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971.
Z. J. Yang E. Harkin‐Jones G. H. Menary C. G. Armstrong 《Polymer Engineering and Science》2004,44(7):1379-1390
A non‐isothermal finite element (FE) model for the injection stretch‐blow molding (ISBM) process of polyethylene terephthalate (PET) bottles is presented in this paper. The constitutive behavior of PET is modeled by the physically based Buckley glass‐rubber model in form of UMAT in ABAQUS. The heat transfer between the stretch rod, the preform, and the mold is modeled. Particular attention is paid to thermal and contact modeling, material model, and selection of proper element types. Extensive FE simulations are carried out to model ISBM of a 20 g‐330 ml bottle made in plant tests. Comparisons of numerical results with the measurements demonstrate that the model can satisfactorily predict the bottle thickness and material distributions. Significant nonlinear differentials are found in strain, temperature, and temperature reduction rate in both bottle thickness and length direction during the process. A volume approach is therefore necessary for accurate predictions of final bottle properties because they are governed by orientation and crystallinity, which are highly temperature and strain dependent. Parametric studies on contact modeling and heat transfer coefficient are also conducted and the results are discussed. Polym. Eng. Sci. 44:1379–1390, 2004. © 2004 Society of Plastics Engineers. 相似文献
972.
A simple strategy was developed based on a new reactive function‐ and a salt‐containing new monomer, 4‐vinylbenzyl dimethyl 2‐(dimethylphosphino)ethyl phosphonium chloride (VDEPC), to obtain stable humidity‐sensitive membranes. The major ingredient of a humid membrane is crosslinked polyelectrolytes obtained from copolymers of VDEPC/2‐ethylhexyl acrylate (2‐EHA) = 1/0, 4/1, and 2/1. Isothermal humidity absorption experiments were performed for the estimation of humidity‐sensing materials. The crosslinked copolymers prepared from the reaction of VDEPC/2‐EHA = 4/1 with 1,4‐dichlorobutane showed an average impedance of 595, 39.1, and 3.9 KΩ at 30, 60, and 90% RH, respectively. Their hysteresis, temperature dependence, frequency dependence, and response time were measured. The reliability including water resistance and a long‐term stability were estimated for the application of the common humidity sensor. © 2003 Wiley Periodicals, Inc. J Appl Polym Sci 89: 1062–1070, 2003 相似文献
973.
Shrikrishina D. Sartale Huang-Wei Shiu Wen-Hua Wen Meng-Fan Luo Y. C. Lin Yao-Jane Hsu 《Catalysis Letters》2007,119(1-2):95-100
Using a scanning-tunneling microscope, reflection high-energy electron diffraction and photoelectron spectra with synchrotron
radiation, we investigated the temperature dependence of the dehydrogenation of cyclohexene (C6H10) adsorbed on Pt nanoclusters supported on an ultra-thin film of Al2O3/NiAl(100). The Pt clusters, grown by vapor deposition, are structurally ordered and exhibit a mean diameter 2.2 nm and height
0.4 nm. The progress of dehydrogenation was monitored through the temporal variation of C 1s photoelectron spectra; analysis
of these features revealed that the dehydrogenation of cyclohexene with increasing sample temperature occurs as a sequential
process beginning around 150 K, a temperature significantly less than that for Pt single-crystal surfaces. The dehydrogenation
behavior, particularly the decomposition into elemental carbon, is found to vary with Pt coverage. 相似文献
974.
Web服务基于标准的数据格式和协议,如XML、SOAP和HTTP,不同平台和操作系统的客户和服务端可以基于同样的协议,没有障碍地通信,Web服务客户端只需标识Web服务的位置及其可以调用的方法,就可以简单地使用Web服务。微软公司的.NET框架针对Web服务提供了广泛的支持。因此研究了.NET环境下Web Services的构建、处理流程,举例说明了Web服务的典型应用。 相似文献
975.
976.
David M. Owen Atul H. Chokshi Steven R. Nutt 《Journal of the American Ceramic Society》1997,80(9):2433-2436
Constant-stress tensile creep experiments on a superplastic 3-mol%-yttria-stabilized tetragonal zirconia composite with 20 wt% alumina revealed that cavities nucleate relatively early during tensile deformation. The number of cavities nucleated increases with increasing imposed stress. The cavities nucleate at triple points associated largely with an alumina grain, and then grow rapidly in a cracklike manner to attain dimensions on the order of the grain facet size. It is suggested that coarser-grained superplastic ceramics exhibit lower ductility due to the ease in formation of such grain boundary facet-cracks and their interlinkage to form a macroscopic crack of critical dimensions. 相似文献
977.
