Effect of storage temperature on phenolics stability in hawthorn (Crataegus pinnatifida var. major) fruits and a hawthorn drink

The stability of five major phenolics, namely (−)-epicatechin (EC), procyanidin B₂ (PC-B₂), chlorogenic acid (ChA), hyperoside (HP) and isoquercitrin (IQ), in hawthorn fruits and a canned hawthorn drink were evaluated during 6 months of storage in the dark at three different temperatures (4, 23 and 40 °C). HPLC with a diode-array detector was used to determine the contents of the individual compounds. The results showed that the studied phenolics in the hawthorn fruits and the drink were both stable at 4 °C and relatively unstable at 23 and 40 °C with varied extents of degradation. At room temperature (23 °C), marked degradations of EC and PC-B₂ were observed in both the fruits and the drink with around 50% and 30% decrease after a 6-month storage, respectively. A more significant decrease of the phenolics was observed at 40 °C, especially for EC and PC-B₂, which were almost completely degraded after a 6-month storage. HP, IQ and ChA were relatively stable at 23 °C, but unstable at 40 °C. Therefore, low-temperature storage is recommended for maintaining the quality and efficacy of hawthorn fruits and its preparations.     

钢结构防火涂料应用中存在的几个问题

在分析钢结构防火涂料应用发展现状的基础上,针对实际应用中影响质量的几个问题进行了剖析,提出了改进的建议。     

超高强度钢连续冷却组织和时效反应的研究EI

观察分析了冷却速度对低合金超高强度钢（４０ＣｒＭｎＳｉＭｏＶＡ）精细组织的影响。结果表明，在冷却、低温等温（或回火）过程中，钢显微组织中的马氏体或贝氏体存在时效阶段。其组织特征为呢纹花样。α和ε间的取向不满足Ｊａｃｋ关系，它属一种新的取向关系。过渡型碳化物可直接从呢纹花样区析出。     

离心式冷水机组在线监控系统研究

阐述了离心式冷水机且在线监控系统的工作特点以及对监控的要求，说明了在线监控系统的基本配置，关键技术点和功能模块化的软硬件设计。     

Evaluation of accuracy of measuring intraocular pressure by handheld non-contact applanation tonometer

PURPOSE: To evaluate the accuracy of measuring intraocular pressure by handheld non-contact applanation tonometer. METHOD: 58 patients' (113 eyes) intraocular pressure were measured by Keeler, non-contact tonometer and R 900 Goldmann applanation tonometer and the results of measurement of intraocular pressure by the two kinds of tonometers were compared. RESULT: The mean intraocular pressure measured by non-contact is 16.31 +/- 5.59 mmHg and 17.49 +/- 6.13 mmHg (1 mmHg = 0.1333 kPa) by Goldmann applanation tonometer, respectively. There was no statistical significance to be found (P > 0.05) between the two methods. By linear correlation and regression analysis, a positive correlation was found between the two methods (r = 0.8942, b = 0.8154). CONCLUSION: The handheld non-contact tonometer has the same accuracy and reliability of measurement of intraocular pressure comparing with Goldmann applanation tonometer, and it can be used in glaucoma clinic and screening.     

Monoalkyl Esters of Isoalkylphosphonic Acid as Extractants in Rare Earth Separation

Four monoalkyl esters of isoalkylphosphonic acids have been studied for the chromatographic separation ofrare earths (RE).The relationship between distribution ratios and acid concentration of the eluants forsamarium and ytterbium has been explored.The characteristics of these extractants loaded onto macroreticularpoly (methyl methacrylate) resin beads for the separation of lanthanum,cerium,praseodymium and neodymiumhave been compared.Among the extractants studied,mono(1-methylheptyl) ester of isooctylphosphonic acidwas found to be the best for RE separation.The acidity for separation is lower than any known P-containingextractants for the same purpose.For instance,with 1.73 mol·L~(-1) nitric acid as eluent,thulium,ytterbium andlutetium can be separated quantitatively.The extractant-loaded resins possess high column efficiency with goodkinetic characteristics.The extraction mechanism was also explored.     

高频MnZn功率铁氧体烧结工艺研究

按照氧化物陶瓷工艺对高频MnZn功率铁氧体烧结工艺条件进行了研究。烧结温度越高，晶粒越大，晶界越薄，电阻率越低，磁芯损耗越大，起始磁导率和烧结密度分别在1240℃和1230℃达到最大值。延长保温时间，可以使晶粒充分生长，晶界变薄，电阻率减小，损耗增大。保温3h后，起始磁导率和烧结密度均可达到最大值。氧分压越低，材料起始磁导率越高，电阻率越小，损耗越大，但氧分压低于5％后烧结密度不再继续增加。     

求新 求精 求效益

我是 1990年 8月毕业于上海工程技术大学到英雄金笔厂工作的 ,从事笔类设计至今已有 12个年头了。从一个只有理论知识、冲劲十足的大学生 ,逐渐成熟稳健起来 ,现在担任企业的研究所所长 ,主要负责设计工作 ,其间确有许多体验值得回顾。在刚进厂的那段时间里 ,我在成品车间里摸爬滚打 ,熟悉产品的各道生产工序 ,为今后的工作打基础。我并不象有些大学生认为进车间实习只是过过场子 ,而是决心扎扎实实地去学一些实在的东西 ,虚心向各道生产工序的老师傅请教 ,从模具开制到成品装配 ,不厌其烦 ,凡有工作都动手 ,为的是把上上下下的工艺摸透彻。…     

DCA-112催化裂化抑焦剂的工业应用

针对改善催化裂化反应微环境研制开发的DCA - 112催化裂化抑焦剂 ,具有抑制生焦、改善产品分布、应用流程简单、加注方便等特点 ,经中石化长炼分公司 1Mt/a重油催化装置工业应用表明 ,在相近的工艺条件下 ,掺渣比提高 4 13个质量百分点 ,总液收提高 1 0 2个质量百分点。     

新钢炼铁系统技术进步

通过加强精料、实施技术改造、优化高炉操作等措施，新钢炼铁生产取得了明显的进步，技术经济指标明显改善。