Effect of hollow glass beads on density and mechanical properties of silicone rubber composites

In this work, low density hollow glass beads (HGB)/silicon rubber (SR) composites were prepared by solution method and flocculation process. The prepared samples were characterized by scanning electron microscopy, Fourier transform infrared spectroscopy, tensile test, and friction test. The results show that the densities of SR composites decrease from 1.140 to 0.792 g/cm³ with the addition of HGB. By comparing theoretical density with true density, it can be estimated that the ratio of shattered HGB increase from 8.79% to 24.76%. Especially, the mechanical properties of SR composites were improved by surface modification of HGB. By adding surface-modified HGB at 5 and 10 wt%, the tensile strengths of SR composites were enhanced by 17.8% and 28.2%, respectively. In addition, tear strength, shore A hardness, compression set, and friction property were significantly ameliorated. Furthermore, the mechanism of surface-modified HGB in mechanical properties was analyzed.     

Preparation of treelike and rodlike carboxymethylated nanocellulose and their effect on carboxymethyl cellulose films

In this work, carboxymethyl cellulose (CMC) with low substitution degree, followed by different posttreatments, was applied to prepare treelike CMC nanofibrils (CMCNFs) and rodlike CMC nanocrystals (CMCNCs), and their performance in CMC composite film was evaluated simultaneously. From transmission electron microscopy results, it was found that the treelike CMCNCFs exhibited a lager aspect ratio compared to the rodlike CMCNCs. As for reinforcing CMC film, 4 wt% was the best adding amount, at this time, the tensile strength of CMC/CMCNFs and CMC/CMCNCs composite films was increased by 72.1% and 47.3%, respectively. Moreover, adding these nanofillers to CMC also could enhance the thermal stability of composite films slightly, while the transmittance of composite films was reduced at the same time. In addition, CMC/CMCNFs film was designed as a packaging box to determine its performance. Therefore, this study could reveal the differences of properties for composites with different types of nanocellulose and provide a foundation for further application of nanocellulose.     

Enhanced interfacial adhesion of aramid fiber reinforced rubber composites through bio-inspired surface modification and aramid nanofiber coating

In order to improve the interfacial adhesion between aramid fiber (AF) and rubber matrix, a simple and facile method of aramid nanofiber (ANF) coating is demonstrated in this article. Tannic acid (TA) and polyethyleneimine (PEI) are polymerized in an alkaline solution to form a thin TA/PEI (TP) layer that is deposited on the surface of AF to introduce functional groups such as hydroxyl and amino groups. Then, the ANF coating is utilized to construct nanostructures on the surface of AF to improve the interfacial adhesion between the fiber and the rubber. Through hydrogen bonding and/or π-π stacking between the TP layer and the ANF, the ANF coating is firmly attached to the surface of AF. Compared with the untreated fiber, the interfacial adhesion of AF coated with ANF after 1, 3, 5, 7, 9 deposition cycles is increased by 27.8%, 29.1%, 31.5%, 43.1%, and 30.3%, and the mechanical properties of the fibers remain almost unchanged. This method shows its advantages of simple, facile, and time-effective, which is of great significance for industrial applications.     

车间硫化烟气与实验室模拟硫化烟气相关性研究

采用热脱附-气相色谱/质谱和顶空气相色谱/质谱分别对车间硫化烟气和实验室模拟硫化烟气进行分析,并研究两者间的关系。结果表明：车间硫化烟气热脱附优化条件为脱附温度　180 ℃,脱附时间　15 min,冷阱温度　－65 ℃;以顶空进样器模拟橡胶硫化过程来进行实验室模拟硫化烟气成分分析;相同胶料的车间硫化烟气检出成分少于实验室模拟硫化烟气检出成分,但两者大部分成分相同,相同成分多为毒性较大的含氮类化合物和苯等;车间硫化烟气与实验室模拟硫化烟气解析量基本呈正相关。     

