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41.
The aim of the present paper is to review the recent progress in the synthesis of in situ particle reinforced aluminum composites
using thermal, mechanical and combined mechanical-thermal activation of aluminothermic reduction reactions. The combination
of combustion synthesis (CS) and mechanosynthesis (MS) is the most recent development in the processing of advanced materials
like micro and nano aluminum based composites. The combined mechanical thermal synthesis (MTS) has widened the possibilities
for both CS and MS. MTS holds great potential for commercial viability and offers exciting processing route for the synthesis
of advanced materials. Enhanced reaction kinetics and extended concentration limits in MTS are demonstrated by illustrating
the synthesis of aluminum based nanocomposite involving Al–CeO2. 相似文献
42.
Hideo Sawada Hiroshi Kakehi Masashi Koizumi Yoshihiro Katoh Masashi Miura 《Journal of Materials Science》2007,42(17):7147-7153
Fluoroalkyl end-capped N-(1,1-dimethyl-3-oxobutyl)acrylamide oligomer [RF-(DOBAA)
n
-RF] reacted with tetraethoxysilane (TEOS) and silica nanoparticles in the presence of low-molecular weight biocides such as
hibitane, hinokitiol, and hinokioil under alkaline conditions to afford RF-(DOBAA)
n
-RF/silica nanocomposites-encapsulated these biocides in excellent to moderate isolated yields. Fluoroalkyl end-capped N,N-dimethylacrylamide oligomer [RF-(DMAA)
n
-RF] and acrylic acid oligomer [RF-(ACA)
n
-RF]/silica nanocomposites-encapsulated hibitane were obtained under similar conditions. Dynamic light scattering measurements
showed that the size of these fluorinated nanocomposites-encapsulated biocides thus obtained is nanometer size-controlled.
Additionally, these fluorinated nanocomposites were shown to have a good dispersibility and stability in methanol and water.
Of particular interest, these fluorinated nanocomposites-encapsulated biocides were found to have a good antibacterial activity
against Staphylococcus aureus, and these nanocomposites were applied to the surface modification of traditional organic polymers such as poly(methyl methacrylate). 相似文献
43.
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45.
Mamiko Hori Cécile Pagnoux Jean-François Baumard Masayuki Nogami 《Journal of Materials Science》2007,42(1):80-86
A new method is proposed to produce gold nanoparticles (GNP) by in situ reduction of a gold salt dissolved in water. The reducing
agent used is Tiron instead of the citrate anion most often mentioned in literature. The influence of various parameters has
been investigated, such as the content of Tiron with respect to that of the precursor of gold HAuCl4, or the initial pH of the solution after mixing of reactants. It is shown that Tiron also exerts a positive influence as
a dispersant, which impedes agglomeration of gold nanoparticles. The typical average size of GNP synthesized in the present
work is close to 7 nm. 相似文献
46.
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49.
In this paper, two brittle fracture problems are numerically simulated: the failure of a ceramic ring under centrifugal loading and crack branching in a PMMA strip. A three‐dimensional finite element package in which cohesive elements are dynamically inserted has been developed. The cohesive elements' strength is chosen to follow a modified weakest link Weibull distribution. The probability of introducing a weak cohesive element is set to increase with the cohesive element size. This reflects the physically based effect according to which larger elements are more likely to contain defects. The calculations illustrate how the area dependence of the Weibull model can be used to effectively address mesh dependency. On the other hand, regular Weibull distributions have failed to reduce mesh dependency for the examples shown in this paper. The ceramic ring calculations revealed that two distinct phenomena appear depending on the magnitude of the Weibull modulus. For low Weibull modulus, the fragmentation of the ring is dominated by heterogeneities. Whereas many cracks were generated, few of them could propagate to the outer surface. Monte Carlo simulations revealed that for highly heterogeneous rings, the number of small fragments was large and that few large fragments were generated. For high Weibull modulus, signifying that the ring is close to being homogeneous, the fragmentation process was very different. Monte Carlo simulations highlighted that a larger number of large fragments are generated due to crack branching. Copyright © 2003 John Wiley & Sons, Ltd. 相似文献
50.