A Newly Developed Non, Destructive Tritium Measurement Technique and Its Application to V-4Cr-4Ti Alloy

A non-destructive and in-situ technique for the measurement of tritium in materials, namely β-ray-induced X-ray spectrometry （BIXS）, has been developed recently. In the present study a V-4Cr-4Ti alloy was pre-heated at 1000℃ for 2 h to form a recrystallization structure before the tritium absorption experiments were conducted. Firstly the hydrogen isotope gas was charazterized by means of a quadrupole mass spectrometer （QMS） and a small-sized ionization chamber. Then hydrogen isotope absorption tests of V-4Cr-4Ti alloy were performed at 400 ℃ and the atomic concentration of hydrogen isotope in V-4Cr-4Ti alloy was estimated as 0.17% with a tritium content of approximately 2.5 ppm. Experimental results indicate that BIXS is a quite useful tool for quantitatively measuring the tritium content and tritium distribution in the surface layers of vanadium alloys and no strong trapping effects of tritium exist in the pre-heated V-4Cr-4Ti alloy.     

重庆温泉寺及其寺庙园林史略

本文以重庆温泉寺庙园林为例,说明现在重庆园林布局仍以寺庙建筑为中心,组成严整的东西对称格局,其建造充分体现了“天人合一”的思想境界和“道”的自然无为的原则。     

The oxidation of two ternary Ni-Cu-10 at.% Al alloys in 1 atm of pure O2 at 800-900 °C

The oxidation of the ternary alloys Ni-45Cu-10Al and Ni-30Cu-10Al has been studied at 800-900 °C under 1 atm O₂. The presence of 10 at.% Al reduces significantly the oxidation rate of the corresponding Cu-Ni alloys during the initial oxidation stages, even before the establishment of a complete Al₂O₃ layer. The weight of individual sample of the two ternary Ni-Cu-10Al alloys at 800 °C increases more rapidly than at 900 °C during the initial oxidation stage. As oxidation proceeds, the weight gain at 800 °C slows down to a degree that the total weight gain after 24 h oxidation at 800 °C is less than that at 900 °C. Due to a faster formation of the Al₂O₃ layer, which suppresses earlier the further oxidation of Cu and Ni, the external region of the scales grown on Ni-45Cu-10Al contain much less Cu and Ni oxides than those grown on Ni-30Cu-10Al. The transition from the internal oxidation to the selective external oxidation of the most reactive component Al in Ni-Cu-Al alloys is favored by higher values of the Al content, of temperature and of the Cu/Ni ratio.     

氢化物发生原子吸收光谱法测定金属锌中的痕量汞

采用氢化物发生原子吸收光谱法测定金属锌中的痕量汞，研究了金属锌消解的最佳条件，本法简便、快速、重现性好，准确度高，灵敏度为0．73μg/L，检测限为0．22μg/L，相对标准偏差为3．1％，回收率为96％-102％。     

双功能加氢精制催化剂在焦化富气制氢中的应用

介绍了JT-1G／JT-4加氢精制催化剂的烯烃饱和功能和有机硫转化功能；阐述了该催化剂在中石油辽河石化分公司、浙江工程设计院共同开发的用于焦化富气制氢原料的烯烃饱和及有机硫转化的新加氢工艺——逆流-等温-绝热加氢精制工艺中的使用情况。原料中体积分数13％～16％的烯烃经过加氢精制后降至0；原料中有机硫得到充分转化；焦化富气经过加氢精制后，满足了作为制氢原料的要求，降低了制氢成本。     

M－Z型铌酸锂高速调制器

报道了采用行波电极结构的偏振型和与偏振无关型Ｔｉ：ＬｉＮｂＯ３高速强度调制器，其中与偏振无关的高速强度调制器是首次研制成功。     

筛查基因突变的新技术——循环双脱氧指纹图谱法及其应用

建立了适用于大批量标本基因突变筛查的双脱氧指纹图谱法即ｄｄＦ。该技术民测定ＤＮＡ序列的双脱氧末端终止法及ＳＳＣＰ二者长处于一身，即只作一个双脱氧末端终止反应，然后将反应产物在与ＳＳＣＰ相同的电泳条件下进行聚丙烯酰胺凝胶电泳，这样有突变的样品不会漏检，阳性检出率高达１００％。     

掺富勒烯SiO2气凝胶的制备与发光性质研究

本文利用溶胶－凝胶工艺成功地将富勒烯掺入了ＳｉＯ２气凝胶的纳米孔洞中，在Ａｒ＾＋离子激光激发下，观察到了很强的可见光发射，对该现象作了初步的解释。     

3％克百威颗粒剂生产工艺技术的改进

论述了以国产克百威代替进口７５％呋喃丹母粉加工３％颗粒剂的技术改进；并通过产品质量、药效、毒理、残留、环保诸方面的对比，证明改进后的工艺技术是成功的，具有独创性，为以产顶进，节汇创汇，闯出了一条新路子。     

The effect of insulin-like growth factor-1 on cyclic change of tendon cell

BACKGROUND: Myoclonus is a possible side effect of opioid therapy, and have been described following systemic as well as spinal application. CASE REPORT: We report the case of a patient with metastatic carcinoma of the rectum who developed myoclonus following administration of high-dose epidural combined with iv morphine. This complication occurred with maximum daily doses of 300 mg epidurally and 80 mg intravenously and disappeared completely after dose reduction. Treatment trials are presented, the pathophysiology of the myoclonus is discussed. CONCLUSION: For treatment of opioid-induced myoclonus a dose reduction or a change of the opioid should be considered as well as symptomatic treatment with benzodiazepines or baclofen.