高温深层缓速酸化优化研究及应用

针对临南油田酸化效果差的问题,从油藏地质特点出发,分析了制约其酸化效果的主要因素,即地层温度、铁离子二次沉淀、地层深部改造等。通过室内研究,优选出一种高性能的缓速酸,该酸液具有溶蚀率高、缓速性能好、能有效防止铁离子二次沉淀、与地层水配伍性好等特点。同时还对酸化施工工艺进行了优化,配套了适合的返排工艺。该工艺在现场应用后,酸化效果得到了明显的改善。     

Upconversion emission of a novel glass ceramic containing Er: BaYF5 nano-crystals

In order to develop highly efficient upconversion (UC) material, Er³⁺-doped oxyfluoride glass ceramics containing BaYF₅ nano-crystals were fabricated for the first time. The randomly distributed BaYF₅ nano-particles with the size of nearly 25 nm precipitated from the glass matrix at about 700 °C, then tended to aggregate slightly with the increase of heating temperature, resulting in the enhancement of Er³⁺ UC emission in the wavelength ranging from 500 nm to 700 nm. The UC process was found very sensitive to Er³⁺ content: with the increase of Er³⁺ content from 0.5% to 1.0%, the UC intensity behaved with drastic exaltation; while further increasing Er³⁺ content to 2.0% resulted in a notable fluorescence quenching. Significantly, the UC efficiency of present glass ceramic preponderates notably over that of the previously reported glass ceramic containing LaF₃, implying its superior UC potentiality.     

一种基于循环小波累积量的谐波恢复方法

循环统计量是乘性和加性噪声中谐波恢复问题的主要分析工具之一。本文在其基础上提出了一种新的理论与方法——基于循环小波累积量的谐波恢复方法。首先,提出了循环小波累积量的定义。然后,建立了基于一阶、二阶、三阶循环小波累积量的谐波分量的频率和相位的估计方法。在此基础上,采用了一种可调参数的小波,通过调节其参数来改善传统方法中频率分辨率低的缺陷。最后给出了模拟实验结果。     

六通道瞬态光学高温计

六通道瞬态光学高温计是在可见光和近红外光谱范围内 ,把光源的热辐射取出六个波段进行测量。每个波段信号通过各自的光纤传输、光电倍增管探测和记录仪器记录。系统的时间分辨率小于 30 ns,冲击温度测量范围为 2 30 0～ 90 0 0 K,测量误差小于 5 % ,给出了以碘化钠、硝基甲烷和空气为样品的若干实验结果     

含过期火药粉状工业炸药的研究

文章概要论述了一种新型民用炸药－含过期火药粉状工业炸药在配方、制造工艺等方面所进行的实验研究。结果表明，该炸药性能良好、制造技术安全可靠，值得推广。     

奇异摄动系统的极限解

本文在前人工作的基础上,利用广义函数理论讨论了一般形式下的奇异摄动系统E(ε)(?)=A(ε)x+B(ε)u在v→0~+时的极限解问题,得出了这一极限解存在的充要条件。     

The effect of insulin-like growth factor-1 on cyclic change of tendon cell

BACKGROUND: Myoclonus is a possible side effect of opioid therapy, and have been described following systemic as well as spinal application. CASE REPORT: We report the case of a patient with metastatic carcinoma of the rectum who developed myoclonus following administration of high-dose epidural combined with iv morphine. This complication occurred with maximum daily doses of 300 mg epidurally and 80 mg intravenously and disappeared completely after dose reduction. Treatment trials are presented, the pathophysiology of the myoclonus is discussed. CONCLUSION: For treatment of opioid-induced myoclonus a dose reduction or a change of the opioid should be considered as well as symptomatic treatment with benzodiazepines or baclofen.     

Enhancement effect of organic solvents on the line intensity of lower power argon ICP-AES：Part I On the nebulization procedure

The procedure of nebulization was studied with the introduction of ethanol into a lower power argon ICE It was found that as ethanol introduced, the physical properties of solutions changed, which results in an improvement on the nebulization efficiency. An empirical relationship between the concentration of the aerosol and the solution properties ( viscosity, density, and surface tension) is presented.     

时效处理对 TiNi 合金相变与性能的影响

通过用ＴＥＭ等方法研究热处理制度（固溶处理、时效处理）对ＴｉＮｉ合金相变组织和性能的影响，找出了最佳热处理制度。结果表明，在４５０～５００℃进行时效处理，Ｔｉ－５０．８ａｔ％Ｎｉ的合金出现了大量的Ｔｉ３Ｎｉ４相，且恢复率最高。