Simple Preparation of Crystal Co3（BTC）2·12H2O and Its Catalytic Activity in CO Oxidation Reaction

Crystalline metal-organic framework cobalt(Ⅱ) benzenetricarboxylate Co3(BTC)2?12H2O(MOF-Co) has been prepared using solvothermal method. The reaction of cobalt(Ⅱ) nitrate and 1,3,5-benzenetricarboxylic(BTC) acid in a mixed solution of N,N-dimethylformamide(DMF)/C2H5OH/H2O(1:1:1, ν/ν) at low temperature for short reaction times produced this crystalline compound. Compared with traditional hydrothermal method, a mixed solution method for the synthesis of crystalline metal complex was found to be highly efficient. After water molecules were removed from this metal complex, its exposed nodes served as active sites. When this MOF-Co was employed in the oxidation of CO, it showed good catalytic properties causing 100% conversion of CO to CO2 at low temperature of 160 ℃.     

论我国高职院校如何破解毕业生就业结构性矛盾

高等职业教育作为我国高等教育的重要组成部分,在现阶段经济社会发展中发挥越来越重要的作用。通过分析高职院校自身教学特点,提出教学体系构建和教改内容应加强与劳动力市场需求相对接,探讨破解毕业生就业结构性矛盾的措施,力求为社会培养高素质的技术技能型毕业生。     

Influence of static pre-loading on the dynamic bending strength of concrete with particle element modeling

Experimental tests show that static pre-loading has a significant effect on the dynamic strength of concrete.Based on meso-scale particle element model,numerical simulations of dynamic bending tests with pre-loading are performed.Complete stress–strain relationships are then obtained.Significant increase in dynamic strength is found when the pre-loadings are imposed within the elastic limit of concrete.However,when the imposition of pre-loadings reaches the plastic or softening range,dynamic strengths may gradually decrease along with the increase in pre-loadings.The distribution of energy components and the failure modes are discussed to explain the mechanisms of the phenomena.     

微创业:大学生创业实践教育的思考

大学生创业实践是高校创业教育的一个难题。当前国内高校创业教育普遍存在实践教育环节薄弱、效果不显著等问题,本研究同步社会经济发展,尝试以微创业视角思考高校创业实践教育,通过梳理微创业的概念及应用,从契合大学生需求角度分析微创业具有的时代性、低门槛、大众化、创新性等特点。并根据高校实际情况,从完善微创业环境、开设微创业课程、建立微创业实践基地、提供微创业网络平台服务等方面提出推动高校大学生微创业的路径建议。     

应用型本科数学类专业职业技能培养研究

构建应用型本科数学类专业职业技能课程体系,强化职业资格认证,提高数学类专业学生就业能力,拓展数学类专业就业领域.     

读者决策采购（PDA）成功实施的关键性因素分析

读者决策采购作为一种全新的基于读者需求的资源建设模式,目前国内还没有高校图书馆实施。介绍了读者决策采购面临的问题,提出PDA要在我国高校图书馆成功实施,需制定严格的标准、选择合适书商并及时进行跟踪与评价。     

Large magnetic-field-induced strains in rare earth polycrystalline Ni-Mn-Ga

The magnetic-field-induced strains (MFIS) of polycrystalline Ni50Mn29Ga21 alloys containing Tb were studied. A large MFIS of-1.10% was obtained under compressive prestress conditions. The addition of Tb can fine the crystal grains, enhance the bending strength obviously, and make MFIS increase further, indicating that a moderate amount of Tb does not hinder twin boundary motion and it conversely makes the material more practical.     

氩弧焊未熔合缺陷的定位分析

氩弧焊在压力容器制造行业运用越来越广泛.正确检出氩弧焊焊接缺陷的位置,不仅能保证设备的安全运行,而且可以节约人力、材料、能源和缩短工期.当采用射线方法检测氩弧焊焊缝质量时,可通过X光底片判断缺陷的埋藏深度.……     

AN APPROACH TO THE ACTIVATION PROCESS OF LaNi_5

本文研究了LaNi_5在不同温度和压力下的活化过程。结果表明,LaNi_5的活化可分为三个阶段,即孕育期;吸氢速度随时间增加而增加的第一阶段和吸氢速度随时间增加而减少的第二阶段。讨论了每一阶段的特征,并给出了吸氢速度的近似表达式。     

机械零件刚度的模糊可靠性设计

介绍了机械零件刚度模糊可靠性设计变形分布参数和刚度隶属函数的确定,导出了零件刚度模糊可靠度的计算公式,并通过机床主轴模糊可靠性设计实例说明机械零件模糊可靠性的计算方法.