真空蒸发沉积VOPc薄膜及磁场对薄膜结构与性能的影响

用真空蒸发制备了酞菁氧钒 (VOPc)薄膜 ,并在磁场中进行了热处理。用X光电子能谱、X射线衍射、紫外 可见吸收光谱、原子力显微镜等手段对制备的薄膜进行了表征。结果表明沉积的酞菁氧钒薄膜为α 型 ,成分接近酞菁氧钒的分子式。制备的薄膜在磁场中进行了热处理 ,发现磁场使酞菁氧钒薄膜性质发生改变 :UV VIS吸收谱Q带发生红移 ;XRD谱图衍射峰强度明显增强 ,峰位略有变化 ;原子力显微镜 (AFM)分析发现晶粒大小无明显变化。以上结果说明磁场的存在使得VOPc分子在热处理过程中发生了定向的排列     

固体火箭发动机喷管用C/C复合材料的研究进展

C/C复合材料已成为固体火箭发动机(SRM)最理想的喷管材料。综述了国内外SRM喷管用C/C复合材料的研究进展、应用状况以及烧蚀性能的研究状况,展望了今后C/C复合材料喷管的发展趋势。     

A Parallel Deadlock Detection Algorithm with O(1) Overall Run-time Complexity

This article proposes a novel parallel, hardware-oriented deadlock detection algorithm for multiprocessor system-on-chips. The proposed algorithm takes full advantage of hardware parallelism in computation and maintains information needed by deadlock detection through classifying all resource allocation events and performing class specific operations, which together make the overall run-time complexity of the new method O(1). We implement the proposed algorithm in Verilog HDL and demonstrate in the simulation that each algorithm invocation takes at most four clock cycles in hardware.     

一种高抗干扰的DSP输入输出信号传输电路的设计

介绍和比较了现有的DSP输入输出信号传输方法,设计了一种高抗干扰的DSP输入输出信号传输电路,论述了该电路工作原理,给出了电路主要参数的设计计算。通过实验验证了该传输电路的可行性。     

A Newly Developed Non, Destructive Tritium Measurement Technique and Its Application to V-4Cr-4Ti Alloy

A non-destructive and in-situ technique for the measurement of tritium in materials, namely β-ray-induced X-ray spectrometry （BIXS）, has been developed recently. In the present study a V-4Cr-4Ti alloy was pre-heated at 1000℃ for 2 h to form a recrystallization structure before the tritium absorption experiments were conducted. Firstly the hydrogen isotope gas was charazterized by means of a quadrupole mass spectrometer （QMS） and a small-sized ionization chamber. Then hydrogen isotope absorption tests of V-4Cr-4Ti alloy were performed at 400 ℃ and the atomic concentration of hydrogen isotope in V-4Cr-4Ti alloy was estimated as 0.17% with a tritium content of approximately 2.5 ppm. Experimental results indicate that BIXS is a quite useful tool for quantitatively measuring the tritium content and tritium distribution in the surface layers of vanadium alloys and no strong trapping effects of tritium exist in the pre-heated V-4Cr-4Ti alloy.     

重庆温泉寺及其寺庙园林史略

本文以重庆温泉寺庙园林为例,说明现在重庆园林布局仍以寺庙建筑为中心,组成严整的东西对称格局,其建造充分体现了“天人合一”的思想境界和“道”的自然无为的原则。     

The oxidation of two ternary Ni-Cu-10 at.% Al alloys in 1 atm of pure O2 at 800-900 °C

The oxidation of the ternary alloys Ni-45Cu-10Al and Ni-30Cu-10Al has been studied at 800-900 °C under 1 atm O₂. The presence of 10 at.% Al reduces significantly the oxidation rate of the corresponding Cu-Ni alloys during the initial oxidation stages, even before the establishment of a complete Al₂O₃ layer. The weight of individual sample of the two ternary Ni-Cu-10Al alloys at 800 °C increases more rapidly than at 900 °C during the initial oxidation stage. As oxidation proceeds, the weight gain at 800 °C slows down to a degree that the total weight gain after 24 h oxidation at 800 °C is less than that at 900 °C. Due to a faster formation of the Al₂O₃ layer, which suppresses earlier the further oxidation of Cu and Ni, the external region of the scales grown on Ni-45Cu-10Al contain much less Cu and Ni oxides than those grown on Ni-30Cu-10Al. The transition from the internal oxidation to the selective external oxidation of the most reactive component Al in Ni-Cu-Al alloys is favored by higher values of the Al content, of temperature and of the Cu/Ni ratio.     

双功能加氢精制催化剂在焦化富气制氢中的应用

介绍了JT-1G／JT-4加氢精制催化剂的烯烃饱和功能和有机硫转化功能；阐述了该催化剂在中石油辽河石化分公司、浙江工程设计院共同开发的用于焦化富气制氢原料的烯烃饱和及有机硫转化的新加氢工艺——逆流-等温-绝热加氢精制工艺中的使用情况。原料中体积分数13％～16％的烯烃经过加氢精制后降至0；原料中有机硫得到充分转化；焦化富气经过加氢精制后，满足了作为制氢原料的要求，降低了制氢成本。     

PLC模糊控制方法在电站辅机设备控制中的应用

本文具体论述了基于PLC的模糊闭环控制系统实现方法，该方法充分利用PLC的特点，使系统具有高可靠性，低成本，同时可实现较好的控制性能，对于大滞后，非线性，数字模型难以建立，且控制精度和快速性要求都不太高的辅机设备控制系统是一种较为理想的控制方案。     

M－Z型铌酸锂高速调制器

报道了采用行波电极结构的偏振型和与偏振无关型Ｔｉ：ＬｉＮｂＯ３高速强度调制器，其中与偏振无关的高速强度调制器是首次研制成功。