基于深度学习增强的LSD杆塔倾斜度检测

杆塔的倾倒会对整个电网产生严重的破坏并威胁周围居民的生命安全,电力巡检无人机利用计算机视觉对杆塔进行巡检既节省了人力资源又显著地提高了电网的巡检效率.为了国网巡检人员在杆塔倾倒前及时得到预警,对电力巡检无人机中的基于计算机视觉的杆塔倾斜检测算法进行了研究,设计了一种基于YOLOv3的深度神经网络结合LSD线段提取方法对杆塔的倾斜进行检测.利用在山西电网无人机实际巡检的杆塔图片制作杆塔的VOC2007数据集并利用YOLOv3神经网络对杆塔进行目标检测,并将检测后得到的Bounding box根据网络训练后的mIOU参数进行微调后作为LSD检测的ROI.接着,该方法在ROI中将检测的线段进行过滤和融合,根据杆塔特点进行杆塔的二次识别.最后利用得到的杆塔外边线做出该方向上的杆塔中线并计算杆塔在该方向的倾斜度.该文中实验利用山西国网电力公司提供的数据进行验证,结果表明,杆塔的倾斜检测效果在各种拍摄高度和背景干扰下都较为精确,杆塔目标的正确识别率达到97％,倾斜度检测平均误差小于0.85°.     

测试性能估算的测试集重排序方法

目前在集成电路测试中,测试时间长、测试效率低是影响测试成本的关键问题之一,针对此问题提出了一种基于测试性能估算的测试集重排序方法。首先针对不同的故障类型进行分类建模,然后对每种故障类型进行仿真,通过在每个逻辑门注入故障,统计测试向量命中故障门的面积之和来估算测试向量的测试性能,最后根据测试性能的优劣对测试集进行重新排序。实验表明,对于单固定故障使用排序后的测试集测试可以减少5329%的故障检测时间。该方法是通过对电路的逻辑结构进行分析和统计然后对测试集进行优化,对ISCAS 89标准电路进行试验,与其他测试集重排序对比,有着明显的优化。算法运行完全是基于软件的,不需要增加任何硬件开销,可以直接相容于传统的集成电路测试流程。     

基于Abaqus的医用塑料止血夹结构仿真分析及优化设计

以医用止血夹为研究对象,分析其受力状况并建立力学模型,应用Abaqus软件对其闭合过程中的受力变形和应力应变情况进行模拟仿真分析,并根据分析结果对产品结构进行优化设计。结果表明,优化后止血夹闭合时塑性铰处的塑性应变比原方案降低了60.5 %,确保产品能够满足使用要求。     

Self-Diffusion of Iron in Molten Fe-C Alloys

Self-diffusion coefficients of iron in molten Fe-C alloys have been measured by using the capillary method. In addition, the samples have been autoradiographed and sectioned to insure that no significant convection has occurred during the diffusion. The results can be represented by the equation D = 4.3×10^?3 exp (—12.200/RT) for carbon = 4.6 pct and T = 1513° to 1633°K; and D = 1.0×10^?2 exp (—15,700/RT) for carbon = 2.5 pct and T = 1613° to 1673°K. The D values are higher and the heat of activation for diffusion lower in alloys containing more carbon. Calculation based on the Einstein-Stokes equation indicates that the diffusing species is iron ion.     

Effect of ZrO<Subscript>2</Subscript> coating on<Emphasis Type="Italic">in vitro</Emphasis> formation of calcium phosphate

We prepared zirconia thin films on (100) Si wafer by using a chemical solution deposition with a zirconium naphthenate as a starting material. The films were pyrolyzed at 500°C for 10 min and finally annealed for 30 min in air at 500°C. Amorphous films after annealing had no distinct structure and were uniform along the cross section line.In vitro formation of the calcium phosphate was evaluated by the field emission-scanning electron microscope, energy dispersive X-ray spectrometer and Fourier transform infrared spectroscopy.