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91.
Christian P. Romero Jonathan I. Avila Edgardo Cisternas Guerau B. Cabrera Alejandro L. Cabrera Kristiaan Temst Margriet J. Van Bael 《Journal of Materials Science》2007,42(18):7667-7672
Hydrogen desorption curves were obtained from a sample composed of a square arrangement of Co dots with average diameter of
4.4 μm, separated by a distance of 11.6 μm. A macroscopic sample of Co dots grown on a 2.5 × 2.5 cm Si substrate was made
by standard lithographic techniques and used in these experiments. Thermal programmed desorption (TPD) was performed under
ultra-high vacuum conditions. Hydrogen TPD curves were obtained from a 1 × 1 cm Co dots samples displaying a maximum of intensity
at 425 K. Hydrogen TPD curve was also obtained from 1 cm× 1 cm samples of Co films and Co foils for comparison. The hydrogen
TPD curves have decreasing intensity from the Co foils to the Co dots and finally to the Co films. This indicates that there
are more sites for hydrogen adsorption on the Co dots than in the Co films. This is a surprising result because there is approximately
8.7 times less Co atoms exposed in the Co dots that in the Co film sample. A desorption energy of 27 kcal/mol was obtained
for the Co dots suggesting that hydrogen is adsorbed on an hcp hollow site of the Co dot crystalline structure. 相似文献
92.
The aim of the present paper is to review the recent progress in the synthesis of in situ particle reinforced aluminum composites
using thermal, mechanical and combined mechanical-thermal activation of aluminothermic reduction reactions. The combination
of combustion synthesis (CS) and mechanosynthesis (MS) is the most recent development in the processing of advanced materials
like micro and nano aluminum based composites. The combined mechanical thermal synthesis (MTS) has widened the possibilities
for both CS and MS. MTS holds great potential for commercial viability and offers exciting processing route for the synthesis
of advanced materials. Enhanced reaction kinetics and extended concentration limits in MTS are demonstrated by illustrating
the synthesis of aluminum based nanocomposite involving Al–CeO2. 相似文献
93.
Hideo Sawada Hiroshi Kakehi Masashi Koizumi Yoshihiro Katoh Masashi Miura 《Journal of Materials Science》2007,42(17):7147-7153
Fluoroalkyl end-capped N-(1,1-dimethyl-3-oxobutyl)acrylamide oligomer [RF-(DOBAA)
n
-RF] reacted with tetraethoxysilane (TEOS) and silica nanoparticles in the presence of low-molecular weight biocides such as
hibitane, hinokitiol, and hinokioil under alkaline conditions to afford RF-(DOBAA)
n
-RF/silica nanocomposites-encapsulated these biocides in excellent to moderate isolated yields. Fluoroalkyl end-capped N,N-dimethylacrylamide oligomer [RF-(DMAA)
n
-RF] and acrylic acid oligomer [RF-(ACA)
n
-RF]/silica nanocomposites-encapsulated hibitane were obtained under similar conditions. Dynamic light scattering measurements
showed that the size of these fluorinated nanocomposites-encapsulated biocides thus obtained is nanometer size-controlled.
Additionally, these fluorinated nanocomposites were shown to have a good dispersibility and stability in methanol and water.
Of particular interest, these fluorinated nanocomposites-encapsulated biocides were found to have a good antibacterial activity
against Staphylococcus aureus, and these nanocomposites were applied to the surface modification of traditional organic polymers such as poly(methyl methacrylate). 相似文献
94.
95.
96.
Mamiko Hori Cécile Pagnoux Jean-François Baumard Masayuki Nogami 《Journal of Materials Science》2007,42(1):80-86
A new method is proposed to produce gold nanoparticles (GNP) by in situ reduction of a gold salt dissolved in water. The reducing
agent used is Tiron instead of the citrate anion most often mentioned in literature. The influence of various parameters has
been investigated, such as the content of Tiron with respect to that of the precursor of gold HAuCl4, or the initial pH of the solution after mixing of reactants. It is shown that Tiron also exerts a positive influence as
a dispersant, which impedes agglomeration of gold nanoparticles. The typical average size of GNP synthesized in the present
work is close to 7 nm. 相似文献
97.
98.
M. K. Bakhadyrkhanov O. É. Sattarov Kh. M. Iliev K. S. Ayupov Tuérdi Umaier 《Semiconductors》2005,39(7):789-791
It is experimentally ascertained that light stimulates the negative magnetoresistance observed in a high electric field in silicon doped with boron and manganese. The optimum conditions (the electric field, temperature, illumination, and resistivity of the material) for observation of the largest magnitude of negative magnetoresistance in (Si:B):Mn are determined. The dependence of the negative magnetoresistance on the concentration of compensating impurity is established. 相似文献
99.
This letter presents some further results on the local stability in equilibrium for Internet congestion control algorithm proposed by Low et al., (IEEE/ACM Transactions on Networking, 1999). The propagation delay d(t) is assumed to be time-varying and have maximum and minimum delay bounds (i.e., d/sub m//spl les/d(t)/spl les/d/sub M/), which is more general than the assumption (0相似文献
100.
In recent years, constructing a virtual backbone by nodes in a connected dominating set (CDS) has been proposed to improve the performance of ad hoc wireless networks. In general, a dominating set satisfies that every vertex in the graph is either in the set or adjacent to a vertex in the set. A CDS is a dominating set that also induces a connected sub‐graph. However, finding the minimum connected dominating set (MCDS) is a well‐known NP‐hard problem in graph theory. Approximation algorithms for MCDS have been proposed in the literature. Most of these algorithms suffer from a poor approximation ratio, and from high time complexity and message complexity. In this paper, we present a new distributed approximation algorithm that constructs a MCDS for wireless ad hoc networks based on a maximal independent set (MIS). Our algorithm, which is fully localized, has a constant approximation ratio, and O(n) time and O(n) message complexity. In this algorithm, each node only requires the knowledge of its one‐hop neighbours and there is only one shortest path connecting two dominators that are at most three hops away. We not only give theoretical performance analysis for our algorithm, but also conduct extensive simulation to compare our algorithm with other algorithms in the literature. Simulation results and theoretical analysis show that our algorithm has better efficiency and performance than others. Copyright © 2005 John Wiley & Sons, Ltd. 相似文献