La2（MoO4）3：Eu均-花瓣状微／纳米结构的构筑及其荧光性能

在表面活性剂十二烷基硫酸钠（SDS）的作用下，采用温和的水热方法，成功制备了Eu掺杂的花瓣状L丑2（MoO4）3：Eu纳米微结构。这些形貌新颖的微米绒球的直径约3μm，由厚度30nm左右的纳米片次级结构单元自组装构筑而成，分散性良好，形貌规整、大小均一。通过XRD、SEM、TEM测试技术，研究了形貌的形成机理。由于具有良好的结晶度，这些花瓣状La2（MoO4）3：Eu纳米微结构显示出良好的发光性能。     

Hydriding and Dehydriding Characteristics of Mechanically Alloyed LaMg_(17) Ni Composite Material

Magnesiumandmagnesiumalloyshavebeenin vestigatedashydrogenstoragematerialsforseveralde cadesbecausefarmorehydrogenbyweightcanbestoredinthemthaninmostoftheothercurrentlyknownhydrogenstoragealloys .Moreover ,thehighnaturalabundanceofMg ,itslightmassandenviron mentalcompatibilitypotentiallymakemagnesiumoneofthemostprospectivecandidatesforfuturehydrogenstoragematerials .Unfortunately ,thepracticalappli cationofMganditsalloyshasbeenlimitedonlytocertainstoragedevicebecauseoftheirpoorhydriding dehydr…     

活性炭吸附法脱除加氢催化柴油中的硫化物

采用5种活性炭对加氢催化柴油进行吸附脱硫,通过对活性炭的吸附效果及工艺参数的研究,探索了活性炭吸附脱硫最适宜的工艺条件。实验结果表明,分别选用比表面积为854.97,1 108.61 m2/g,相应微孔平均孔径为0.581 4,0.627 4 nm的活性炭,在粒度为40~80目,流速为0.25 mL/m in,吸附柱高径比为30/1的条件,可将不同原料油中有机硫含量分别从1 354.96,665.50μg/g降至360.40,69.61μg/g,脱硫率分别为73.40%和89.54%;在20~100℃时,随着温度的升高,活性炭吸附脱硫效果增强。     

北京火车站抗震鉴定与加固技术

北京火车站是首都重要的标志性建筑之一 ,195 9年建成 ,当时按 7度设防考虑 ,存在着许多不符合抗震要求的问题 ,一些设施也明显不能满足现代使用功能要求。北京火车站抗震加固与改造设计项目组 ,运用多种先进的加固手段 ,在保持原建筑外貌不变的前提下 ,实现了抗震能力和改善使用功能的协调 ,取得了大型公共建筑加固改造的新经验     

弹药内弹道性能检验新方法数学模型的建立

本文对弹药内弹道性能检验的传统方法存在的问题进行了分析,提出了一种新的检验方法,重点对新的检验方法的数学模型的建立过程进行了论述。并对数学模型的精度进行了分析、检验和验证。     

油田开发经济运行质量研究与应用

提出了油田开发经济运行质量的研究方法和技术思路。对胜利油区几种典型的油藏类型进行了经济运行质量评价。以老河口油田桩106块为例，提出了提高油田经济运行质量的三条基本途径，取得了较好的实际应用效果。     

Reduced drug accumulation and multidrug resistance in human breast cancer cells without associated P-glycoprotein or MRP overexpression

MCF-7 human breast cancer cells selected in Adriamycin in the presence of verapamil developed a multidrug resistant phenotype, which was characterized by as much as 100,000-fold resistance to mitoxantrone, 667-fold resistance to daunorubicin, and 600-fold resistance to doxorubicin. Immunoblot and PCR analyses demonstrated no increase in MDR-1 or MRP expression in resistant cells, relative to parental cells. This phenotype is similar to one previously described in mitoxantrone-selected cells. The cells, designated MCF-7 AdVp, displayed a slower growth rate without alteration in topoisomerase II alpha level or activity. Increased efflux and reduced accumulation of daunomycin and rhodamine were observed when compared to parental cells. Depletion of ATP resulted in complete abrogation of efflux of both daunomycin and rhodamine. No apparent alterations in subcellular daunorubicin distribution were observed by confocal microscopy. No differences were noted in intracellular pH. Molecular cloning studies using DNA differential display identified increased expression of the alpha subunit of the amiloride-sensitive sodium channel in resistant cells. Quantitative PCR studies demonstrated an eightfold overexpression of the alpha subunit of the Na+ channel in the resistant subline. This channel may be linked to the mechanism of drug resistance in the AdVp cells. The results presented here support the hypothesis that a novel energy-dependent protein is responsible for the efflux in the AdVp cells. Further identification awaits molecular cloning studies.     

Synthesis, structure and fluorescence properties of a highly stable indium(III)-2,5-pyridinedicarboxylate coordination polymer

The hydrothermal reaction of 2,5-pyridinedicarboxylic acid (H₂PDC), diethylene triamine and In(NO₃)₃·4.5H₂O gave rise to a two-dimensional (2D) coordination polymer In(OH)(2,5-PDC). This compound crystallizes in the orthorhombic space group Iba2, with cell parameters, a = 12.656(3) Å, b = 20.114(4) Å, c = 6.2216(1) Å, V = 1583.9(5) Å³ and Z = 8. Its structure contains one-dimensional In–O–In–O– chains, which are further linked by 2,5-PDC ligands into a 2D supramolecular neutral framework. The adjacent 2D layers are parallel with each other and construct a three-dimensional framework via hydrogen bands. At room temperature, the compound exhibits intense photoluminescence. On the basis of the results of TG/DTA analyses, the structure is thermally stable up to 390 °C.     

钙钛矿型钛酸锶的制备、结构与性能

钛酸锶是一种具有重要电性质的陶瓷材料 ,因而在工业上得到了广泛的应用。本文介绍了钛酸锶的几种常见的合成方法 ,并简要的介绍了钛酸锶的结构与性能