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11.
纳米β-NiOOH的固相合成及其性能 总被引:14,自引:1,他引:13
首次利用固相氧化法制备了 β NiOOH纳米粉体样品 ,经X射线衍射和透射电镜测试结果表明所得样品 β NiOOH粒子呈球形 ,粒径大小在 2 0~ 40nm之间。热重与差热分析结果表明当温度超过 10 0℃ ,样品开始不可逆地分解为NiO。运用恒流充放电、循环伏安以及Tafel极化等电化学测试对样品的电化学性能进行了初步研究。结果表明 :β NiOOH的交换电流密度高于 β Ni(OH) 2 的交换电流密度约一个数量级 ,具有较好的电极可逆性、较高的质量比容量以及优良的容量保持率 ,适于作为Zn/NiOOH类型镍电池的正极活性材料 相似文献
12.
电站锅炉制粉系统的爆炸原因与防范对策 总被引:1,自引:0,他引:1
火力发电厂制粉系统爆炸事故时有发生 ,重大设备损坏 ,造成了严重的经济损失。本文通过分析研究 ,找出制粉系统爆炸的原因 ,从措施上、煤的质量控制上及制粉系统结构改造上提出了防范的对策。 相似文献
13.
A novel ultra-wideband (UWB) bandpass filter (BPF) is presented using the hybrid microstrip and coplanar waveguide (CPW) structure. A CPW nonuniform resonator or multiple-mode resonator (MMR) is constructed to produce its first three resonant modes occurring around the lower end, center, and higher end of the UWB band. Then, a microstrip/CPW surface-to-surface coupled line is formed and modeled to allocate the enhanced coupling peak around the center of this UWB band, i.e., 6.85GHz. As such, a five-pole UWB BPF is built up and realized with the passband covering the entire UWB band (3.1-10.6GHz). A predicted frequency response is finally verified by the experiment. In addition, the designed UWB filter, with a single resonator, only occupies one full-wavelength in length or 16.9mm. 相似文献
14.
Xue‐Bing Zhao Lei Wang De‐Hua Liu 《Journal of chemical technology and biotechnology (Oxford, Oxfordshire : 1986)》2008,83(6):950-956
Previous work has shown that the enzymatic hydrolysis of sugarcane bagasse could be greatly enhanced by peracetic acid (PAA) pretreatment. There are several factors affecting the enzymatic digestibility of the biomass, including lignin and hemicelluloses content, cellulose crystallinity, acetyl group content, accessible surface area and so on. The objective of this work is to analyze the mechanism of the enhancement of enzymatic digestibility caused by PAA pretreatment. Delignification resulted in an increase of the surface area and reduction of the irreversible absorption of cellulase, which helped to increase the enzymatic digestibility. The Fourier transform infrared (FTIR) spectrum showed that the absorption peaks of aromatic skeletal vibrations were weakened or disappeared after PAA pretreatment. However, the infrared crystallization index (N.O'KI) was increased. X‐ray diffraction (XRD) analysis indicated that the crystallinity of PAA‐treated samples was increased owing to the partial removal of amorphous lignin and hemicelluloses and probable physical change of cellulose. The effect of acetyl group content on enzymatic digestibility is negligible compared with the degree of delignification and crystallinity. The results indicate that enhancement of enzymatic digestibility of sugarcane bagasse by PAA pretreatment is achieved mainly by delignification and an increase in the surface area and exposure of cellulose fibers. Copyright © 2008 Society of Chemical Industry 相似文献
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16.
Young Sil Jeon Jing Lei Ji-Heung Kim 《Journal of Industrial and Engineering Chemistry》2008,14(6):726-731
This study examined the removal of some basic dyes, such as Methylene Blue, Malachite Green and Methyl Orange, using alginate or alginate/polyaspartate composite gel beads. The adsorption of dyes from aqueous solutions at 25 °C was examined using a batch sorption technique. The effects of CaCl2 and the dye concentration on the adsorption were examined. Type-S adsorption isotherms were obtained, which is characteristic of a weak solute–solid interaction. The ionic interaction between the dye molecule and gel matrix appears to be responsible for the efficient adsorption of cationic dyes in this system. These results suggest that an alginate/polyaspartate gel can be used as an effective sorbent for water pollutants such as dyes, and the immobilization of these organic contaminants in the hydrogels from wastewater can solve one of the most important environmental problems in the related industry. 相似文献
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18.
