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991.
采用浸渍法制备负载金属Pd(其中金属Pd含量0.6g/L)活性组分的金属蜂窝载体催化剂,应用于甲烷部分氧化制合成气。实验表明,焙烧温度为950℃的催化剂较600℃的催化剂甲烷转化率、CO和H2的选择性更高,焙烧温度为950℃的催化剂在反应温度800℃,GHSV=1×105ml/g·h条件下,甲烷转化率为91%,CO和H2的选择性分别达到90%和89%。用SEM与XPS对催化剂进行表征,结果表明,950℃焙烧催化剂并没有出现明显的烧结现象,且可能由于更多零价Pd的出现,使得该催化剂的性能更好。由于金属蜂窝载体优良的导热性,对950℃焙烧温度制备的金属蜂窝催化剂,催化剂床层的飞温点温度小于880℃,可以解决其它类型催化剂在甲烷部分氧化反应中出现的飞温问题,具有一定的工业化意义。 相似文献
992.
993.
依据金属凝固的基本理论,在Oldfield的连续形核和晶粒长大模型基础上,引入了时间因子,运用随机方法,建立了连续冷却条件下形核和生长的随机模型,使形核和生长模型函数与时间直接相关,反映了连续冷却条件下的金属凝固微观组织的演化过程。基于上述模型,编制了计算模拟程序,模拟了Zn-5Al共晶合金微观组织的凝固过程,并用试验结果对模拟结果进行了验证对比,模拟结果与试验结果基本相符。 相似文献
994.
The need for new, improved solder alloys and a better understanding of reactions during the soldering process grows steadily
as the need for smaller and more reliable electronic products increases. Information obtained from phase equilibria data and
thermodynamic calculations has proven to be an important tool in the design and understanding of new lead-free solder alloys.
A wide range of candidate alloys can be rapidly evaluated for proper freezing ranges, susceptibility to contamination effects,
and reactions with substrate materials before the expensive process of preparing and testing candidate alloys is initiated. 相似文献
995.
Terry C. Lowe Ruslan Z. Valiev 《JOM Journal of the Minerals, Metals and Materials Society》2004,56(10):64-68
Severe plastic deformation (SPD) has emerged as a promising method to produce ultrafine-grained materials with attractive
properties. Today, SPD techniques are rapidly developing and are on the verge of moving from lab-scale research into commercial
production. This paper discusses new trends in the development of SPD techniques suchas high-pressure torsion and equal-channel
angle pressing, as well as new alternative techniques for introducing SPD. The paper also contains a comparative analysis
of SPD techniques in terms of their relative capabilities for grain refinement, enhancement of properties, and potential to
economically produce ultrafine-grained metals and alloys.
For more information, contact Terry C. Lowe, Science and Technology Base Programs, Los Alamos National Laboratory, Los Alamos,
NM 87545; (505) 667-7824; fax (505) 665-3199; e-mail tlowe@lanl.gov. 相似文献
996.
Casting/mold thermal contact heat transfer during solidification of Al-Cu-Si alloy (LM 21) plates in thick and thin molds 总被引:1,自引:0,他引:1
K. Narayan Prabhu Bheemappa Chowdary N. Venkataraman 《Journal of Materials Engineering and Performance》2005,14(5):604-609
Heat flow at the casting/mold interface was assessed and studied during solidification of Al-Cu-Si (LM 21) alloy in preheated
cast iron molds of two different thicknesses, coated with graphite and alumina based dressings. The casting and the mold were
instrumented with thermocouples connected to a computer controlled temperature data acquisition system. The thermal history
at nodal locations in the mold and casting obtained during experimentation was used to estimate the heat flux by solving the
one-dimensional inverse heat conduction problem. The cooling rate and solidification time were measured using the computer-aided
cooling curve analysis data. The estimated heat flux transients showed a peak due to the formation of a stable solid shell,
which has a higher thermal conductivity compared with the liquid metal in contact with the mold wall prior to the occurrence
of the peak. The high values of heat flux transients obtained with thin molds were attributed to mold distortion due to thermal
stresses. For thin molds, assumption of Newtonian heating yielded reliable interfacial heat transfer coefficients as compared
with one-dimensional inverse modeling. The time of occurrence of peak heat flux increased with a decrease in the mold wall
thickness and increase in the casting thickness. 相似文献
997.
Wen-Fung Wang 《Journal of Materials Engineering and Performance》2007,16(5):533-538
Two types of Hoganas iron powders—sponge (NC), and highly compressible (SC) were investigated. These specimens were compacted
with a pressure of 300, 400, 500, 600, and 700 MPa, before sintering in a production belt-type furnace. Steam treatment of
the specimens was at 570 °C for 30 min. The sintered density and as-sintered hardness increase with increasing compaction
pressure, and are significantly influenced by the powder structural characteristics. During steam treatment the type of powder
and compaction pressure have an important influence on the extent of pore closure and weight gain. The maximum hardness was
obtained for the components compacted at a pressure of 500 MPa for both groups of iron powders. Surface pore closure and oxidation
resistance of the steam-treated components are improved with increasing compaction pressure. 相似文献
998.
0IntroductionCompared with conventional welding methods,laserwelding has many advantages,such as large penetrationratio,small HAZ,small welding deformation.Another ad-vantage of laser welding is easy to weld complicated com-ponents because laser can be transferred by mirrors andoptical fiber.The laser welding will find wide applicationswith the laser system developing.Induced-plasma,molten pool and keyhole are mainphenomena in study of laser welding process.The varietiesof them indicate the … 相似文献
999.
Young-Wook Kim Yong-Seong Chun Ji Yeon Park Woo Seog Ryu Dong-Soo Park 《Metals and Materials International》2007,13(3):197-200
A new process using SiC fiber fabrics and SiC tapes to produce dense 2D SiC fiber-SiC (SiC/SiC) composites is demonstrated.
The strategy for fabricating the SiC/SiC composites involves: (i) alternately stacking the SiC fiber fabrics and SiC tapes
at room temperature, (ii) pyrolyzing of the stacked composites, and (iii) hot-pressing the pyrolyzed composites. By controlling
the hot-pressing temperature, it is possible to obtain dense 2D SiC/SiC composites with relative densities of >98%. The 2D
SiC/SiC composites show no degradation of the SiC fibers and a higher mechanical strength. 相似文献
1000.
D. S. van Vuuren A. D. Engelbrecht T. D. Hadley 《JOM Journal of the Minerals, Metals and Materials Society》2005,57(10):53-55
The value chain of titanium products shows that the difference between the cost of titanium ingot and titanium dioxide is
about $9/kg titanium. In contrast, the price of aluminum, which is produced in a similar way, is only about $1.7/kg. Electrowinning
of molten titanium from titanium dioxide is therefore believed to have significant potential to reduce the cost of titanium
products. The process is hampered by the high operating temperatures and sophisticated materials of construction required;
the high affinity of titanium for carbon, oxygen, and nitrogen; and physical and chemical properties of the different titanium
oxide species when reducing titanium from Ti4+ to metallic titanium.
For more information, contact D.S. van Vuuren, CSIR, Materials and Manufacturing Technology Department, Meiring Naude Road,
Pretoria, Gauteng 0181, South Africa; +27 12-841 2375; fax +27 841 2135; e-mail dvvuuren@csir.co.za. 相似文献