AZ31镁合金板材在热处理中组织和性能的演变

研究了热处理对AZ31镁合金轧制板材显微组织、室温力学性能和成形性能的影响。热处理温度在300～350℃范围时,显微组织观察表明,热处理后孪晶消失、组织逐渐趋于均匀化、平均晶粒尺寸变小;力学性能和胀形性能测试结果表明,板材的屈服强度明显降低、抗拉强度略有下降、屈强比降低、伸长率提高,杯突值提高。在350℃、15 min空冷处理后,AZ31镁合金板材的综合性能最好。     

One‐Step Hydrothermal Synthesis of 2D Hexagonal Nanoplates of α‐Fe2O3/Graphene Composites with Enhanced Photocatalytic Activity

There has been significant progress in the field of semiconductor photocatalysis, but it is still a challenge to fabricate low‐cost and high‐activity photocatalysts because of safety issues and non‐secondary pollution to the environment. Here, 2D hexagonal nanoplates of α‐Fe₂O₃/graphene composites with relatively good distribution are synthesized for the first time using a simple, one‐step, template‐free, hydrothermal method that achieves the effective reduction of the graphene oxide (GO) to graphene and intimate and large contact interfaces of the α‐Fe₂O₃ nanoplates with graphene. The α‐Fe₂O₃/graphene composites showed significantly enhancement in the photocatalytic activity compared with the pure α‐Fe₂O₃ nanoplates. At an optimal ratio of 5 wt% graphene, 98% of Rhodamine (RhB) is decomposed with 20 min of irradiation, and the rate constant of the composites is almost four times higher than that of pure α‐Fe₂O₃ nanoplates. The decisive factors in improving the photocatalytic performance are the intimate and large contact interfaces between 2D hexagonal α‐Fe₂O₃ nanoplates and graphene, in addition to the high electron withdrawing/storing ability and the highconductivity of reduced graphene oxide (RGO) formed during the hydrothermal reaction. The effective charge transfer from α‐Fe₂O₃ nanoplates to graphene sheets is demonstrated by the significant weakening of photoluminescence in α‐Fe₂O₃/graphene composites.     

硫铝酸盐水泥负温混凝土的应用

介绍硫铝酸盐早强水泥的特性、施工方法及注意事项。为严寒地区冬季砼施工提供了经验。     

东海乌参肽对小鼠酒精性肝损伤及肠道菌群的调节作用

目的：探讨东海乌参肽（Acaudina leucoprocta peptides,ALPs）对小鼠酒精性肝损伤和肠道菌群的调节作用。方法：将45 只C57BL/6N雄性小鼠随机分为正常组、模型组、阳性药物组（80 mg/（kg mb·d）水飞蓟宾）、ALPs低剂量组（200 mg/（kg mb·d）ALPs）和ALPs高剂量组（400 mg/（kg mb·d）ALPs）。采用慢性酒精干预3 周后进行急性酒精灌胃建立小鼠肝损伤模型,检测小鼠血清和肝脏组织相关生化指标、观察肝脏和结肠组织形态学变化;取小鼠粪便进行16S rRNA测序,分析肠道菌群多样性。结果：ALPs可以显著改善小鼠的肝脏和结肠组织损伤,降低酒精性肝损伤血清标志物丙氨酸转氨酶和天冬氨酸转氨酶的活力,提升乙醇代谢相关酶的活力,抑制酒精性肝损伤小鼠肝脏中的脂肪蓄积,减少肿瘤坏死因子-α、白介素（interleukin,IL）-1β、干扰素-γ和IL-6的分泌及氧化应激标志物丙二醛的含量。ALPs显著改善小鼠肠道菌群的α-多样性和β-多样性,调节多种门、纲、科细菌的相对丰度,改善乙醇诱导的小鼠肠道菌群紊乱并使其趋于正常。结论：ALPs对乙醇诱导的小鼠肝损伤具有明显的保护作用,其机制与ALPs抗氧化、抗炎和改善肠道菌群紊乱相关。     

认知无线电网络中物理层频谱检测算法的研究

频谱检测是认知无线电网络(CRN)的关键技术之一,本文对认知无线电网络中物理层频谱检测的算法进行了研究.首先阐述了经典检测算法的应用场景、检测性能和设备实现复杂度,针对经典算法中的问题和不足,提出一系列改进型算法以及利用信号与噪声相关性差异的新型检测算法,并对各种检测算法进行了分类比较,在此基础上提出了结合不同检测算法优势的CRN检测策略,最后指出可能的研究方向.     

