化学法和机械法从大肠杆菌释放人肿瘤坏死因子

对化学法和机械法破碎基因工程大肠杆菌以释放人肿瘤坏死因子的影响因素作了考察。在化学法破菌中研究了破碎时间、试剂浓度、溶剂ｐＨ值、加入表面活性剂等因素的影响。在机械法破碎中研究了停留时间、装珠量、搅拌转速、细胞浓度等的影响，对操作条件进行了优化。通过对二者的比较，发现机械法破碎细胞效率高，但产生细小的碎片不利后分离；化学法释放产物有选择性，但操作时间长。     

水泥厂风管钢支架设计浅议

对几种形式的风管铜支架进行了受力分析，阐述了各种形式风管支架的优缺点。     

Preparation and Electric Properties of Dense Nanocrystalline Zinc Oxide Ceramics

This communication reports on the preparation and electric properties of dense nanocrystalline ZnO ceramics. By spark plasma sintering, nanocrystalline (∼100 nm) ZnO ceramics with a high density of 98.5% were obtained at a very low temperature of 550°C. Electric property measurement revealed a novel conduction nonlinearity in the sample sintered at 500°C. This phenomenon is due to the nanometerization of ZnO crystal and the grain boundary layer with an amorphous interfacial layer.     

聚乙二醇—三氯化钕配位聚合物的合成和表征

本文以聚乙二醇为配位体，首镒合成了三价稀土金属钕的配位聚合物。实验测定了配位聚合物的红外光谱。     

Crystallization and crosslinking of polyamide‐1010 under elevated pressure

The structure and thermal properties of polyamide‐1010 (PA1010), treated at 250°C for 30 min under pressures of 0.7–2.5 GPa, were studied with wide‐angle X‐ray diffraction (WAXD), infrared (IR), differential scanning calorimetry (DSC), and thermogravimetric analysis (TGA). Crystals were formed when the pressures were less than 1.0 GPa or greater than 1.2 GPa. With increasing pressure, the intensity of the diffraction peak at approximately 24° was enhanced, whereas the peak at approximately 20° was depressed. The triclinic crystal structure of PA1010 was preserved. The highest melting temperature of the crystals obtained in this work was 208°C for PA1010 treated at 1.5 GPa. Crosslinking occurred under pressures of 1.0–1.2 GPa. Only a broad diffraction peak centered at approximately 20° was observed on WAXD patterns, and no melting and crystallization peaks were found on DSC curves. IR spectra of crosslinked PA1010 showed a remarkable absorption band at 1370 cm^?1. The N? H stretching vibration band at 3305 cm^?1 was weakened. Crystallized PA1010 had a higher thermal stability than crosslinked PA1010, as indicated on TGA curves by a higher onset temperature of decomposition. © 2002 Wiley Periodicals, Inc. J Appl Polym Sci 83: 2522–2527, 2002     

铌锌酸铅基陶瓷相变的热力学分析

ＰＺＮ基陶瓷在烧结过程中都要经历由焦绿石相朝钙钛矿相的转变。ＰＺＮ基陶瓷中钙钛矿相含量的多少与添加剂的种类及数量密切相关，本工作根据化学热力学理论，讨论了内应力对化学势的影响，建立了一个热力学模型，并用该模型讨论了ＰＺＮ基陶瓷在烧结时的相变过程。     

基于CORS的地壳运动变形监测分析 基准的合理选择方法

介绍了GPS定位中有关坐标参考框架的一些重要概念,对坐标参考框架的一致性问题和采用GPS协议地球坐标系(ITRF或WGS-84)作为变形基准的特点及其适用性进行了对比分析,提出了采用ITRF作为变形分析基准时的坐标参考框架的转换与统一方法.     

为了建设最安全最放心的校舍——记第五届中国建筑学会建筑创作奖获得者王蔚

今年3月5日,第十一届全国人大二次会议在北京召开,国务院总理温家宝在政府工作报告中作出承诺：“要把学校建成最安全、家长最放心的地方”,当时的人民大会堂里响起了热烈的掌声……     

基于小波变换的手骨图像边缘提取方法

为了探求可以同步分离手指骨和腕骨各部分轮廓的方法,便于骨龄测定。针对医学图像特点和要求,引入小波变换,结合传统图像分割方法,采用边缘生长和寻找大区域的方法,实现手骨同步分离。研究表明该方法能够较为精确的、全自动的分离手骨各部分,能够同步分离目标边缘,同时保留细节信息。     

真型开关柜模拟缺陷下的局部放电试验研究

由于目前开关柜带电检测数据多为间接状态量,难以直接反映开关柜内部局部放电量的大小,容易造成对缺陷的误判。为此利用真型开关柜搭建了开关柜缺陷模拟试验装置,首先利用该装置模拟针板放电缺陷,采用超声波检测法（AE）、暂态地电位检测法（TEV）、特高频检测法（UHF）与脉冲电流法（PC）的比对找出针板放电的规律,包括带电检测信号的典型图谱以及与局部放电量对应关系。最后针对该装置提出了后续的研究范围。