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141.
Summary Novel hyperbranched copolymers were successfully synthesized by the controlled charge transfer complex inimer and living radical copolymerization of p-(chloromethyl)styrene (PCMS) and acrylonitrile (AN). The resulting copolymers were characterized by SEC, NMR, FTIR, DSC and elemental analysis etc.. The influences of reaction conditions, such as the polymerization temperature, the catalyst (CuBr) concentration and the monomer ratio, on the resulting copolymers were investigated in detail. The monomer reactivity ratios were evaluated to be rPCMS=0.937 and rAN=0.088 respectively by the Fineman-Ross method. The higher are the polymerization temperature and the ratio of catalyst to monomer, the higher is the branching degree of the resulting copolymer. When the amount of monomer AN was used in excess than that of the monomer PCMS in the raw feed, the hyperbranched predominantly alternating copolymers HP[PCMS-co-AN] could be obtained. These hyperbranched copolymers were successfully used as functional macroinitiators to synthesize the star-shaped poly(PCMS-co-AN)/poly(MMA) block copolymers. 相似文献
142.
Plastic deformation and fracture of binary TiAl-base alloys 总被引:4,自引:0,他引:4
The mechanical behavior of binary TiAl alloys containing 46 to 60 at. pct Al has been studied in bulk materials preparedvia rapid solidification processing. Bending and tensile tests were carried out at room temperature as a function of Al concentration.
A few alloys were also tested from liquid nitrogen temperature to ∼ 1000°C. Deformation substructures were studied by analytical
transmission electron microscopy and fracture modes by scanning electron microscopy (SEM). It was found that both microstructure
and composition strongly affect the mechanical behavior of TiAl-base alloys. A duplex structure, which contains both primary
y grains and transformedγ/α
2 lamellar grains, is more deformable than a single-phase or a fully transformed structure. The highest plasticities are observed
in duplex alloys containing 48–50 at. pct Al after heat treatment in the center of theγ + α phase field. The deformation of these duplex alloys is facilitated by 1/2[110] slip and {111} twinning, but very limited
superdislocation slip occurs. The twin deformation is suggested to result from a lowered stacking fault energy due to oxygen
depletion or an intrinsic change in chemical bonding. Other factors, such as grain size and grain boundary chemistry and structure,
are important from a fracture point of view. The results on the deformation and fracture modes as a function of test temperature
are also discussed. 相似文献
143.
Yi‐Hung Chen Ching‐Yuan Chang Wei‐Ling Su Chun‐Yu Chiu Yue‐Hwa Yu Pen‐Chi Chiang Chiung‐Fen Chang Je‐Lueng Shie Chyow‐San Chiou Sally IM Chiang 《Journal of chemical technology and biotechnology (Oxford, Oxfordshire : 1986)》2005,80(1):68-75
This study investigates the ozonation of CI Reactive Black 5 (RB5) by using the rotating packed bed (RPB) and completely stirred tank reactor (CSTR) as ozone contactors. The RPB, which provides high gravitational force by adjusting the rotational speed, was employed as a novel ozone contactor. The same ozone dosage was separately introduced into either the RPB or the CSTR for the investigation, while the experimental solution was continuously circulated within the apparatus consisting of the RPB and CSTR. The decolorization and mineralization efficiencies of RB5 in the course of ozonation are compared for these two methods. Moreover, the dissolved and off‐gas ozone concentrations were simultaneously monitored for the further analysis. As a result, the ozone mass transfer rate per unit volume of the RPB was significantly higher because of its higher mass transfer coefficient and gas–liquid concentration driving force. Furthermore, ozonation kinetics was found to be independent of the gravitational magnitude of an ozone gas–liquid contactor. Therefore, the results suggest employing RPBs as ozone‐contacting devices with the advantage of volume reduction. The experimental results, which can be used for further modeling of the ozonation process in the RPB, also show the requirement of correct design for the RPB. Consequently, the present study is useful for the understanding of practical application of RPBs. Copyright © 2004 Society of Chemical Industry 相似文献
144.
本文提出了一种针对木马的静态信息进行分析的新的检测机制,建立了基于BP神经网络的数据处理模型。PE文件是Windows平台下的可执行文件,也是木马等后门程序的主要载体, 由于PE文件的结构复杂、灵活,而BP神经网络摸型的自身要求,导致数据的建摸过程遇到两个难点,本文首先引入了变化粒度的概念,解决了输入端非线性数据的问题。同时,也解决了将PE文件中大量的字符串归一化(0,1)区间)的问题,最终建立了一套较为理想的解决方案,取得了较为理想的测试数据。 相似文献
145.
We report a case of pulmonary carcinosarcoma. Surgery is required for this rare mixed type, biphasic tumor. It is generally considered to be a malignant formation issuing from a single cell line but with a two-way differentiation into epithelial and conjunctive components. There is a differentiation continuum between spindle-cell carcinomas (also called monophasic sarcomatoid carcinoma) and carcinosarcoma (or biphasic sarcomatoid carcinoma) leading to debate concerning the immunohistochemical and ultrastructural features. 相似文献
146.
147.
用宏观断口分析、化学检验、力学性能测定、低倍检查、金相组织及夹杂物评定鉴别、受力分析及强度寿命定量估算的方法,对人字轮被动齿轴端断裂失效原因进行分析,并提出改进措施。 相似文献
148.
PMMA/PBA乳胶IPN阻尼材料的研究 总被引:3,自引:0,他引:3
用乳液聚合方法合成了一系列的互穿聚合物网络,其中包括:PMMA/PBA和P(MMA-co-PMA)/PBA乳胶互穿聚合物网络(LIPN),PMMA/PBA乳胶双向互穿聚合物网络(LBIPN)以及PMMA/PBA界面交联互穿聚合物网络(ICLIPN)。动态力学谱和拉伸试验结果表明:(1)PMMA/PBA互穿聚合物网络的两组分相容性和阻尼性能可通过MMA和PMA共聚来改善;(2)双向互穿技术是一种行之 相似文献
149.
Huai Wen-xin Wuhan University of Hydraulic & Electric Engineering Wuhan Hubei P.R.China Prof.Li Wei 《水动力学研究与进展(B辑)》1993,(3)
Turbulence represents an essential aspect in atmospheric and oceanic circulations.In particu-lar,it is a preponderant factor in the dispersion of pollutants of artificial or natural origin.Thevertical turbulent jets,plumes and buoyant jets discharging into static environment is one of themost important and basic flow patterns related with the environment pollution.These flows havenumerous important applications,for example,thrust augmentors,waste disposal plumes fromstacks and combustion systems,and significant problems of turbulent diffusion. 相似文献
150.
Sianchang Huang Likarn Wang 《Lightwave Technology, Journal of》1996,14(5):661-664
The power penalty induced by imperfect phase recovery in PSK homodyne communication systems with balanced phase-locked loop receivers are exactly evaluated. Optimum phase deviations between the mark-state and the space-state bits are used in this study. This study for the first time shows the imperfect-phase-recovery-induced power penalty as a function of laser linewidth with optimum phase deviations considered. It can be estimated from the theoretical result that an optimal balanced PLL receiver requires the laser linewidth as Δν⩽1.15×10-6× (bit rate) in contrast to the previous reported one Δν⩽5.88×10-6× (bit rate). We also point out here that the previously reported laser linewidth requirement was wrongly estimated 相似文献