represented by that of a circular hole present at the tip and the variation of compressive and shear strain as a function of radial and angular coordinates is determined. The distribution of buckled and delaminated regions is found to follow the compressive strain variation around the notch. The size of the partially delaminated film is found to be larger near the notch and decreased with distance from the notch. The results illustrate that structures with regions of stress concentration should not be provided with brittle protective coatings that will delaminate.
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