老挝占巴色铝土矿可溶性试验研究

本文对老挝占巴色铝土矿进行了不同压力、温度、碱浓度条件下的氧化铝溶出率试验研究,并初步考察赤泥的沉降情况。试验结果:该铝土矿溶出率可达88.9%,显示出该矿良好的工业价值。     

Effect of Magnetic Field on Properties and Element Distribution of Ni-Based WC Composite Coatings

The Ni-based WC coatings enhanced by WC particle were fabricated on FV520B by plasma cladding device. The influence of magnetic force on the microstructure and performance of the coating was investigated. If the magnetic field does not exist, the microstructure of coating is a cluster of block-shaped structures; it is observably different from the dendritic and crumbling snowflake-like structures formed under transverse and longitudinal magnetic fields. The WC particles were distributed at the grain boundary. With the effect of longitudinal magnetic field, wear resistance and erosion resistance of coatings improved markedly. When axial magnetic field intensity came to 38 mT, the microhardness of coatings reached a maximum value, 720 HV0.2. Electron probe microanalyzer (EPMA) indicates the metallurgical combination at the interface and element interdiffusion happened between the coating and substrate.     

SDZ地面测井系统配接SBT扇区水泥胶结测井仪的方法研究

以2种SDZ(地面测井系统)配接SBT(扇区水泥胶结测井仪)为例,介绍了配接下井仪器的组成和信号调试以及现场测井应用。从研究的角度详细介绍了配接不同时序下井仪器的方法和信号处理电路,分析了测井应用中的影响因素。经现场测井应用表明,配接八扇区水泥胶结测井仪的性能稳定、精度高,满足了测井需要。     

某测量吊舱运动框架结构设计与分析

光电测量吊舱工作于高速、高空、高风载、高振动条件下,且受制于其气动特性,故体积无法太大,因此吊舱舱体内部的结构部件需要完全适应上述苛刻条件,且做到结构紧凑。首先分析了吊舱头部局促空间的设计要求。该吊舱头部最大外形尺寸为390 mm600 mm。但该空间内包含三对轴承、四个框架、两套可见光电视系统、一套光路快速控制系统及相关的电路、控制陀螺等元器件。因此在如此狭小的空间内合理配置如此多的系统必须进行相应的结构优化设计与分析。根据充分的论证分析提出了一系列设计要求。根据设计要求对吊舱头部关键部件进行了参数计算、型号选择、结构设计。应用MSCPATRAN软件对基座和横滚框架进行了有限元模态和静力学分析,验证了设计的合理性。     

鄂尔多斯盆地华庆地区延长组6段深水致密砂岩填隙物特征及对储层发育的影响

深水重力流成因的致密砂岩油藏是目前非常规油气勘探开发的新热点。深水环境水动力复杂,填隙物类型及含量变化大,储层微观非均质性强,严重制约了深水沉积储层油气资源的勘探开发进程。通过铸体薄片、扫描电镜、矿物自动识别与分析系统（QEMSCAN）、电子探针和纳米CT等实验分析手段,对鄂尔多斯盆地华庆地区延长组6段（长6段）深水致密砂岩不同填隙物的微观特征进行了精细表征,探讨了不同填隙物对储层孔隙结构及物性的影响。结果表明：杂基并非完全致密,经过成岩改造后的杂基能够产生一定数量的杂基晶间孔和杂基溶孔,孔径介于20~1 000 nm,构成了复杂的杂基次生孔隙网络。当杂基含量≤7%时,杂基次生孔隙发育,对储层产生积极影响。当杂基含量＞7%时,杂基次生孔隙发育程度降低,加剧了储层的致密。粘土矿物胶结物的晶间孔在一定程度上缓解了孔隙度的降低,但不同粘土矿物的形态、产状及对储层造成的敏感性又加剧了粘土矿物与渗透率关系的复杂性。伊利石、伊/蒙混层和绿泥石含量的高值区,储层物性通常较差,优质储层多分布在高岭石的发育区;碳酸盐和硅质胶结物是深水致密砂岩储层物性降低的主要因素。综合分析认为,杂基含量≤7%,且高岭石胶结物相对发育的地区是深水致密砂岩油藏勘探开发的重点区域。     

Preparation and Characterization of Gd3Sc2Ga3O12 Polycrystalline Material by Co-Precipitation Method

Gd3Sc2Ga3O12 polycrystalline material for single crystal growth was prepared with Ga, Gd2O3 and Sc2O3 as starting materials and aqueous ammonia as the precipitator by co-precipitation method. The precursors sintered at various temperatures were characterized by infrared spectra （IR）, X-ray diffractometry （XRD） and transmitted electron microscopy （TEM）. The results showed that pure GSGG phase could be obtained at 900 ℃. The sintered powders were well-dispersed and less-aggregated in the sintered temperature range of 900 - 1000 ℃. XRD and TEM show that the polycrystalline particle sizes of the polycrystalline powders were about 20 - 50 nm. Compared with the method that Ga2O3, Gd2O3 and Sc2O3 were mixed directly and sintered to get polycrystalline materials, the synthesized temperature was lower and sintered time was shorter. Thus co-precipitation was a good method to synthesize GSGG polycrystalline material.     

紫外诱变和丁醇驯化复合选育高产丁醇菌株

本研究以Clostridium beijerinckii NCIMB 8052为出发菌株,利用紫外诱变和高丁醇环境驯化相结合的方法复合选育,最终获得一株耐丁醇的高产突变株,命名为Clostridium beijerinckii ZL01.与出发菌株8052相比,ZL01对丁醇初始浓度的耐受能力从10g/L提高到11g/L.5L发酵罐的分批发酵结果表明,丁醇的产量从10.34g/L增加为15.01g/L,提高45.16％;总溶剂从12.87g/L增加为19.55g/L,提高49.01％;发酵周期缩短4h,发酵强度从0.27g/(L·h)提高为0.44g/(L·h),遗传稳定性实验表明,该菌株连续传代20次,溶剂产量稳定,菌株无明显退化.     

纺织业厂房通风系统改造

介绍了纺织业厂房常用的通风方式,分析了通风系统存在的不足,提出了通风系统的改造方案及节能通风措施,为纺织业厂房通风系统节能环保运行提供新思路和新方法.     

Microstructure and thermal stability of a Ni-Cr-Co-Ti-V-Al high-entropy alloy coating by laser surface alloying

A Ni-Cr-Co-Ti-V-Al high-entropy alloy (HEA) coating with a BCC phase and (Ni, Co)Ti₂ compounds was synthesized successfully by laser surface alloying on a Ti-6Al-4V substrate. The microstructure of as-synthesized coatings is typical, namely, the microstructure from the coating to the substrate changes from equiaxed grains to columnar grains. After remaining at 900 °C for 8 h, the constituent phases remain unchanged. However, owing to the unceasing dissolution of the Ti element, the lattice parameter of the BCC HEA phase changes from 3.06 Å to 3.16 Å. The thermoanalysis results show that the oxidation film on the Ni-Cr-Co-Ti-V-Al HEA coating is mainly composed of TiO₂, V₂O₅, and NiO. The oxidation resistance of this HEA coating may be due to the existence of NiO and the alloying elements Al, Cr, and Co; the oxidation phenomenon should be responsible for the mass increase in the thermogravimetry process. The differential scanning calorimetry and the dynamic differential scanning calorimetry curves show that the synthesized HEA coating is stable below 1005 °C.