N-苄基丙烯酰胺的合成

以丙烯腈和苯甲醇为原料，浓硫酸作催化剂，合成了N-苄基丙烯酰胺（N-BAA）。考察了反应温度、反应时间和催化剂用量等因素对产物收率的影响，得出了最佳反应条件：n（丙烯腈）：n（苯甲醇）：n（浓硫酸）=3：1：1．2，反应时间3h，反应温度60℃。在最佳条件下，N-BAA的收率可达92％。每100g粗产物用10％氢氧化钠溶液提纯，精制产物纯度可达99．80％，熔点为64～65℃。通过红外光谱对产物结构进行了表征。     

智能化中高压变频器实载试验平台的实现

中、高压变频器产量越来越多，但试验手段大多比较落后，一般采用带电机空转的方法。本文介绍了一个高压变频器试验平台，通过该平台可以对电压等级在3kV～10kV、功率在5000kW以下的变频器进行实载试验。     

可拆装高架火炬的应用

结合工程实例,介绍了我国第一座可拆装高架火炬的基本原理及组成,并对可拆装高架火炬与普通高架火炬在安全、技术、安装、维修、占地面积、投资等方面进行了比较,还分析了高架火炬未来的发展趋势.     

有限元技术在数值试井中的应用

分析了试井技术的发展趋势，对有限元分析技术及其发展作了较为全面的介绍，重点阐述了利用有限元技术进行三维建模的方法和步骤，尤其是对复杂的非对称边界和非均质油藏的建模方法和技巧进行了深入探讨。利用数值试井技术，石油工程师可以方便准确地对复杂油藏和边界进行建模，试井的模拟过程和油藏任意位置的压力瞬间变化都可以通过图形和颜色的变化显示出来，解释的精度和速度都得到了大大地提高。     

A novel compact ring dual-mode filter with adjustable second-passband for dual-band applications

In this letter, a novel compact ring dual-mode with adjustable second-passband for dual-band applications are presented. A ring resonator with two different geometric dimensions are derived and designed to have identical fundamental and the first higher-order resonant frequencies, and to establish appropriate couplings in the structure. Moreover, the proposed filter has smaller size as compared with the basic topology of stopband filters and stepped-impedance-resonator (SIR) filters. The measured filter performance is in good agreement with the simulated response.     

Blind estimation of OFDM carrier frequency offset via oversampling

Blind deterministic estimation of the orthogonal frequency division multiplexing (OFDM) frequency offset via oversampling is proposed in this paper. This method utilizes the intrinsic phase shift of neighboring sample points incurred by the frequency offset that is common among all subcarriers. The proposed method is data efficient - it requires only a single OFDM symbol to achieve reliable estimation, hence making it more suitable to systems with stringent delay requirement and mobility-induced channel variation. The proposed scheme is devised to perfectly retrieve frequency offset in the absence of noise. Quite remarkably, we show that in the presence of channel noise, this intuitive scheme is indeed the maximum likelihood estimate of the carrier frequency offset. The possible presence of virtual carriers are also accommodated in the system model, and some interesting observations are obtained. The Cramer-Rao lower bound is derived for the oversampling-based signal model, and we show through numerical simulation that the proposed algorithm is efficient. Practical issues such as identifiability, the front-end filter bandwidth, and the possible presence of correlated noises are also carefully addressed.     

非接触式全场三维激光ESPI与Shearography(NDT)测试技术

本文介绍最新激光电子散斑干涉技术ESPI与Shearography激光错位检测技术的基本原理及其应用.该技术足近十年间发展起来的最新的光测技术,它们的特点是非接触式全场三维测试,适用于新材料研究、电子元器件与构件的力学性能试验、振动测试及无损检测.国外的应用表明,ESPI技术可以提供快速、全场、三维的测试信息,能解决许多目前电测方法所不能解决的复杂问题,是目前具有广泛工程应用前景的先进的光测技术.     

Blind feedforward cyclostationarity-based timing estimation for linear modulations

By exploiting a general cyclostationary (CS) statistics-based framework, this letter develops a rigorous and unified asymptotic (large sample) performance analysis setup for a class of blind feedforward timing epoch estimators for linear modulations transmitted through time nonselective flat-fading channels. Within the proposed CS framework, it is shown that several estimators proposed in the literature can be asymptotically interpreted as maximum likelihood (ML) estimators applied on a (sub)set of the second- (and/or higher) order statistics of the received signal. The asymptotic variance of these ML estimators is established in closed-form expression and compared with the modified Crame/spl acute/r-Rao bound. It is shown that the timing estimator proposed by Oerder and Meyr achieves asymptotically the best performance in the class of estimators which exploit all the second-order statistics of the received signal, and its performance is insensitive to oversampling rates P as long as P/spl ges/3. Further, an asymptotically best consistent estimator, which achieves the lowest asymptotic variance among all the possible estimators that can be derived by exploiting jointly the second- and fourth-order statistics of the received signal, is also proposed.