纳米尺寸硫化镍化学增感剂

本文发现了硫化镍纳米粒子对卤化银乳剂的化学增感作用，采用水不溶性的硫化镍纳米粒子作为化学增感剂，与水溶性的硫代硫酸钠增感剂相比，可以在乳剂灰雾增加不大的条件下明显提高乳剂的感光度和反差。     

高分子水处理剂的绿色化研究进展

简要介绍了近年来水处理领域在高分子水处理剂产品及生产工艺方面的绿色化研究进展状况。     

颗粒活性炭的特性参数与吸附性能的关系试验

采用活性炭进行饮用水的深度处理,选择适合原水水质的活性炭至关重要,通过6种不同颗粒活性炭特性参数的测试,对饮用水有机物的吸附试验以及吸附等温线的测定,结果表明:针对颗粒活性炭的筛选,碘值,亚甲蓝值,吸附等温线的KF及斜率1/n值均不能单独作为评价筛选活性炭优劣的指标,而应综合考虑颗粒活性炭的孔径分布与原水中有机物的相对分子质量分布相匹配等。研究还表明:碘值,亚甲蓝值,吸附等温线的KF存在一定的相关性,从颗粒活性炭的特性参数和吸附性能参数可以推测活性炭滤柱试验吸附效果。颗粒活性炭用于饮用水深度处理,能去除水中相对分子质量小的有机物,处理的水量为颗粒活性炭体积的4800倍时,对CODMn的去除率为15%左右。     

Synthesis,degradation, and drug delivery of cycloaliphatic poly(ester anhydride)s

The high melting point of poly(1,4‐cyclohexanedicarboxylic anhydride) [poly(CHDA)] is a disadvantage, in that it is intractable in the melting process of a drug delivery system. This report relates to diols introduced into the polyanhydride main chain to decrease its melting point. Various poly(ester anhydride)s containing ethylene glycol, 1,3‐propanediol, 1,4‐butanediol, or 1,6‐hexandiol [poly(CHDA–XDO)] were synthesized by the esterification reaction and melt polycondensation. FTIR, DSC, WAXD, and intrinsic viscosity of polymers were recorded and hydrolytic degradation, as well as in vitro drug delivery, was conducted. The results show that the samples are stable in an anhydrous environment at room temperature and degrade in water following a surface erosion mechanism. The degradation period of poly(CHDA–XDO) ranged from 130 to 320 h as a result of the different diols and amounts of XDO introduced. The in vitro drug delivery gave 130–350 h of stable delivery along with the typical surface erosion mechanism. © 2002 Wiley Periodicals, Inc. J Appl Polym Sci 86: 2509–2514, 2002     

汽车刹车片用改性酚醛树脂的生产

在原有的酚醛树脂生产设备上，用腰果壳油和三聚氰胺对酚醛树脂进行改性，制得的改性树脂具有较好的软化点、聚合速度、挥发度和游离酚等性能；并且热分解温度较普通酚醛树脂大大提高。用它作胶粘剂生产的汽车刹车片，冲击强度增大：磨损率降低、摩擦性能提高、产品成本也大为降低。     

成形压力对氧化铝瓷球性能的影响

本文以不同的压力等静压成形瓷球，研究了成形压力对瓷球烧结温度、密度及耐磨性的影响。结果表明：在本研究系统内随着压力的增加瓷球的烧结温度下降，烧成温度范围拓宽。采用150MPa成形的瓷球密度最大且耐磨性最好。     

Augment low-field intra-operative MRI with preoperative MRI using a hybrid non-rigid registration method

Background

Preoperatively acquired diffusion tensor image (DTI) and blood oxygen level dependent (BOLD) have been proved to be effective in providing more anatomical and functional information; however, the brain deformation induced by brain shift and tumor resection severely impairs the correspondence between the image space and the patient space in image-guided neurosurgery.

Method

To address the brain deformation, we developed a hybrid non-rigid registration method to register high-field preoperative MRI with low-field intra-operative MRI in order to recover the deformation induced by brain shift and tumor resection. The registered DTI and BOLD are fused with low-field intra-operative MRI for image-guided neurosurgery.

Results

The proposed hybrid registration method was evaluated by comparing the landmarks predicted by the hybrid registration method with the landmarks identified in the low-field intra-operative MRI for 10 patients. The prediction error of the hybrid method is 1.92 ± 0.54 mm, and the compensation accuracy is 74.3 ± 5.0%. Compared to the landmarks far from the resection region, those near the resection region demonstrated a higher compensation accuracy (P-value = .003) although these landmarks had larger initial displacements.

Conclusions

The proposed hybrid registration method is able to bring preoperatively acquired BOLD and DTI into the operating room and compensate for the deformation to augment low-field intra-operative MRI with rich anatomical and functional information.     

异常高压气井生产动态仿真研究及应用

异常高压气井生产动态仿真方法不仅改变了传统物理仿真成本高、过程复杂的缺点,而且具备了计算机仿真模拟的准确性。考虑异常高压气井流体高压、高温的特点,本文将异常高压气井生产压降分解为地层流动压降、井筒流动压降和嘴流流动压降三个过程,并建立了气井生产动态流动数学模型;本文利用计算机仿真技术模拟了异常高压气井地层流体流动过程、井筒流体流动过程和气嘴流体流动过程,并预测了气井生产动态流动参数,为下步异常高压气井动态配产提供了基础数据。通过实例分析,将计算机仿真预测出的异常高压气井流动参数代入优化配产模型计算出配产结果与实际配产结果十分接近,表明异常高压气井生产动态仿真对实际生产具有重要的指导意义。     

UHMWPE/LDPE复合材料拉伸破坏的声发射特性研究(Ⅱ)

本文续“UHMWPE/LDPE复合材料拉伸破坏的声发射特性研究(Ⅰ)”,进一步研究了UHMWPE/LDPE复合材料拉伸破坏的声发射特性,具体研究了[0°]、[90°]在拉伸破坏过程中声发射参数特征,并对拉伸破坏机理进行了初步的研究。