纺织机械零件CAPP技术的应用研究

要提高产品的竞争能力，必须在企业中加大CAPP的应用力度，笔者通过应用思普CAPP系统（SIPM/CAPP）编制纺织机械零件工艺文件的实践，证明了在企业中应用CAPP是提高产品的市场竞争能力，提高企业工艺快速反应能力的有力工具。     

大型压力容器现场热处理技术

以大连石化350万t/a催化裂化装置再生器为例,研究开发大型炼油化工设备现场新型热处理工艺。通过设置必要的热气流导向装置,采用微正压内燃工艺,配备新型大功率燃油喷嘴、用DCS集散控制系统调节油风比例和烟囱热量排放张合度,对超厚壁板适当增加电加热辅助热处理,解决了大容积、变截面、不等壁厚、超重设备施工现场热处理温度调整难度大、不均衡等技术问题。实践证明,应用该技术进行热处理,具有工期短、效果好、经济效益明显等特点。     

锰锌铁氧体纳米粉体的液相制备及磁性能

以δ-FeOOH为前驱体,用氨水调节溶液的pH值,分别采用(1)90℃水浴加热动态转化、(2)沸腾回流动态转化,(3)90℃静态转化及(4)200℃水热法四种方法合成了锰锌铁氧体纳米粉体.采用X射线衍射仪(XRD),透射电子显微镜(TEM)、振动样品磁强计(VSM)和X射线荧光光谱仪(XRF)等方法对粉体进行了表征,对四种液相法制备的锰锌铁氧体纳米粉体的结构和性能等进行了对比和分析.结果表明,四种方法中沸腾回流相转化法得到的产物具有磁性能较好、形状较规则、粒径可控等优点.     

Novel blood-compatible waterborne polyurethane using chitosan as an extender

A series of novel block polymers of polyurethane (PU) and chitosan have been prepared in two steps. The first step is the preparation of PU prepolymer, obtained from polytetramethylene oxide glycol (PTMO, M_n = 1000), isophrone diisocyanate (IPDI), and 2,2′-dimethylol propionic acid (DMPA), followed by ionizing PU prepolymer with triethylamine (TEA). The second step involves PU chain-extended by water-soluble chitosan of low molecular weight (M_n = 5000) by self-emulsion polymerization method. The sizes of the latex particles, morphology, and copolymer architecture have been characterized by dynamic light scattering (DLS), general tensile test, infrared spectroscopy (IR), surface contact angle measurement, and transmission electron microscopy (TEM). Furthermore, it shows that the addition of chitosan remarkably increases anticoagulative property of PU elastomers confirmed by the recalcification time. © 2008 Wiley Periodicals, Inc. J Appl Polym Sci, 2008     

A disposable sensor based on immobilization of acetylcholinesterase to multiwall carbon nanotube modified screen-printed electrode for determination of carbaryl

A simple method has been devised for immobilization of acetylcholinesterase (AChE) covalent bonding to a multiwall carbon nanotube (MWNT)-cross-linked cellulose acetate composite on a screen-printed carbon electrode (SPCE) and a sensitive and disposable amperometric sensor for rapid determination of carbaryl pesticide is proposed. The immobilized enzyme was preserved on this film because of the excellent biocompatibility and non-toxicity of cellulose acetate. Based on the inherent conductive properties of the MWNT, the immobilized AChE had greater affinity for ATCl and excellent catalytic effect in the hydrolysis of ATCl. MWNT improved the interface enzymatic hydrolysis reaction and increased the amperometric response of the sensor. Under optimum conditions, the inhibition of carbaryl on AChE increased linearly with the increasing concentration of carbaryl in two ranges, from 0.01 to 0.5 μg mL⁻¹ and from 2 to 20 μg mL⁻¹, with the correlation coefficients of 0.9985 and 0.9977, respectively. The detection limit was 0.004 μg mL⁻¹ taken as the concentration equivalent to 10% decrease in signal. The sensor showed acceptable stability, accuracy and could be fabricated in batches, thus it is economic and portable. This type of disposable enzyme-based amperometric sensor has extensive application potential in environmental monitoring of pesticides.     

国产新型铜带冷轧机

铜带冷轧机是铜带材生产的关键设备。20多年来，通过铜带冷轧机研制开发领域的广大科技人员的共同努力，国产铜带冷轧机获得了长足的发展。本文重点介绍几种主要机型，并分析其优缺点，同时指出今后国产铜带冷轧机的发展方向。     

原料磨同步机励磁装置的改造

分析原料磨同步机所使用的KGLF型励磁装置在实际运行中存在的问题，介绍采用LZK-3型微机励磁装置的改造实践。     

武钢钢铁产品创新的战略思考

产品创新是企业生存和发展的基础。分析了武钢钢铁产品的市场需求，找出了武钢企业外部环境的机会与威胁和企业内部的优势与劣势，提出了产品创新的战略措施。     

一个通用代理计费系统开发框架的设计与实现

用户在不同的网络环境中选择不同的代理软件实现上网和用户管理，这些代理软件既有共性又各具特色，为减少开发不同代理计费软件的工作量，提高开发效率，加快开发周期，提出利用软件重用的思想，将代理软件的差异集中到少数几个类的实现上，设计并实现一个通用代理计费系统开发框架，基于此框架利用相对简单的步骤开发了基于SQUID的代理计费系统，验证了框架的实用性和可行性，达到了设计目标。     

聚丙烯酸酯防水乳液的研究进展

综述了聚丙烯酸酯防水乳液的理论研究进展，重点评述了组合功能单体、优选乳化体系和进行粒子设计三方面的改性手段。