电位滴定法研究~(99)Tc-HMDP和~(99)Tc-HEDP中Tc的氧化态

~(99)Tc-HMDP和~(99)Tc-HEDP溶液是在相应的螫合剂存在下,用过量SnCl_2还原~(99)TcO_4-制得。用标准I_2液对SnCl_2进行了剩余量电位滴定,确定了在pH～3的介质中,~(99)Tc-HMDP和~(99)Tc-HE-DP中~(99)Tc的氧化态均为+4。全部实验在N_2气流中进行。~(99)Tc-HMDP和~(99)Tc-HEDP的紫外光谱表明:在用I_2滴定的过程中,~(99)Tc只处于一种氧化态+4;将它们放置在空气中,一小时后仍较稳定。     

Speech Enhancement via Residual Dense Generative Adversarial Network

Generative adversarial networks (GANs) are paid more attention to dealing with the end-to-end speech enhancement in recent years. Various GAN-based enhancement methods are presented to improve the quality of reconstructed speech. However, the performance of these GAN-based methods is worse than those of masking-based methods. To tackle this problem, we propose speech enhancement method with a residual dense generative adversarial network (RDGAN) contributing to map the log-power spectrum (LPS) of degraded speech to the clean one. In detail, a residual dense block (RDB) architecture is designed to better estimate the LPS of clean speech, which can extract rich local features of LPS through densely connected convolution layers. Meanwhile, sequential RDB connections are incorporated on various scales of LPS. It significantly increases the feature learning flexibility and robustness in the time-frequency domain. Simulations show that the proposed method achieves attractive speech enhancement performance in various acoustic environments. Specifically, in the untrained acoustic test with limited priors, e.g., unmatched signal-to-noise ratio (SNR) and unmatched noise category, RDGAN can still outperform the existing GAN-based methods and masking-based method in the measures of PESQ and other evaluation indexes. It indicates that our method is more generalized in untrained conditions.     

云计算安全：概念、现状与关键技术

随着云计算的广泛应用,云计算安全问题逐渐凸显出来。文章首先阐述了云计算安全相关概念,并对云计算的安全问题和云计算安全特征进行分析,然后对云计算安全的现状和典型的云计算安全体系架构进行了介绍,并对云计算安全的关键技术进行分析,最后给出了结论。     

一种并行冗余遥控锁定投放控制系统

以海上无人演练战场等复杂环境下实现对大负载作战单元的遥控布放为需求,提出了一种包含短波、超短波和卫星无线信道,以及本地端手动控制的多并行冗余锁定投放控制系统.设计了一种新型锁定投放装置,使用恒流源驱动的直流减速电机推动锁闩执行布放任务,具有功耗小、负载大等优点;在锁定投放装置的控制器中并行集成了以上几种投放控制接口,能以互为备份的方式执行任意种或多种投放控制指令,提高了系统的鲁棒性.该锁定投放控制系统已多次执行海上任务,工作稳定可靠.     

Low‐voltage and high‐transmittance blue‐phase liquid‐crystal device with slanted electrodes

Abstract— A low‐voltage (～10 V_rms) and high‐transmittance (～90%) polymer‐stabilized blue‐phase liquid‐crystal (BPLC) device with a slanted‐electrodes structure is proposed. Unlike the vertical‐field‐switching (VFS) mode in which oblique incident light and a vertical field are employed, the proposed device utilizes normal incident light and an oblique field. The slanted electrodes generate a strong and uniform oblique electric field, which contributes in obtaining low voltage and high transmittance. Moreover, no couple films or prism sheets are needed, which helps to enhance the optical efficiency and simplify of the device structure. This device has great potential application for emerging BPLC displays and photonic devices.     

超重力对燃烧合成Ti（C，N）-TiB2复合粉体的影响

以Ti和B4C为起始反应物，分别在常规和超重力条件下通过燃烧合成技术制备出Ti（C,N）-TiB2复合粉体，利用XRD和SEM对燃烧产物进行了表征，研究了起始组成和超重力条件对燃烧产物相组成和微观形貌的影响。结果表明，燃烧产物主要由Ti（C，N）和TiB2组成，通过改变起始配方中Ti／B4C的摩尔比，可以调节产物中Ti（C，N）和TiB2的相对含量。超重力条件下，反应物颗粒接触更加充分，碰撞更加频繁，因而晶粒形态发育更加完整，生成规则的多面体。     

巨磁电阻材料的研究与应用

介绍了一种新型的磁性功能材料－巨磁电阻材料，综述了其研究进展情况。并就它在巨磁电阻传感器、高密度磁记录读出磁头、巨磁电阻随机存储器以及自旋晶体管等磁电子元器件上的进行了论述。     

Formation of WC/Ni hard alloy coating by laser cladding of W/C/Ni pure element powder blend

WC/Ni coating was formed by laser cladding of a W/C/Ni powder blend. The formed WC crystals have rectangular or quadrangle cross-section shapes with size of 2–30 μm. Step, twist and cross growth morphologies of WC formation were observed. The coating contains WC, CW_3, WNi, FeW₃C, Fe₆W₆C, W₃O, W, C, and (Fe,Ni) phases.     

饮用水中天然有机物的分析与表征方法

天然有机物(NOM)是一类分布广泛、成分复杂的有机混合物,可严重影响饮用水的处理效率,并可能对出水水质产生严重的不利影响。因此,为了改进和优化饮用水的处理过程,在研究和实际应用阶段对NOM进行表征和定量以了解其结构特性和反应性具有重要意义。文中先对NOM的富集方法进行了介绍,接着梳理了不同分离方法的依据及作用,最后总结了各类表征方法的原理及应用,以期有助于对NOM和饮用水处理的深入研究。     

考虑多元可控负荷协调的配网鲁棒优化经济调度模型

为有效应对大规模分布式可再生能源和可控负荷接入配网后在经济优化调度方面所带来的挑战,本文建立考虑多元可控负荷协调的配网鲁棒优化经济调度模型.首先考虑电池储能系统、电动汽车及可参与需求侧管理的电负荷的能量转移特性,建立多元可控负荷可调模型;进而考虑配网中多元可控负荷的调峰能力及动态约束以运行成本最低建立配网鲁棒经济优化调度模型;最后,以蒙东某配网实际数据为例,在改进IEEE 14节点配电系统上进行调度仿真分析,验证本文所提出模型可充分利用多元可控负荷的调节能力,有效提升配网运行经济性.