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171.
Mamiko Hori Cécile Pagnoux Jean-François Baumard Masayuki Nogami 《Journal of Materials Science》2007,42(1):80-86
A new method is proposed to produce gold nanoparticles (GNP) by in situ reduction of a gold salt dissolved in water. The reducing
agent used is Tiron instead of the citrate anion most often mentioned in literature. The influence of various parameters has
been investigated, such as the content of Tiron with respect to that of the precursor of gold HAuCl4, or the initial pH of the solution after mixing of reactants. It is shown that Tiron also exerts a positive influence as
a dispersant, which impedes agglomeration of gold nanoparticles. The typical average size of GNP synthesized in the present
work is close to 7 nm. 相似文献
172.
173.
M. K. Bakhadyrkhanov O. É. Sattarov Kh. M. Iliev K. S. Ayupov Tuérdi Umaier 《Semiconductors》2005,39(7):789-791
It is experimentally ascertained that light stimulates the negative magnetoresistance observed in a high electric field in silicon doped with boron and manganese. The optimum conditions (the electric field, temperature, illumination, and resistivity of the material) for observation of the largest magnitude of negative magnetoresistance in (Si:B):Mn are determined. The dependence of the negative magnetoresistance on the concentration of compensating impurity is established. 相似文献
174.
Effect of boron on the low-cycle fatigue behavior and deformation structure of INCONEL 718 at 650 °C
L. Xiao M. C. Chaturvedi D. L. Chen 《Metallurgical and Materials Transactions A》2004,35(11):3477-3487
Symmetrical push-pull low-cycle fatigue (LCF) tests were performed on INCONEL 718 (IN718) containing 12, 29, 60, and 100 ppm
B at 650 °C. The results showed that all the alloys experienced a relatively short period of initial cyclic hardening at low
strain amplitudes, followed by a regime of saturation or slightly continuous cyclic softening. The initial cyclic hardening
phase decreased with increasing strain amplitudes, and disappeared at the high strain amplitudes. A serrated flow was observed
in the plastic regions of cyclic stress-strain hysteresis loops. The saturated cyclic stress amplitude at a given strain amplitude
was highest for the alloy with 60 ppm B, and lowest for the alloy with 12 ppm B. The LCF lifetime increased with increasing
B concentration up to 60 ppm, and then decreased as the B content increased from 60 to 100 ppm. Fractographic analysis suggested
that the fracture mode changed from intergranular to transgranular cracking as the B concentration increased. The characteristic
deformation microstructures produced by LCF tests at 650 °C, examined via transmission electron microscopy, were regularly spaced arrays of planar deformation bands on {111} slip planes in all four
alloys. A ladderlike structure was observed in some local regions in the alloy with 12 ppm B. Heavily deformed planar deformation
bands were observed in the fatigued specimens with 100 ppm B. The mechanism of improvement in the LCF life of IN718 due to
B addition is discussed. 相似文献
175.
The stress intensity factors for a short crack partially penetrating an inclusion of arbitrary shape
Some approximate solutions for predicting the stress intensity factor of a short crack penetrating an inclusion of arbitrary
shape have been developed under mode I and mode II loading conditions. The derivation of the fundamental formula is based
on the transformation toughening theory. The transformation strains in the inclusion are induced by the crack-tip field and
remotely applied stresses, and approximately evaluated by the Eshelby equivalent inclusion theory. As validated by detailed
finite element (FE) analyses, the developed solutions have good accuracy for different inclusion shape and for a wide range
of modulus ratio between inclusion and matrix material. 相似文献
176.
An overview of nondestructive evaluation methods 总被引:1,自引:0,他引:1
Marvin Trimm 《Journal of Failure Analysis and Prevention》2003,3(3):17-31
ondestructive evaluation is described as nondestructive testing (NDT), nondestructive inspection (NDI), and nondestructive
examination (NDE). The activities associated with the evaluation include testing, inspection, and examination and primarily
involve looking at (or through) and/or measuring some characteristic of an object. Frequently there is a desire to determine
some characteristic of the object or to determine whether the object contains irregularities, discontinuities, or flaws. These
examinations, inspections, or tests are used to determine the physical soundness of a material without impairing its usefulness.
Nondestructive evaluation is a powerful tool that can help assure safety, quality, and reliability; increase productivity;
decrease liability; protect the environment; and save money. In this article, nondestructive evaluation is represented by
the acronym NDE. 相似文献
177.
Nguyen An Tien I. Ya. Mittova O. V. Almjasheva S. A. Kirillova V. V. Gusarov 《Glass Physics and Chemistry》2008,34(6):756-761
Nanocrystalline LaFeO3 is prepared by the dehydration of coprecipitated lanthanum and iron(III) hydroxides. It is shown that the behavior of the samples during heating and the size distribution of LaFeO3 nanocrystals can be considerably different depending on the scheme used for coprecipitation of lanthanum and iron hydroxides; independently of the method employed for coprecipitation of the initial compounds, sintering of the samples at 950°C leads to the formation of lanthanum orthoferrite crystals up to 100 nm in size. 相似文献
178.
Vjacheslav V. Zuev 《Journal of Polymer Research》2008,15(5):351-356
Functionalized polyanilines containing biphenyl, terphenyl, carbazole, anthracene, and 4-n-hexylphenyl moieties were synthesized though the reaction of polyaniline in emeraldine base form with sodium salt of corresponding
vinylketoaromatics with quantitative yields. Polymers were characterized with Fourier transform infrared spectroscopy, proton
nuclear magnetic resonance spectroscopy, and thermogravimetry. The emission characteristics of these polymers in N-methyl-2-pyrrolidone solution were examined. The functionalized polyanilines exhibited an intense green emission. 相似文献
179.
We propose two new antidiffusive schemes for advection (or linear transport), one of them being a mixture of Roe’s Super-Bee
scheme and of the “Ultra-Bee” scheme. We show how to apply these schemes to treat time-dependent first order Hamilton–Jacobi–Bellman
equations with discontinuous initial data, possibly infinitely-valued. Numerical tests are proposed, in one and two space
dimensions, in order to validate the methods
AMS subject classifications. Primary 65M12, Secondary 58J47 相似文献
180.