Lei Liu Ying Kong Hong Xu Jin P. Li Jin X. Dong Zhi Lin 《Microporous and mesoporous materials》2008,115(3):624-628
A three-dimensional zinc phosphate compound with DFT topology, designated as ZnPO4-EU1, has been synthesized by an ionothermal approach from the system HF-ZnO–P2O5-choline chloride-imidazolidone. Ethylenediamine, derived from decomposition of the imidazolidone component of the deep-eutectic solvent (DES) itself, is delivered to the synthesis and serves as an appropriate template for ZnPO4-EU1. Experiments in which the synthesis conditions were varied showed that ZnPO4-EU1 may be prepared over a wide molar ratio of P/Zn = 0.55–13.0. Powder X-ray diffraction patterns have been obtained at intervals to track the crystallization process of this material. The experimental data show that Zn3(PO4)2 · 4H2O (a dense phase) was first isolated from the DES after reaction for 1 h. Subsequently, the pure phase of ZnPO4-EU1 was obtained with increasing crystallization time from 12 h to 72 h. The experimental results show that the nucleation and crystallization take place with relatively low levels of solvent degradation, demonstrating that zinc phosphate with a three-dimensional framework can be synthesized by in situ generation of an appropriate template using an unstable DES at high temperatures (150–200 °C). 相似文献
19.
A high-power and high-repetition-rate passively Q -switched ytterbium-doped single-mode double-clad fiber laser was built using a Cr4+:YAG saturable absorber (SA). Two different SAs with initial transmissions of Tomicron = 30% and Tomicron = 50% were studied. At the maximum coupled pump power of 9.8 W, an output power of 4.7 W, pulse duration of 143 ns, pulse repetition rate of 253 KHz, pulse energy of 18.5 muJ, and slope efficiency of 49% were obtained with the Tomicron = 30% SA. 相似文献
20.
Alia-Klein Nelly; Goldstein Rita Z.; Tomasi Dardo; Zhang Lei; Fagin-Jones Stephanie; Telang Frank; Wang Gene-Jack; Fowler Joanna S.; Volkow Nora D. 《Canadian Metallurgical Quarterly》2007,7(4):735
Reports an error in "What is in a word? No versus Yes differentially engage the lateral orbitofrontal cortex" by Nelly Alia-Klein, Rita Z. Goldstein, Dardo Tomasi, Lei Zhang, Stephanie Fagin-Jones, Frank Telang, Gene-Jack Wang, Joanna S. Fowler and Nora D. Volkow (Emotion, 2007[Aug], Vol 7[3], 649-659). The supplemental materials link should appear as follows: http://dx.doi.org/10.1037/1528-3542.7.3.649.supp. (The following abstract of the original article appeared in record 2007-11660-018.) The words "No" and "Yes" are involved in conditioning to prohibit or encourage behavior, respectively. The authors, therefore, hypothesized that these words would be attributed to endogenous valence, activating neuronal circuits involved with valence and emotional control. Functional MRI (fMRI) at 4 Tesla was used to record regional brain activity while participants were exposed to emphatic vocalizations of the words. Results showed that No and Yes were associated with opposite brain-behavior responses; while No was negatively valenced, produced slower response times, and evoked a negative signal in the right lateral orbitofrontal cortex (OFC), Yes was positively valenced, produced faster response times, and evoked a positive signal in a contiguous region of the OFC. Attribution of negative valence to No and trait anger control were associated with increased responsivity of the OFC to No. Inasmuch as sensitivity to the prohibitive command No develops during childhood through interaction with primary caregivers as the first social objects, our findings may implicate the lateral OFC in the neurobiology of emotion regulation and subsequent social development. (PsycINFO Database Record (c) 2010 APA, all rights reserved) 相似文献