EDTA络合滴定法快速测定碳酸锆中锆铪含量

锆铪氧化物含量的测定通常采用苦杏仁酸[C6H5CH（OH）COOH]重量法。该法经典、准确,但操作烦琐,分析时间长,对日常生产、入库或销售不利。乙二胺四乙酸二钠（EDTA）络合滴定法（容量法）操作简便、快速、准确,适合日常检验。但用基准氧化锌、高纯二氧化锆或氯氧化锆来标定EDTA时,测定结果偏低。采用重量法和容量法相结合,先用重量法测定锆铪氧化物含量,以已知锆铪氧化物含量的碳酸锆作标定物,再标定EDTA标准溶液的滴定度,用此EDTA标准溶液测定相同原料生产的碳酸锆。该法简便、快速、准确,试剂安全性好。     

江苏省地震前方指挥车应急数据信息通信方式的实现

前方指挥车是在有地震灾害事件发生时,能够立即响应,并快速到达地震震中所在地,立即开展现场信息汇集与共享、地震灾情动态评估和修正、辅助决策建议及时生成、现场资源调度和管理,实现前方指挥部与现场工作人员、国家指挥部、区域指挥部的不同应用系统之间的数据信息的共享和传递.本文主要介绍前方指挥车两种不同应急通信方式,并讨论各自的优缺点.     

Synthesis and light‐emitting properties of new poly(p‐phenylenevinylene) derivatives containing oxadiazole moiety

Two new poly(p‐phenylenevinylene) (PPV) derivatives containing oxadiazole moiety (OXA‐PPV1 and OXA‐PPV2) were synthesized by the Wittig condensation polymerization reaction. Their thermal and light‐emitting properties were investigated. The single‐ and triple‐layer electroluminescent (EL) devices with configurations of ITO/polymer/Al and ITO/polymer/OXD‐7/Alq₃/Al were fabricated. They exhibited blue emission at 470 nm for OXA‐PPV1 and green emission at 560 nm for OXA‐PPV2. The turn‐on voltages of triple‐layer device were 11 V for OXA‐PPV1 and 8 V for OXA‐PPV2. The triple‐layer EL devices showed much better performance than did the single‐layer devices. The spectra indicated energy transfer occurred from segments of side chain to polymer backbone. © 2002 Wiley Periodicals, Inc. J Appl Polym Sci 85: 422–428, 2002     

一种基于无约束总变分模型的阴影检测方法

阴影检测是进行阴影处理前的重要步骤,总变分模型可以用于影像阴影检测.通过对总变分模型进行改进,提出了一种基于无约束总变分模型的阴影检测方法.经实验及统计分析证明,在合适的迭代条件下,该方法对于单一阴影影像的处理效果理想.     

一种公交网络最优路径新算法*

从出行者的实际情况出发,提出步行愿望系数,综合考虑最小换乘次数、最短时间以及最小费用等因素,提出了一种公交网络最优路径新算法,应用于广州市大学城内公交线路查询,实现相应的仿真系统。     

改进SSR算法在人脸识别中的应用

为提高人脸检测中人脸验证的速度,在平方积分图像和图像窗口的灰度均值及方差快速计算基础上,对传统的SSR算法中人脸验证算法部分进行了改进。应用改进的算法,结合窗口灰度标准化的计算和平均人脸模板的取得,引入相关系数和平均偏差,加快了求解速度,克服了由于噪声点的存在对真实的候选脸图像漏检的情况。人脸检测实验证明应用改进的模板匹配算法的正确性.     

Establishmen and vertification of an improved similitude law for dynamic ice force model test

To study the similitude laws for dynamic ice force model test which is a hot problem in ice mechanics.In this paper,a new modified similitude law for dynamic ice force model test is proposed based on ice-induced virbration theory and two reasonable assumptions.And the new law is vertified with an ice-induced pier virbration example.The numerical calculation results show that,firstly,the error of frequency factor between test value and theory value is small as well as that of displacement and velocity;Secondly,the time scale completely meet the similitude relation,the waveforms anastomotic well,and the phenomenon of offset and omit do not occur;Thirdly,as the damping ratio between prototype and model is nearly equal,the improved similitude law will still be applied.Therefore,the new modified similitude law is feasible to study dynamic ice force model test and can provide reference for the ice mechanics.     

Matlab中的代数环问题及其消除方法

本文以免疫PID的SimuLink模型及其S函数为例引出代数环问题,分析了代数环的基本概念,指出了代数环对控制系统仿真的巨大危害,最后结合实际提出了几种消除代数环的方法。结果表明,代数环消除后提高了系统的仿真精度和运行速度。     

Molten salts/ceramic-foam matrix composites by melt infiltration method as energy storage material

A new type of high temperature energy storage material was obtained through the melt infiltration method, using compounding SiC ceramic foam as matrix and Na₂SO₄ as phase change material. The resulting composite material was measured by XRD, SEM, TG-DSC methods. The experimental results indicate that the composite is composed of silicon carbide, sodium sulfate and square quartz, and no chemical reactions occurs between Na₂SO₄ and SiC matrix. Na₂SO₄ has a good bonding with the SiC ceramic foam matrix. As the composite material is characterized by high thermal energy storage density and high thermal conductivity, it is suit for energy storage under high temperature. Funded by the “863” Hi-Tech Research and Development Program of China (2008AA05Z418)     

略论“公民意识”、“公民教育”和外语教师的“全球意识”

简要综述了国内外＂公民意识＂和＂公民教育＂的研究现状,认为在全球化背景下,国家＂公民意识＂的培养,也应包括世界公民意识的培养。外语教育是培养学生成为合格的世界公民的一个重要途径;外语教师肩负着培养＂全球公民意识公民＂的特殊使命,理应加强自身的＂公民意识＂培养,努力掌握全球化知识,提升全球化素质。