既有地下空间改建成大型地铁枢纽的综合施工技术

利用既有地下空间改建成地铁交通换乘枢纽,是城市发展和轨道交通建设的另类延伸,它避免了在闹市中心区“大开大挖”,在施工周期、建设成本以及社会效益等多个方面有着明显的优势。通过周密的研究和精心的施工组织,对此类改建进行了完美的演绎,上海市港汇广场地下空间改建轨道交通枢纽工程圆满完成．     

地层倾角测井在沉积微相研究中的应用

针对雁木西油田白垩系低阻油层受沉积相带及其断裂、构造和岩性等多种因素控制影响,测井信息应用难度增大的特点,采用地层倾角测井资料确定古水流方向、砂体延伸、层理构造和微相特征。利用倾角方位频率矢量统计,确定出白垩系K1s3、K1s2、K1s1目的层段古水流及其相应河道砂体延伸方向为北北东20°。利用层理构造倾角模式分析,确定出白垩系K1s3、K1s2、K1s1期分别发育楔状交错层理、波状斜层理、波状交错层理和水平层理,结合岩心、井径、自然伽马和微侧向电阻率曲线特征,分别阐明白垩系K1s3、K1s2到K1s1期水动力能量由较高到较低变化,形成了扇三角洲前缘扇中的水下辫状河道到扇端的浅水河道有利微相砂体发育带,由南南西向北北东方向展布,控制研究区最为有利的油气储集砂体分布。     

Mass transfer area in a multi-stage high-speed disperser with split packing

In this study, the mean droplet diameter in the cavity zone and the total mass transfer area of a multi-stage highspeed disperser(HSD) reactor with different packing combinations were measured and evaluated. The effects of rotational speed and packing radius, as well as the packing ring radius and numbers, on the mean droplet diameter and the total mass transfer area were evaluated. A model was established to calculate the mass transfer area in the cavity zone in the HSD reactor, and it was found that the packings contribute 61%–82% of the total mass transfer area. A correlation for predicting the mass transfer area in the packing zone was regressed by the dimensionless analysis method. An enhancement factor based on the mass transfer area in the packing zone was proposed to evaluate the effect of packing combination on mass transfer area. Two optimum packing combinations were proposed in consideration of the mean droplet diameter and the enhancement factor.     

Zn对Cu-Zn-Al催化乙酸甲酯加氢反应的影响

采用共沉淀法制备Cu-Zn-Al催化剂,采用XRD、N2等温吸附-脱附、SEM、H2-TPR、XPS和ICP-OES等手段对催化剂进行表征。结果发现,Zn的加入降低了Cu-Zn-Al催化剂颗粒的团聚程度,提高了活性中心Cu组分的分散度。并且Zn含量的改变可以影响Cu组分的价态分布,进而影响其催化性能。当n(Cu)/n(Zn)=2/3时,n(Cu+)/n(Cu0)为1.04,Cu-Zn-Al对乙酸甲酯(MA)加氢反应具有最优的催化性能。在反应温度为240 ℃、反应压力为3.0 MPa、n(H2)/n(MA)=20的最优条件下,Cu-Zn-Al催化乙酸甲酯反应中乙酸甲酯转化率为98.8%,甲醇和乙醇选择性分别为99.4%和98.7%。对Cu-Zn-Al催化剂进行300 h寿命测试,乙酸甲酯转化率一直稳定在98%以上,甲醇和乙醇选择性则分别保持在99%和98%左右。