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991.
何庆复 《武汉理工大学学报(材料科学英文版)》2009,24(3):428-431
Behaviour of hardening and serration yield of a Fe-Ni-Cr alloy under isothermal cycling (ISC) and out-phase TMF was studied
on the basis of varied hysteresis loops. Cycling hardening and serrated yielding for ISC depend on the temperature and the
total strain range, stronger hardening with serrated yielding at higher strain range under ISC at 600 °C, but no hardening
and serrated yielding occurred under ISC at 800 °C. Stronger hardening with stress serration occurred at the thermal path
going to the lowest temperature, no stress serration occurred at the highest temperature under the out-phase. The hardening
also depends on the total strain range, higher total strain range with lower cycling temperature resulted in a stronger hardening
and remarkable serration yielding behavior. Weaker hardening without serrated yielding occurred at near 800 °C may due to
an obvious cycling stress drop under out-phase TMF. Change in the shape of the hysteresis loops also expresses the degree
of the damage of the tested alloy under out-phase and ISC. 相似文献
992.
章桥新 《武汉理工大学学报(材料科学英文版)》2009,24(6):871-874
Silver powder was fabricated by spray pyrolysis, using 2%–20% AgNO3 solution, 336–500 mL/h flux of AgNO3 solution, 0.28–0.32 MPa flux of carrier gas and in the 620–820 °C temperature range. The effects of furnace set temperature,
concentration of AgNO3 aqueous solution, flux of AgNO3 aqueous solution as well as carrier gas on the morphology and particle size distribution of silver powder, were investigated.
The experimental results showed that with the high concentration of AgNO3 aqueous solution, the average grain size of silver decreased with the increasing of furnace set temperature. But the gain
size distribution was not homogenous, the discontinuous grain growth occurred. With the low concentration of AgNO3 aqueous solution, the higher furnace set temperature made the nano sliver grains sintered together to grow. Nano silver powder
about 100 nm was fabricated by spray pyrolysis, using 2wt% AgNO3 solutions, 336 mL/h flux of AgNO3 aqueous solution, 0.32 MPa flux of carrier gas at 720 °C furnace set temperature. 相似文献
993.
Systematical investigations of zero-field resistivity, magnetoresistance and magnetization were performed for a typical manganese compound La2/3Ca1/3MnO3. It is argued that the common origin for insulator-metal and paramagenetic ferromagnetic-transitions as well as colossal magnetoresistance is due to the formation of ferromagnetic clusters in the paramagnetic background. The transition to metallic state is resulted from percolation of ferromagnetic metallic clusters, while the colossal magnetoresistance is due to the application of magnetic field, which accelerates the growth of ferromagnetic metallic clusters and causes the shift of the onset temperature for the metallic percolation to higher temperature. Based on the random resistor network model, the zero-field resistivity versus temperature dependence is simulated by using experimental parameters, and experimental data well agree with those in whole temperature range, giving a strong support to our approach. 相似文献
994.
贺海燕 《武汉理工大学学报(材料科学英文版)》2009,24(3):359-362
Fatigue-free Bi3.2La0.8Ti3O12 ferroelectric thin films were successfully prepared on p-Si (100) substrates using metalorganic solution deposition process. The orientation and formation of 5-layers thin films
were studied under different processing conditions using XRD. Experimental results indicate that increase in annealing time
at 700 °C after preannealing for 10 min at 400 °C can remarkably increase (200)-orientation of the films derived from the
precursor solutions with two contents of citric acid. Meanwhile, high content of citric acid increases the film thickness
and is conducive to the a-orientation of the films with the preannealing, and low concentration of the solution is conducive to the c-orientation of
the films without the preannealing. 相似文献
995.