Graft copolymerization of acrylic acid (AA) onto polyphenylene sulfide (PPS) nonwoven initiated by low temperature plasma was studied. The effects of various conditions on graft reaction and the grafting rate were investigated. SEM images showed that PPS nonwoven was grafted, and the graft copolymerization only occurred on the surface of PPS. It may be due to the chain transference going with the graft copolymerization. It was found that with the increasing of plasma power, treatment time, space between electrodes, monomer concentration, and temperature of graft polymerization, the grafting rate increased at first, went to the top, and then decreased. The PPS nonwoven surface graft reaction could be optimized by the following processing conditions: 120 s of plasma treatment time, 50 W of plasma power, 1.5 cm of space between electrodes, 30% (w/w) of monomer concentration, and 50°C of temperature of graft polymerization. Measurement of XPS showed that the peak of C1s of graft polyacrylic acid was existed, and the peak area increased with the increase of the grafting rate. © 2006 Wiley Periodicals, Inc. J Appl Polym Sci 102: 5884–5889, 2006 相似文献
978.
Liquid nitrile rubber, hyperbranched polyester, and core/shell rubber particles of various functionality, namely, vinyl, carboxyl, and epoxy, were added up to 20 wt % to a bisphenol‐A‐based vinylester–urethane hybrid (VEUH) resin to improve its toughness. The toughness was characterized by the fracture toughness (Kc) and energy (Gc) determined on compact tensile (CT) specimens at ambient temperature. Toughness improvement in VEUH was mostly achieved when the modifiers reacted with the secondary hydroxyl groups of the bismethacryloxy vinyl ester resin and with the isocyanate of the polyisocyanate compound, instead of participating in the free‐radical crosslinking via styrene copolymerization. Thus, incorporation of carboxyl‐terminated liquid nitrile rubber (CTBN) yielded the highest toughness upgrade with at least a 20 wt % modifier content. It was, however, accompanied by a reduction in both the stiffness and glass transition temperature (Tg) of the VEUH resin. Albeit functionalized (epoxy and vinyl, respectively) hyperbranched polymers were less efficient toughness modifiers than was CTBN, they showed no adverse effect on the stiffness and Tg. Use of core/shell modifiers did not result in toughness improvement. The above changes in the toughness response were traced to the morphology assessed by dynamic mechanical thermal analysis (DMTA) and fractographic inspection of the fracture surface of broken CT specimens. © 2002 Wiley Periodicals, Inc. J Appl Polym Sci 84: 672–680, 2002; DOI 10.1002/app.10392 相似文献
979.
Song-Ya Ma Ming-Xing Luo Xiu-Bo Chen Yi-Xian Yang 《Quantum Information Processing》2014,13(9):1951-1965
Two schemes via different entangled resources as the quantum channel are proposed to realize remote preparation of an arbitrary four-particle \(\chi \) -state with high success probabilities. To design these protocols, some useful and general measurement bases are constructed, which have no restrictions on the coefficients of the prepared states. It is shown that through a four-particle projective measurement and two-step three-particle projective measurement under the novel sets of mutually orthogonal basis vectors, the original state can be prepared with the probability 50 and 100 %, respectively. And for the first scheme, the special cases of the prepared state that the success probability reaches up to 100 % are discussed by the permutation group. Furthermore, the present schemes are extended to the non-maximally entangled quantum channel, and the classical communication costs are calculated. 相似文献
980.
Chih‐Chen Yih 《Asian journal of control》2014,16(6):1880-1890
Underactuated vehicles are those in which the number of control inputs is less than the degrees of freedom to be controlled. Using actuated wheels, velocity control of the two‐wheeled self‐balancing vehicle drives the vehicle at a desired speed and balances the body of the vehicle. First, we investigate the effects of friction on the wheel and derive the hybrid model of rolling and slipping. Second, we propose a nonlinear sliding mode velocity control scheme for the pure rolling model of the two‐wheeled vehicle. We present the design of the corresponding sliding surfaces and internal dynamics of the two‐wheeled vehicle. Our stability analysis reveals that the proposed sliding mode method can guarantee the asymptotic stability of the error dynamics for velocity control of the underactuated vehicle. Compared to linear optimal control, our numerical simulations demonstrate that the proposed sliding mode schemes can effectively control the velocity under the circumstances of parametric variations, emergency braking, and rapid acceleration in slippery road conditions. The proposed velocity control and the simulation improve our understanding on designing velocity control of the two‐wheeled self‐balancing vehicle. 相似文献