A series of dimer acid-based polyamides were synthesized by melt-polycondensation of dimer acid and various aromatic diamines,
and were characterized by Fourier transform infrared spectrum (FT-IR) and nuclear magnetic resonance (1H NMR). The physical properties of the polyamides, such as glass transition temperature, melting temperature, decomposition
temperature and mechanical properties were also investigated. The polyamides’ intrinsic viscosity ranges from 1.8 dL·g−1 to 2.2 dL·g−1, and the melting temperature ranges from 140 °C to 181 °C. The glass transition temperatures, observed from dynamic mechanical
analysis, fall in the range of 34.8–48.2 °C. The physical and mechanical properties of the resultant polyamides are similar
to those of the PA1212. The heat resistance and mechanical properties of poly (4, 4′-diphenylsulfone dimeramide) (PSD) and
poly(4, 4′-diphenyl dimeramide) (PPDI) are comparable to those of PA1212. 相似文献
996.
艾桃桃 《武汉理工大学学报(材料科学英文版)》2009,24(5):732-735
Al2O3/TiAl composites were successfully fabricated by hot-press-assisted exothermic dispersion method with elemental powder mixtures of Ti, Al TiO2 and Nb2O5, and the microstructure and mechanical properties were investigated. The results indicate the fine Al2O3 particles tend to disperse on the grain boundaries. The grain size of TiAl matrix decreases and the hardness increases with increasing Nb2O5 content. The bending strength and fracture toughness reach to a maximum when Nb2O5 content is 6 wt%, under 642 MPa and 6.69 MPa·m1/2, respectively. Based on the fractography and the observation of crack propagation path, it is concluded that the strengthening and toughening of such composites at room temperature can be attributed to the refinement of the TiAl matrix, the deflection behavior in the crack propagation and the dispersion of Al2O3 particles. 相似文献
997.
Fe-Ni-Al mixtures as hot-pressing sintering additive to Titanium diboride (TiB2) were studied. It is found that liquid alloy formed under high temperature hardly has effects on the densification behaviors
of TiB2-independent. Fe-Ni-Al additive just works as filler between TiB2 particles and does not change the TiB2-independent sintering behaviors. Pressing mode has a great effect on the liquid flowing between TiB2 particles. Multiple-steps pressing mode will give more time and space for the liquid flowing and improve the relative density
of TiB2-Fe-Ni-Al cermet. 相似文献
998.
通用突变控制方法及其在潜艇中的应用 总被引:1,自引:0,他引:1
王晓玢 《哈尔滨工业大学学报》2009,41(9):87-90
运用非线性动力学和突变理论,研究了高维系统建立具有理想特性突变的控制方法.引入冲失滤波器保证系统平衡点不变,并利用隐式判据、中心流形定理以及规范形法确定控制增益.以潜艇空间运动为例,阐述计算的全过程.该控制方法简便、快捷,可广泛应用到实际控制系统的设计中. 相似文献
999.
基于广义AIC和RPC的OFDM航空信道估计算法 总被引:1,自引:0,他引:1
文章通过对航空信道的分析,指出其稀疏信道特征,使用普通算法对此信道进行信道估计会引入高阶矩阵运算,为加快收敛速度、降低实现难度,文中提出了一种利用GAIC(generalized Akaike information criterion)准则和RPC(repeated phase-rotated Chu)训练序列的OFDM航空信道LS(1east squares)估计方法,该方法利用GAIC准则确定信道模型的阶次及抽头位置,为减小信道估计的运算复杂度,引入RPC序列作为训练序列,既满足了LS(least squares)估计,又大大简化了计算复杂度.文章针对具体应用给出文中算法的性能仿真结果,证明了此算法可避免高阶矩阵运算,节约了大量权值可忽略抽头所引入的资源占用和计算量,且显著减小估计误差,可更好跟踪快变的稀疏信道. 相似文献
1000.
To predict and optimize the temperature distribution of slab continuous casting in steady operational state, a three-dimensional model (named offline model) based on the heat transfer and solidification theories was developed. Both heat transfer and flux distribution characteristics of the nozzle sprays on the slab were considered, and the complicated boundary condi-tions, such as spray cooling, natural convection, thermal radiation as well as contact cooling of individual rolls were involved in the model. ... 相似文献